CN209108139U - A kind of ultra micro extraction equipment - Google Patents

A kind of ultra micro extraction equipment Download PDF

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Publication number
CN209108139U
CN209108139U CN201821295444.2U CN201821295444U CN209108139U CN 209108139 U CN209108139 U CN 209108139U CN 201821295444 U CN201821295444 U CN 201821295444U CN 209108139 U CN209108139 U CN 209108139U
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pipeline
fluid reservoir
ultra micro
feed inlet
communicated
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王升贵
唐川
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JIUXIANZUN HUOSHAN DENDROBIUM Co Ltd
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JIUXIANZUN HUOSHAN DENDROBIUM Co Ltd
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Abstract

The utility model discloses a kind of ultra micro extraction equipments, including service sink, machine for traditional Chinese medicinal material,table cutting, water purification system, colloid mill, the first fluid reservoir, the second fluid reservoir, single-effect concentrator, tube centrifuge, spherical scraper concentrator, low temperature continuous vacuum film drier to be sequentially connected together by pipeline, transmission device;This ultra micro extraction equipment can sequentially realize a whole set of process of Dendrobidium huoshanness extraction, and high degree of automation is practical, can improve the utilization rate of Dendrobidium huoshanness to the greatest extent, save plant resources;Whole process sufficiently relies on device height difference to transmit using pipeline, reduces pollution section, promotes working efficiency, low energy consumption, environmentally protective, moreover it is possible to processing cost be greatly reduced, be suitable in the industry cycle popularizing.

Description

A kind of ultra micro extraction equipment
Technical field
The utility model belongs to medicinal plant processing technique field, and in particular to a kind of ultra micro extraction equipment.
Background technique
Dendrobidium huoshanness (Dendrobium huoshanense CZ.Tang et S.J.Cheng) is orchid family Dendrobium many years Raw herbaceous plant is commonly called as " rice dry measure used in former times ", originates in Huoshan and neighborhood.Dendrobidium huoshanness is recorded in " Mingyi Bielu " earliest, because Its is rare rare and famous domestic and international." hundred careless mirrors " record: " dendrobium nobile has a kind of short cun of shape to be permitted when close, thin such as wick, color blueness Huang, nozzle it is sweet in flavor, it is micro- to have sliding saliva, be six mansion An Zhou and Ying Zhou Huoshan County out, name Dendrobidium huoshanness, most preferably." modern research shows that There is the ingredients such as Dendrobidium huoshanness polysaccharide rich in, alkaloid, polyphenol, amino acid, microelement voiceless sound improving eyesight, liver protection to protect Throat, nourishing Yin and clearing heat, nourishing the stomach to improve the production of body fluid, inhibition growth of tumour cell, strengthen immunity and other effects.
In the deep development and utilization of resources of medicinal plant, the extraction of effective ingredients in plant be highly important link it One.The selection of extracting method and extract equipment be the key that determine can realize plant resources efficiently, higher value application.Currently, It is existing to take based on more traditional extracting method extracts with the single tank of interval, in batches in terms of the deep processing of Dendrobidium huoshanness, or It is aided with stirring, supersonic generator or microwave heating equipment, but the biggish leaching liquor of the process requirement (10-20 times) and longer Extraction time (3-8h, 3-5 times), at the same the extraction yield (ratio that extract weight accounts for crude drug dry weight) of the technique and effectively Constituents extraction rate (%) (amount of effective component accounts for the ratio of effective component total amount in crude drug in extract) is still undesirable, respectively For 15%-25% and 10%-15%, prolonged decoct increases energy consumption, and production cost is high.And in this process, greatly Part is thermo-labile, oxidizable ingredient is seriously damaged, and extract obtained effect certainly will have a greatly reduced quality.
Ultra micro extraction equipment is the improvement to traditional extract equipment technique, using colloid mill can to Dendrobidium huoshanness into The cell partial size of the extraction of row ultra micro, treated Dendrobidium huoshanness is between 2-200 μm, wherein 50 μm or less partial sizes account for 80%, the effective component of Dendrobidium huoshanness and nutriment can be made sufficiently to discharge, form suspension, while can preferably reduce The deep processing link of Dendrobidium huoshanness reduces processing cost.
Utility model content
The technical problem to be solved by the utility model is to: overcome the deficiencies of the prior art and provide a kind of ultra micro extraction Device obtains the effective component of Dendrobidium huoshanness to greatest extent, improves Dendrobidium huoshanness utilization rate, processing cost is greatly reduced.
The utility model solves above-mentioned technical problem using following technical scheme:
A kind of ultra micro extraction equipment, including service sink, machine for traditional Chinese medicinal material,table cutting, water purification system, colloid mill, the first liquid storage Tank, the second fluid reservoir, single-effect concentrator, tube centrifuge, spherical scraper concentrator, low temperature continuous vacuum film drier, lead to Piping, transmission device are sequentially connected together;
The service sink discharge end is connected with machine for traditional Chinese medicinal material,table cutting feeding end, the both ends of the water purification system respectively and cleaning Pond, colloid mill are communicated by pipeline;The machine for traditional Chinese medicinal material,table cutting discharge end and colloid mill upper end feed inlet pass through pipeline It communicates, and machine for traditional Chinese medicinal material,table cutting discharge end height is higher than colloid mill upper end;Colloid mill upper end feed inlet and first Fluid reservoir lower end is communicated by pipeline, and colloid mill upper end level is higher than the first fluid reservoir lower end, is lower than the first fluid reservoir Upper end;First fluid reservoir upper end and colloid mill upper end feed inlet are communicated by pipeline;Colloid mill lower end discharge port and Second fluid reservoir upper end is communicated by pipeline, and the second fluid reservoir lower end and single-effect concentrator upper end feed inlet are communicated by pipeline, Single-effect concentrator lower end discharge port and tube centrifuge lower end feed inlet are communicated by pipeline;Tube centrifuge upper end discharge port and Spherical scraper concentrator upper end feed inlet is communicated by pipeline, and spherical scraper concentrator lower end discharge port and low temperature continuous vacuum are thin The dry machine inlet of film is communicated by pipeline.
Further, the service sink is in rectangular parallelepiped structure, and bottom is equipped with a drain valve, is equipped with one in the service sink cavity Both ends have the groove profile sieve of hanging ring, and the bottom of the sieve is designed for movable, and packaged type escalator, which is caught on, to be hung Ring.
Further, the machine for traditional Chinese medicinal material,table cutting is provided with perpendicular type groove on a moving belt, is provided below in the conveyer belt Vibrating motor.
Further, the perpendicular type groove and vibrating motor be point-blank.
Further, the tube centrifuge carries out solid-liquid separation treatment, feed inlet, waste material row to Dendrobidium huoshanness concentrate It exports in the lower end of centrifugation component, discharge port is in the upper end of centrifugation component.
Further, the low temperature continuous vacuum film drier be will be concentrated in vacuo, Transmission system, spraying system and coating What system combined is dried device to Dendrobidium huoshanness concentrate.
The utility model technology is the utility model has the advantages that this ultra micro extraction equipment can sequentially realize a whole set of work of Dendrobidium huoshanness extraction Sequence, high degree of automation is practical, can improve the utilization rate of Dendrobidium huoshanness to the greatest extent, saves plant resources;Entirely Process sufficiently relies on device height difference to transmit using pipeline, reduces pollution section, promotes working efficiency, and low energy consumption, green Environmental protection, moreover it is possible to processing cost be greatly reduced, be suitable in the industry cycle popularizing.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of ultra micro extraction equipment described in the utility model embodiment;
Fig. 2 is the structural schematic diagram of service sink described in the utility model embodiment;
Fig. 3 is the structural schematic diagram of machine for traditional Chinese medicinal material,table cutting conveyer belt described in the utility model embodiment.
Specific embodiment
For convenient for those skilled in the art understand that technical solutions of the utility model, practical new to this now in conjunction with Figure of description Type technical solution is described further.
Embodiment one
Refering to fig. 1, present embodiment discloses a kind of ultra micro extraction equipment, including extraction, separation of solid and liquid and drying device, tools Body include be sequentially connected by pipeline with transmission device together with service sink 1, machine for traditional Chinese medicinal material,table cutting 2, water purification system 3, colloid Grinder 4, the first fluid reservoir 5, the second fluid reservoir 6, single-effect concentrator 7, tube centrifuge 8, spherical scraper concentrator 9, low temperature Continuous vacuum film drier 10.
1 discharge end of service sink is connected with 2 feeding end of machine for traditional Chinese medicinal material,table cutting by mobile liftable motor transmission device, institute The both ends for stating water purification system 3 are communicated with service sink 1, colloid mill 4 by pipeline respectively;The machine for traditional Chinese medicinal material,table cutting 2 discharges End and 4 upper end feed inlet of colloid mill are communicated by pipeline, and 2 discharge end height of machine for traditional Chinese medicinal material,table cutting is higher than colloid mill 4 Upper end;The 4 upper end feed inlet of colloid mill and 5 lower end of the first fluid reservoir are communicated by pipeline, and 4 upper end of colloid mill Height is higher than 5 lower end of the first fluid reservoir, is lower than 5 upper end of the first fluid reservoir;4 upper end of first fluid reservoir, 5 upper end and colloid mill Feed inlet is communicated by pipeline;4 lower end discharge port of colloid mill and 6 upper end of the second fluid reservoir are communicated by pipeline, are completed suddenly The extraction of mountain dendrobium nobile.
Second fluid reservoir, 6 lower end and 7 upper end feed inlet of single-effect concentrator are communicated by pipeline, under single-effect concentrator 7 It brings out material mouth and 8 lower end feed inlet of tube centrifuge is communicated by pipeline, completed using tube centrifuge 8 to single-effect concentrator 7 The concentrate of preparation carries out solid-liquid separation treatment, and feed inlet, waste gate are in the lower end of centrifugation component, and discharge port is in centrifugation group The upper end of part.
8 upper end discharge port of tube centrifuge and spherical 9 upper end feed inlet of scraper concentrator are communicated by pipeline, spherical scraper plate 9 lower end discharge port of inspissator and 10 feed inlet of low temperature continuous vacuum film drier are communicated by pipeline, and then are completed dried Journey.
The connecting valve 11 between the 4 upper end feed inlet of colloid mill and 5 lower end of the first fluid reservoir;First fluid reservoir Connecting valve 12 between 4 upper end feed inlet of 5 upper ends and colloid mill;4 lower end discharge port of colloid mill and the second fluid reservoir 6 Connecting valve 14 between upper end;Connecting valve 13 between the valve 12 and valve 14 again;Second fluid reservoir, 6 lower end and single-action are dense Connecting valve 15 between 7 upper end feed inlet of contracting device;7 lower end discharge port of single-effect concentrator and 8 lower end feed inlet of tube centrifuge it Between connecting valve 16;Connecting valve 17 between 9 upper end feed inlet of 8 upper end discharge port of tube centrifuge and spherical scraper concentrator.
Referring to Fig.2, the service sink 1 is in rectangular parallelepiped structure, bottom is equipped with a drain valve 11, in 1 cavity of service sink Groove profile sieve 12 equipped with one with elevating function, 12 aperture of sieve are 10-30 mesh, and both ends are provided with hanging ring 121, described The bottom of sieve 12 is designed for movable, and elevating function is controlled by packaged type escalator.Specific work process Are as follows: after cleaning, 1 bottom discharge valve 11 of service sink is opened, waste water is discharged from bottom, closes drain valve 11, re-injects pure Change water to be cleaned, recycle 3-5 times, after cleaning, waste water is discharged, hoist hook (not shown) is caught on into groove profile sieve Button is risen in 12 hanging ring 121 of net, starting, moves to above 2 hopper of machine for traditional Chinese medicinal material,table cutting, 12 bottom of groove profile sieve is opened, by Huoshan stone Dry measure used in former times pours into medicine cutter hopper.Compared to the prior art, the contaminant filters such as apparatus of the present invention silt are abundant, and cleaning efficiency is high;It passes It needs to pull Dendrobidium huoshanness out manually after the every cleaning of system service sink one time, after waste water discharge, rinses the adherency impurity such as silt, again Dendrobidium huoshanness is put into service sink, cleaning terminates to be transferred to medicine cutter hopper manually, and this device can greatly promote work effect Rate.
Refering to Fig. 3, the machine for traditional Chinese medicinal material,table cutting 2 is provided in 21 direction of advance of conveyer belt perpendicular on conveyer belt 21 Type groove 211, the perpendicular type groove 211 are equidistant arranged in parallel;The diameter of perpendicular type groove 211 is depending on fresh diameter, can wrap Wrapping fresh item is principle;Vibrating motor 212 is provided below in the conveyer belt 21, has vibrating function, perpendicular 211 He of type groove Vibrating motor 212 point-blank, increases perpendicular type groove 211 in transmission belt 21 and has the device of vibrating function, make fresh item quilt It smoothes out with the fingers along at a direction, is conducive to dissection.
The colloid mill 4 carries out ultra micro extraction to Dendrobidium huoshanness, while can manually adjust power and gap.Place The cell partial size of Dendrobidium huoshanness after reason is between 2-200 μm, wherein 50 μm or less partial sizes account for 80%;Meanwhile it is described 2 fluid reservoirs of connection, the first fluid reservoir 5 temporarily store colloid mill 4 after grinding for first time side by side, and the second fluid reservoir 6 is used The storage of solution after being ground in second.
The tube centrifuge 8 carries out solid-liquid separation treatment to Dendrobidium huoshanness concentrate, and feed inlet, waste gate exist It is centrifuged the lower end of component, discharge port is in the upper end of centrifugation component.
The low temperature continuous vacuum film drier 10 be will be concentrated in vacuo, Transmission system, spraying system and coating system What is combined is dried device to Dendrobidium huoshanness concentrate.
In extraction equipment use process provided by the utility model, sample enters another process after the completion of a process When especially by such as under type realize: cleaning --- slice be mobile liftable motor transmission;Slice --- grinding is by equipment Difference in height pipeline;Grinding --- storage tank is also, pipeline transmission poor by device height;Filtrate --- it is defeated to be concentrated by vacuum pipe It send;First concentrate --- scraper plate, vacuum pipe connection;Concentrate --- cryogenic vacuum is continuous drying, peristaltic pump transmission.This pipe Road transmission reduces pollution section, promotes working efficiency.
Utilize the extracting process of the ultra micro extraction equipment, comprising the following steps:
(1) it cleans: first select in removal of impurities investment service sink 1 by the fresh item of Dendrobidium huoshanness and clean 3-5 times;
(2) it is sliced: after cleaning, waste water is discharged, hoist hook (not shown) is caught on into groove profile sieve hanging ring 121, button is risen in starting, moves to above machine for traditional Chinese medicinal material,table cutting 2 hopper, opens 12 bottom of groove profile sieve, and Dendrobidium huoshanness poured into It carries out cutting into 1-5cm segment in 2 hopper of medicine slicer;
(3) it grinds: the Dendrobidium huoshanness of cutting being transferred to colloid mill 4,10-20 times of purified water is added, opens colloid Grinder 4, starts the cycle over, and accordingly adjusts circulation canal gap depending on Dendrobidium huoshanness fluid state, gradually by Dendrobidium huoshanness shape At to broken wall state, Dendrobidium huoshanness suspension is obtained;
(4) it is sieved: the Dendrobidium huoshanness suspension that step (3) obtains first being removed into corresponding impurity with 150-250 mesh screen, is received Collect filtrate to storage tank;
(5) be concentrated, separate: the filtrate that step (4) are collected first once is concentrated through single-effect concentrator 7, then is centrifuged with tubular type Machine 8 is separated by solid-liquid separation, and filtrate is collected, and is continued to use spherical scraper concentrator 9 and is carried out secondary concentration;
(6) dry: finally concentrate obtained by step (5) is dried using low temperature continuous vacuum film drier 10, It discharges to obtain the final product.
Further, the fresh item of Dendrobidium huoshanness select putting into service sink 1 after removal of impurities in the step (1) and be cleaned, clearly After washing, open 1 bottom discharge valve 11 of service sink, waste water from bottom be discharged, close drain valve 11, re-inject purified water into Row cleaning, recycles 3-5 times.
Further, spherical scraper concentrator 9 is continued to use in the step (5) and carries out secondary concentration, and temperature of charge is set 55-60 DEG C, start vacuum pump, until concentrate relative density is 1.1-1.2.
Further, drying means in the step (6) specifically: the position of adjustable spraying rifle is allowed to keep with transmission belt The gap of 2-4mm starts spray gun compressed air and Material peristaltic pump, Dendrobidium huoshanness concentrate is squeezed into drier with peristaltic pump Spray gun opens painting work, is spread evenly across concentrate in transmission belt, forms film layer, and the speed that transmission belt is arranged exists 0.5-2m/10min, it is 5% hereinafter, discharge port is arranged that Dendrobidium huoshanness concentrate, which is dried in the way for being transmitted to discharge port to moisture, Grinding device directly crushed 70-90 mesh, obtain Dendrobii extract.
The extraction yield of the present apparatus in process of production reaches 60-70%, and Dendrobidium huoshanness polysaccharide extract rate (%) can reach 55%-70%.
A kind of application of ultra micro extraction equipment, specially Dendrobidium huoshanness particle, Dendrobidium huoshanness medicinal extract, Dendrobidium huoshanness wine with And the application in Dendrobidium huoshanness skin-protection product preparation process.
Embodiment two
The present embodiment and embodiment one the difference is that, be equipped with filter membrane (in figure not in the lower section of the second fluid reservoir 6 Show), filter membrane can effective impurity screening.It can choose economic benefits and social benefits or Three-effect concentration device in the selection of single-effect concentrator 7, from And improve thickening efficiency.

Claims (7)

1. a kind of ultra micro extraction equipment, which is characterized in that including service sink (1), machine for traditional Chinese medicinal material,table cutting (2), water purification system (3), Colloid mill (4), the first fluid reservoir (5), the second fluid reservoir (6), single-effect concentrator (7), tube centrifuge (8), spherical shape are scraped Plate inspissator (9), low temperature continuous vacuum film drier (10) are sequentially connected together by pipeline, transmission device;
Service sink (1) discharge end is connected with machine for traditional Chinese medicinal material,table cutting (2) feeding end, the both ends difference of the water purification system (3) It is communicated with service sink (1), colloid mill (4) by pipeline;Machine for traditional Chinese medicinal material,table cutting (2) discharge end and colloid mill (4) Upper end feed inlet is communicated by pipeline, and machine for traditional Chinese medicinal material,table cutting (2) discharge end height is higher than colloid mill (4) upper end;The glue Body grinder (4) upper end feed inlet and the first fluid reservoir (5) lower end are communicated by pipeline, and colloid mill (4) upper end level Higher than the first fluid reservoir (5) lower end, it is lower than the first fluid reservoir (5) upper end;First fluid reservoir (5) upper end and colloid mill (4) Upper end feed inlet is communicated by pipeline;Colloid mill (4) lower end discharge port and the second fluid reservoir (6) upper end pass through pipeline phase Logical, the second fluid reservoir (6) lower end and single-effect concentrator (7) upper end feed inlet are communicated by pipeline, and single-effect concentrator is brought out under (7) Material mouth and tube centrifuge (8) lower end feed inlet are communicated by pipeline;Tube centrifuge (8) upper end discharge port and spherical scraper plate are dense Contracting device (9) upper end feed inlet is communicated by pipeline, and spherical scraper concentrator (9) lower end discharge port and low temperature continuous vacuum film are dry Dry machine (10) feed inlet is communicated by pipeline.
2. a kind of ultra micro extraction equipment according to claim 1, which is characterized in that the service sink (1) is in cuboid knot Structure, bottom are equipped with a drain valve (11), have the groove profile sieve of hanging ring (121) in service sink (1) cavity equipped with a both ends (12)。
3. a kind of ultra micro extraction equipment according to claim 2, which is characterized in that the bottom of the sieve (12) is that can live Dynamic formula design, packaged type escalator catch on hanging ring (121).
4. a kind of ultra micro extraction equipment according to claim 1, which is characterized in that the machine for traditional Chinese medicinal material,table cutting (2) is passing It send and is provided with perpendicular type groove (211) on band (21), vibrating motor (212) are provided below in the conveyer belt (21).
5. a kind of ultra micro extraction equipment according to claim 4, which is characterized in that the perpendicular type groove (211) and vibration Motor (212) is point-blank.
6. a kind of ultra micro extraction equipment according to claim 1, which is characterized in that the tube centrifuge (8) is to suddenly Mountain dendrobium nobile concentrate carries out solid-liquid separation treatment, and feed inlet, waste gate are in the lower end of centrifugation component, and discharge port is in centrifugation group The upper end of part.
7. a kind of ultra micro extraction equipment according to claim 1, which is characterized in that the low temperature continuous vacuum film drying Machine (10) be will be concentrated in vacuo, Transmission system, spraying system are combined with coating system does to Dendrobidium huoshanness concentrate Dry processing unit.
CN201821295444.2U 2018-08-13 2018-08-13 A kind of ultra micro extraction equipment Active CN209108139U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108888716A (en) * 2018-08-13 2018-11-27 九仙尊霍山石斛股份有限公司 A kind of ultra micro extraction equipment and methods and applications

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108888716A (en) * 2018-08-13 2018-11-27 九仙尊霍山石斛股份有限公司 A kind of ultra micro extraction equipment and methods and applications

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