CN208959367U - A kind of andrographolide refining system - Google Patents

A kind of andrographolide refining system Download PDF

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Publication number
CN208959367U
CN208959367U CN201821608656.1U CN201821608656U CN208959367U CN 208959367 U CN208959367 U CN 208959367U CN 201821608656 U CN201821608656 U CN 201821608656U CN 208959367 U CN208959367 U CN 208959367U
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level
collecting tank
andrographolide
liquid collecting
extractor
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李昌华
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SICHUAN ZIREN PHARMACEUTICAL Co Ltd
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SICHUAN ZIREN PHARMACEUTICAL Co Ltd
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Abstract

The utility model relates to a kind of andrographolide refining systems, including extractor, level-one resin absorbing column, level-one liquid collecting tank, second resin adsorption column, second level liquid collecting tank and the refined solution collecting tank successively to connect from top to bottom.The utility model helps to improve the preparation efficiency of andrographolide, promotes the product quality of the andrographolide of acquisition, provides the andrographolide raw medicine of higher quality for clinical treatment.

Description

A kind of andrographolide refining system
Technical field
The utility model relates to andrographolide preparations, especially related with a kind of andrographolide refining system.
Background technique
Andrographolide has antiphlogistic antibacterial, antiviral and other effects, is widely used in clinical treatment, and demand is very big. The prior art is when carrying out andrographolide preparation, inefficiency and purity is not high, reduces the quality for obtaining andrographolide And production efficiency.
Utility model content
The utility model provides a kind of andrographolide refining system, improves the preparation efficiency of andrographolide, and promotion obtains The product quality of the andrographolide obtained, provides the andrographolide raw medicine of higher quality for clinical treatment.
In order to realize the purpose of this utility model, proposed adoption following technical scheme:
A kind of andrographolide refining system, including extractor (1), the level-one resin absorbing column successively to connect from top to bottom (2), level-one liquid collecting tank (3), second resin adsorption column (4), second level liquid collecting tank (5) and refined solution collecting tank (6);
Angle-inserting type mesh baffle (11) are set in the middle part of the extractor (1), extractor (1) bottom sets up filter layer plate (12), ethyl alcohol holding vessel (13) are connected at the top of extractor (1), metering-type is set between ethyl alcohol holding vessel (13) and extractor (1) Control valve (131), extractor (1) left side wall are defeated close to angle-inserting type mesh baffle (11) interface one end setting Herba Andrographitis crushed material Enter valve (14), extractor (1) bottom is located at angle-inserting type mesh baffle (11) and filters the position setting deslagging between laminate (12) Valve (15);
Extracting solution discharge valve is set on the connecting line between the extractor (1) and level-one resin absorbing column (2) (102);
Level-one vacuum pumping pump (31) are arranged in level-one liquid collecting tank (3) left-hand end;
Second level vacuum pumping pump (51) are arranged in second level liquid collecting tank (5) left-hand end.
Further, the level-one resin absorbing column (2) is detachably connected with level-one liquid collecting tank (3).
Further, the level-one liquid collecting tank (3) is detachably connected with second resin adsorption column (4).
Further, the second resin adsorption column (4) is detachably connected with second level liquid collecting tank (5).
Further, the second level liquid collecting tank (5) is detachably connected with refined solution collecting tank (6).
The beneficial effects of the utility model are:
1, the utility model relates to andrographolide refining system, including successively connect from top to bottom extractor (1), Level-one resin absorbing column (2), level-one liquid collecting tank (3), second resin adsorption column (4), second level liquid collecting tank (5) and refined solution collecting tank (6);Above-mentioned design, using extractor (1), level-one resin absorbing column (2), level-one liquid collecting tank (3), second resin adsorption column (4), The mutual cooperation of second level liquid collecting tank (5) and refined solution collecting tank (6), realizes the extraction and purification of andrographolide, to obtain The andrographolide product for obtaining high-quality, meets clinical use demand.
2, the utility model relates to andrographolide refining system, angle-inserting type mesh baffle is set in the middle part of extractor (1) (11), extractor (1) bottom sets up filter layer plate (12), connects ethyl alcohol holding vessel (13) at the top of extractor (1), ethyl alcohol holding vessel (13) metering-type control valve (131) are set between extractor (1), extractor (1) left side wall is close to angle-inserting type mesh baffle (11) interface one end setting Herba Andrographitis crushed material transfer valve (14), extractor (1) bottom is located at angle-inserting type mesh baffle (11) Residual cake valve (15) are arranged in position between filtering laminate (12);Above-mentioned design, using angle-inserting type mesh baffle (11) and filtering The cooperation of laminate (12) makes Herba Andrographitis powder convenient for carrying out carry out baffle to the Herba Andrographitis crushed material for being used to prepare andrographolide It minces and is come into full contact with the ethyl alcohol exported via ethyl alcohol holding vessel (13), so that the output capacity of andrographolide is improved, it is same with this When, the filtering laminate (12) of design is also convenient for being filtered andrographolide extract liquor, effectively removes bulky grain filter residue, guarantees The smoothness and continuity of andrographolide subsequent purification technique.
3, the utility model relates to andrographolide refining system, level-one resin absorbing column (2) bottom be arranged level-one Second resin adsorption column (4) are arranged in liquid collecting tank (3), level-one liquid collecting tank (3) bottom, second resin adsorption column (4) bottom setting two Grade liquid collecting tank (5);Above-mentioned design, convenient for improving the purity of the andrographolide prepared.
Figure of description
Fig. 1 shows the structural schematic diagram of the utility model andrographolide refining system.
Specific embodiment
As shown in Figure 1, a kind of andrographolide refining system, including successively connect from top to bottom extractor (1), level-one Resin absorbing column (2), level-one liquid collecting tank (3), second resin adsorption column (4), second level liquid collecting tank (5) and refined solution collecting tank (6);
Angle-inserting type mesh baffle (11) are set in the middle part of the extractor (1), extractor (1) bottom sets up filter layer plate (12), ethyl alcohol holding vessel (13) are connected at the top of extractor (1), metering-type is set between ethyl alcohol holding vessel (13) and extractor (1) Control valve (131), extractor (1) left side wall are defeated close to angle-inserting type mesh baffle (11) interface one end setting Herba Andrographitis crushed material Enter valve (14), extractor (1) bottom is located at angle-inserting type mesh baffle (11) and filters the position setting deslagging between laminate (12) Valve (15);
Extracting solution discharge valve is set on the connecting line between the extractor (1) and level-one resin absorbing column (2) (102);
Level-one vacuum pumping pump (31) are arranged in level-one liquid collecting tank (3) left-hand end;
Second level vacuum pumping pump (51) are arranged in second level liquid collecting tank (5) left-hand end.
As an improvement, the level-one resin absorbing column (2) is detachably connected with level-one liquid collecting tank (3).
As an improvement, the level-one liquid collecting tank (3) is detachably connected with second resin adsorption column (4).
As an improvement, the second resin adsorption column (4) is detachably connected with second level liquid collecting tank (5).
As an improvement, the second level liquid collecting tank (5) is detachably connected with refined solution collecting tank (6).
Compared with prior art, the utility model relates to andrographolide refining system, including successively phase from top to bottom Extractor (1), level-one resin absorbing column (2), level-one liquid collecting tank (3), second resin adsorption column (4), the second level liquid collecting tank (5) connect With refined solution collecting tank (6);Above-mentioned design, using extractor (1), level-one resin absorbing column (2), level-one liquid collecting tank (3), second level The mutual cooperation of resin absorbing column (4), second level liquid collecting tank (5) and refined solution collecting tank (6), realizes the extraction of andrographolide Clinical use demand is met to obtain the andrographolide product of high-quality with purifying.
The utility model relates to andrographolide refining system, angle-inserting type mesh baffle is set in the middle part of extractor (1) (11), extractor (1) bottom sets up filter layer plate (12), connects ethyl alcohol holding vessel (13) at the top of extractor (1), ethyl alcohol holding vessel (13) metering-type control valve (131) are set between extractor (1), extractor (1) left side wall is close to angle-inserting type mesh baffle (11) interface one end setting Herba Andrographitis crushed material transfer valve (14), extractor (1) bottom is located at angle-inserting type mesh baffle (11) Residual cake valve (15) are arranged in position between filtering laminate (12);Above-mentioned design, using angle-inserting type mesh baffle (11) and filtering The cooperation of laminate (12) makes Herba Andrographitis powder convenient for carrying out carry out baffle to the Herba Andrographitis crushed material for being used to prepare andrographolide It minces and is come into full contact with the ethyl alcohol exported via ethyl alcohol holding vessel (13), so that the output capacity of andrographolide is improved, it is same with this When, the filtering laminate (12) of design is also convenient for being filtered andrographolide extract liquor, effectively removes bulky grain filter residue, guarantees The smoothness and continuity of andrographolide subsequent purification technique.
The utility model relates to andrographolide refining system, level-one resin absorbing column (2) bottom be arranged level-one collection Second resin adsorption column (4) are arranged in flow container (3), level-one liquid collecting tank (3) bottom, and second level is arranged in second resin adsorption column (4) bottom Liquid collecting tank (5);Above-mentioned design, convenient for improving the purity of the andrographolide prepared.
When the utility model is used, Herba Andrographitis crushed material enters extractor via Herba Andrographitis crushed material transfer valve (14) (1), contacted with the ethyl alcohol exported via ethyl alcohol holding vessel (13) extractor (1) is internal, by by ethyl alcohol by andrographolide Extract is extracted, the andrographolide extracting solution of acquisition pass sequentially through level-one resin absorbing column (2), level-one liquid collecting tank (3), Second resin adsorption column (4) and second level liquid collecting tank (5) complete the purifying of andrographolide extracting solution, final acquisition high-purity Andrographolide is simultaneously stored in refined solution collecting tank (6) inside, and level-one resin absorbing column (2) and second resin adsorption column (4) are right When andrographolide is purified, in elution stage, various concentration can choose, the eluent of different component is eluted.

Claims (5)

1. a kind of andrographolide refining system, which is characterized in that including successively connect from top to bottom extractor (1), level-one Resin absorbing column (2), level-one liquid collecting tank (3), second resin adsorption column (4), second level liquid collecting tank (5) and refined solution collecting tank (6);
Angle-inserting type mesh baffle (11) are set in the middle part of the extractor (1), extractor (1) bottom sets up filter layer plate (12), extraction It takes and connects ethyl alcohol holding vessel (13) at the top of tank (1), metering-type control valve is set between ethyl alcohol holding vessel (13) and extractor (1) (131), Herba Andrographitis crushed material transfer valve is arranged close to angle-inserting type mesh baffle (11) interface one end in extractor (1) left side wall (14), extractor (1) bottom is located at angle-inserting type mesh baffle (11) and filters the position setting residual cake valve between laminate (12) (15);
Extracting solution discharge valve (102) are set on connecting line between the extractor (1) and level-one resin absorbing column (2);
Level-one vacuum pumping pump (31) are arranged in level-one liquid collecting tank (3) left-hand end;
Second level vacuum pumping pump (51) are arranged in second level liquid collecting tank (5) left-hand end.
2. andrographolide refining system according to claim 1, which is characterized in that the level-one resin absorbing column (2) It is detachably connected with level-one liquid collecting tank (3).
3. andrographolide refining system according to claim 1, which is characterized in that the level-one liquid collecting tank (3) and two Grade resins adsorption column (4) is detachably connected.
4. andrographolide refining system according to claim 1, which is characterized in that the second resin adsorption column (4) It is detachably connected with second level liquid collecting tank (5).
5. andrographolide refining system according to claim 1, which is characterized in that the second level liquid collecting tank (5) with it is pure Change liquid collecting tank (6) to be detachably connected.
CN201821608656.1U 2018-03-03 2018-09-30 A kind of andrographolide refining system Active CN208959367U (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201820295664 2018-03-03
CN2018202956649 2018-03-03

Publications (1)

Publication Number Publication Date
CN208959367U true CN208959367U (en) 2019-06-11

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU196119U1 (en) * 2019-11-08 2020-02-18 Артемий Валерьевич Чукичев Mobile device for emulsion extraction of plant materials
CN112979594A (en) * 2021-02-26 2021-06-18 南通科鑫超临界设备有限公司 Supercritical extraction process of andrographolide

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU196119U1 (en) * 2019-11-08 2020-02-18 Артемий Валерьевич Чукичев Mobile device for emulsion extraction of plant materials
CN112979594A (en) * 2021-02-26 2021-06-18 南通科鑫超临界设备有限公司 Supercritical extraction process of andrographolide
CN112979594B (en) * 2021-02-26 2021-12-14 南通科鑫超临界设备有限公司 Supercritical extraction process of andrographolide

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Address after: 638000 West Section 3, Shenzhen Road, Guanghan City, Deyang City, Sichuan Province

Patentee after: SICHUAN ZIREN PHARMACEUTICAL CO., LTD.

Address before: 638000 West Section of Shenzhen Road, Guanghan City, Deyang City, Sichuan Province

Patentee before: SICHUAN ZIREN PHARMACEUTICAL CO., LTD.

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