CN208449350U - A kind of distillation apparatus - Google Patents

A kind of distillation apparatus Download PDF

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Publication number
CN208449350U
CN208449350U CN201820374146.6U CN201820374146U CN208449350U CN 208449350 U CN208449350 U CN 208449350U CN 201820374146 U CN201820374146 U CN 201820374146U CN 208449350 U CN208449350 U CN 208449350U
Authority
CN
China
Prior art keywords
type
supporing shell
bable tops
condensing bulb
distillation apparatus
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820374146.6U
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Chinese (zh)
Inventor
白晓明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hebei Hebei Ji Group Instrument Co Ltd
Original Assignee
Hebei Hebei Ji Group Instrument Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hebei Hebei Ji Group Instrument Co Ltd filed Critical Hebei Hebei Ji Group Instrument Co Ltd
Priority to CN201820374146.6U priority Critical patent/CN208449350U/en
Application granted granted Critical
Publication of CN208449350U publication Critical patent/CN208449350U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model discloses a kind of distillation apparatus, belong to distillation equipment technical field, including L-type supporing shell, cucurbit, condensing bulb, Backflow bottle, L-type supporing shell includes the first supporting bable tops and the second supporting bable tops being parallel to each other, fixed bracket and stove mouth are provided on first supporting bable tops, fixed device is set on the second supporting bable tops, heating device and condenser system corresponding with condensing bulb are provided in L-type supporing shell, condensing bulb is equipped with the condensate inlet being connected to condenser system and condensate outlet and the retort gas entrance being connected to cucurbit, the distillating liquid outlet being connected to Backflow bottle, fixed device includes being fixedly installed on fixed ring hollow on the second supporting bable tops, the contact block that the other end of several springs and spring for being fixedly installed on fixed ring inner surface affixed one is in contact with Backflow bottle outer surface.The distillation of the utility model collection it is used be installed on one, it is easy to operate and have the advantages such as safety coefficient height, distillation efficiency height.

Description

A kind of distillation apparatus
Technical field
The utility model relates to distillation equipment technical field, especially a kind of distillation apparatus.
Background technique
What the principle of distillation apparatus was all made of at this stage is thermodynamic (al) separating technology, and what he utilized is mixing liquid or liquid- The boiling point of each component is different in solid system, evaporates low boiling component, then condense to separate the unit process of entire component, It is the joint of evaporation and condensation two kinds of units operation.Therefore it evaporates and condensation is the Main Stage of distillation apparatus.
Involved distillation apparatus is generally used for laboratory or analysis center, dress used in such distillation apparatus at present Set comparatively laborious, the space occupied is bigger, and one side distillation apparatus the use of consumptive material is frangible glass apparatus, for example steam Bottle, condensing bulb, Backflow bottle are evaporated, but existing distillation apparatus facility does not also carry out special processing to these glass apparatus, causes Keep distillation apparatus safety coefficient relatively low, another convenience, distillation apparatus is condensed only with single cooling system, i.e., in condensing bulb Water inlet for circulating chilled water, water outlet are set, cause that condensation effect is poor, distillation efficiency is low.
Utility model content
The utility model technical issues that need to address are to provide a kind of distillation apparatus, are installed on one used in collection distillation, It is easy to operate and have the advantages such as safety coefficient height, distillation efficiency height.
In order to solve the above technical problems, the technical scheme adopted by the utility model is:
A kind of distillation apparatus, including L-type supporing shell, cucurbit, condensing bulb, Backflow bottle, the L-type supporing shell includes phase Mutually parallel the first supporting bable tops and the second supporting bable tops are provided with for fixing consolidating for condensing bulb on first supporting bable tops The fixation device for fixing Backflow bottle is arranged on second supporting bable tops for fixed rack and stove mouth for placing cucurbit, The heating device for heating cucurbit and condenser system corresponding with condensing bulb, institute are provided in the L-type supporing shell It states condensing bulb and is equipped with the condensate inlet being connected to condenser system and condensate outlet and the distillation gas being connected to cucurbit Body entrance, the distillating liquid being connected to Backflow bottle outlet, the fixation device include being fixedly installed on the second supporting bable tops The other end affixed one of hollow fixed ring, several springs and spring for being fixedly installed on fixed ring inner surface and reflux The contact block that bottle outer surface is in contact.
Technical solutions of the utility model further improvement lies in that: heating device includes that be set to L-type supporting shell intracorporal Ceramic heater, the main control circuit being electrically connected with ceramic heater, are additionally provided in the L-type supporing shell and main control electricity The control switch of road connection.
Technical solutions of the utility model further improvement lies in that: several stove mouths and phase are set in L-type supporing shell The heating device answered.
Technical solutions of the utility model further improvement lies in that: the number of spring is at least 3.
Technical solutions of the utility model further improvement lies in that: a boss, the boss position are set in L-type supporing shell The groove for accommodating condensing bulb efferent duct is opened up between the first supporting surface and the second supporting surface, on boss.
Technical solutions of the utility model further improvement lies in that: copper heat dissipating ring is arranged on condensing bulb.
By adopting the above-described technical solution, the technological progress that the utility model obtains is:
Cucurbit, condensing bulb, Backflow bottle, heating device, condenser system and control switch are respectively provided with by the utility model To L-type supporing shell, solves the defect that occupied space is big, cumbersome.
Further, it is also provided with the fixation device for fixing Backflow bottle in L-type supporing shell, improves traditional return Stream bottle only places supporing shell surface, is easy to happen collision, causes the safety coefficient of distillation apparatus low.In addition, fixed device uses Backflow bottle is fixed in the fixed ring of adjustability, and the use scope of the present apparatus can be made bigger, adapts to the Backflow bottle of different model.
Further, a boss is set between the first supporting surface and the second supporting surface of L-type supporing shell, is opened up on boss For accommodating the groove of condensing bulb efferent duct, fixed condensing bulb efferent duct can be played the role of, improve safety coefficient.
Further, it is arranged copper heat dissipating ring on condensing bulb, on the basis of existing condenser system, improves condensation effect, Accelerate condensation, and then improves distillation efficiency.
Detailed description of the invention
Fig. 1 is the utility model structure principle chart;
Fig. 2 is the schematic diagram of the fixation device of the utility model;
Fig. 3 is the structural schematic diagram of supporing shell;
Wherein, 1, L-type supporing shell, 2, cucurbit, 3, condensing bulb, 4, Backflow bottle, the 5, first supporting bable tops, 6, second Support table top, 7, fixed bracket, 8, fixed device, 8-1, fixed ring, 8-2 spring, 8-3, contact block, 9, condensate inlet, 10, cold Condensate outlet, 11, retort gas entrance, 12, distillating liquid outlet, 13, control switch, 14, groove, 15, temperature display.
Specific embodiment
The utility model is described in further details below with reference to embodiment:
As shown in Figure 1, Figure 3, a kind of distillation apparatus, including L-type supporing shell 1, cucurbit 2, condensing bulb 3, Backflow bottle 4, with And heating device and condensing unit in L-type supporing shell 1, wherein the utility model uses heating device for ceramic heat Device replaces common electrothermal furnace or electric jacket using ceramic heater, may be implemented that heating is fast, waterproof safety performance is good, section The advantages such as energy consumption reduction, condensing unit use dual-cooled system, are as arranged copper dissipate in the built-in circulatory system and condensing bulb 3 Hot ring, wherein the built-in circulatory system includes being built in cooling water tank and the compression connecting with cooling water tank in L-type supporing shell Machine takes dual-cooled system in this way on the basis of existing condenser system, improves condensation effect, accelerates condensation, and then improve Distillation efficiency.
L-type supporing shell 1 is additionally provided with the main control circuit being electrically connected with ceramic heater, also sets in L-type supporing shell It is equipped with the control switch 13 connecting with main control circuit, for controlling the power on/off of ceramic heater, is also set in L-type supporing shell Be equipped with temperature display 15, by control switch 13 adjust ceramic heater heating temperature, and by temperature display 15 into Row display, realizes single-point single control, is beneficial to energy conservation consumption reduction.
L-type supporing shell 1 includes the first supporting bable tops 5 and the second supporting bable tops 6 being parallel to each other, as shown in figure 3, first The fixation bracket 7 for fixing condensing bulb 3 and the stove mouth for placing cucurbit 2, the second supporting table are provided on supporting bable tops 5 Fixation device 8 for fixing Backflow bottle is set on face 6, and wherein condensing bulb 3 includes bottle body, is located at the condensation of bottle body inside spin shape Pipe is additionally provided with the condensate inlet 9 being connected to condenser system and condensate outlet 10 on condensing bulb 3 and is connected to cucurbit Retort gas entrance 11, the distillating liquid being connected to Backflow bottle outlet 12, wherein cucurbit, condensing bulb, the company between Backflow bottle It connects and is all made of glass tube and is connected to, be more in line with the working principle of distillation test.One boss is set in L-type supporing shell 1, it is convex Platform opens up the groove 14 for accommodating condensing bulb efferent duct between the first supporting surface and the second supporting surface, on boss, can be with Play the role of fixed condensing bulb efferent duct, improves safety coefficient.
Further in view of test process is using being full glass apparatus, avoids colliding during test, cause back Stream bottle moves, and damages Backflow bottle, as shown in Fig. 2, the fixed dress for fixing Backflow bottle is arranged on the second supporting bable tops 8 are set, wherein fixed device includes being fixedly installed on fixed ring 8-1 hollow on the second supporting bable tops, being fixedly installed on fixed ring The contact block 8-3 that the other end affixed one of several springs 8-2 and spring on inner surface are in contact with Backflow bottle outer surface, Firm effect not only can be played to Backflow bottle, the maximum for being greater than Backflow bottle for also designing the internal diameter of fixed ring is directly Diameter, and various types of Backflow bottles are adapted to by the design of spring, increase the use scope of distillation apparatus.
The number of spring is at least 3, and spring is uniformly set on the same periphery of fixed ring, further, can Contact block to be designed as to the rubber pad of softwood matter, realizes that the contact with Backflow bottle contacts to be soft, a kind of guarantor is played to Backflow bottle The effect of shield.
Further, for convenience simultaneously carry out multiple distillation tests, be arranged in L-type supporing shell several stove mouths and Corresponding heating device, cucurbit, condensing bulb, the number of Backflow bottle are corresponding with stove mouth, and wherein several condensing bulbs are mutually gone here and there The distillating liquid outlet of connection, the retort gas entrance, the last one condensing bulb of first condensing bulb is connected to condenser system.

Claims (6)

1. a kind of distillation apparatus, it is characterised in that: including L-type supporing shell (1), cucurbit (2), condensing bulb (3), Backflow bottle (4), The L-type supporing shell (1) includes the first supporting bable tops (5) and the second supporting bable tops (6) being parallel to each other, first support It is provided with the fixation bracket (7) for fixing condensing bulb (3) and the stove mouth for placing cucurbit on table top (5), described second Fixation device (8) for fixing Backflow bottle is set on supporting bable tops (6), is additionally provided in the L-type supporing shell for adding The heating device of thermal distillation bottle and condenser system corresponding with condensing bulb, the condensing bulb are equipped with and are connected to condenser system Condensate inlet (9) and condensate outlet (10) and the retort gas entrance (11) being connected to cucurbit are connected to Backflow bottle Distillating liquid export (12), the fixation device (8) includes being fixedly installed on fixed ring hollow on the second supporting bable tops The other end affixed one and Backflow bottle of (8-1), several springs (8-2) and spring being fixedly installed on fixed ring inner surface The contact block (8-3) that outer surface is in contact.
2. a kind of distillation apparatus according to claim 1, it is characterised in that: the heating device includes being set to L-type support Shell intracorporal ceramic heater, the main control circuit that is electrically connected with ceramic heater, is also set up on the L-type supporing shell (1) There is the control switch (13) connecting with main control circuit.
3. a kind of distillation apparatus according to claim 1, it is characterised in that: several stoves are arranged in the L-type supporing shell Mouth and corresponding heating device.
4. a kind of distillation apparatus according to claim 1, it is characterised in that: the number of the spring (8-2) is at least 3.
5. a kind of distillation apparatus according to claim 1, it is characterised in that: a boss, institute are arranged in the L-type supporing shell It states boss and opens up groove for accommodating condensing bulb efferent duct between the first supporting surface and the second supporting surface, on boss (14).
6. described in any item a kind of distillation apparatus according to claim 1~5, it is characterised in that: be arranged copper on the condensing bulb (3) Matter heat dissipating ring.
CN201820374146.6U 2018-03-20 2018-03-20 A kind of distillation apparatus Expired - Fee Related CN208449350U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820374146.6U CN208449350U (en) 2018-03-20 2018-03-20 A kind of distillation apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820374146.6U CN208449350U (en) 2018-03-20 2018-03-20 A kind of distillation apparatus

Publications (1)

Publication Number Publication Date
CN208449350U true CN208449350U (en) 2019-02-01

Family

ID=65156165

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820374146.6U Expired - Fee Related CN208449350U (en) 2018-03-20 2018-03-20 A kind of distillation apparatus

Country Status (1)

Country Link
CN (1) CN208449350U (en)

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190201

Termination date: 20210320