CN208482027U - A kind of novel integrated distillation apparatus - Google Patents
A kind of novel integrated distillation apparatus Download PDFInfo
- Publication number
- CN208482027U CN208482027U CN201820114150.9U CN201820114150U CN208482027U CN 208482027 U CN208482027 U CN 208482027U CN 201820114150 U CN201820114150 U CN 201820114150U CN 208482027 U CN208482027 U CN 208482027U
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- CN
- China
- Prior art keywords
- cucurbit
- shell
- safe ball
- condensing bulb
- distillate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of novel integrated distillation apparatus, distillation apparatus further includes safe ball, chilled water unit built in enclosure interior, hull outside is equipped with observation window of liquid level, multiple computer heating control switches corresponding with electric heating cover are installed on shell, heating lamp, shell upper end is equipped with fixed device, cucurbit is placed on electric heating cover, cucurbit upper end is connected with safe ball, safe ball upper end is connected with condensing bulb, condensing bulb is connected with distillate effuser, suck-back device is installed close at condensing bulb on distillate effuser, distillate effuser is connected with returnable bottle.The advantage is that: the utility model in multiple cucurbits simultaneously in use, the cooling water in condensing bulb is back to inside chilled water unit after repeatedly utilizing, saved water resource, and reduce the quantity of distillation apparatus；It replaces round bottom cucurbit to facilitate after use with cylindrical cucurbit to clean cucurbit, reduce bringing into for the subsequent other product impurity of distillation.
Description
Technical field
The utility model belongs to chemical test Instrument technology field, and in particular to a kind of novel integrated distillation apparatus.
Background technique
Distillation is laboratory separation, purification liquefied mixture is commonly used and important preprocess method,.Traditional arrangement is logical
Asbestos gauge partner's electric furnace heating wire directly heats, when heated since uneven heating is easy to cause explosion, and traditional distilling apparatus
Multiple samples cannot be distilled simultaneously, can only single furnace monocyte sample distillation so that distilling apparatus occupies much room in laboratory.
Existing patent No. CN101530821A discloses an intelligent integrated distillation apparatus, including cucurbit, condensing bulb, reflux
Bottle and electric heating cover, condensing bulb include bottle body, are located at the intracorporal condenser pipe of bottle, further include shell, electric heating is set on shell
Interior and correspond and be equipped with stove mouth in case top, cucurbit is placed in stove mouth；The bottle body of condensing bulb is clamped with clip, folder
Son is affixed by bracket and shell, and condensing bulb bottle body is equipped with water inlet, water outlet, is provided with cold water storage cistern, condenser pipe in shell
Upper/lower terminal be respectively air inlet, liquid storage mouth, air inlet and cucurbit are tightly connected, and liquid outlet and Backflow bottle are tightly connected,
Main control circuit is installed in shell, heating mantle is connect with main control circuit point, and shell is equipped with and connect with main control circuit
Control knob.Distillation apparatus Ji Ji is distilled with one is installed on, and occupied space is few, easy to operate, it can be achieved that intelligentized control method.But
The device is connected with protective gas in use, is appropriate to and needs to distill using the product of nitrogen protection, and using
Conventional round bottom cucurbit, after use, round bottom cucurbit is inconvenient to clean, and has brought into for the other products of subsequent distillation miscellaneous
Matter.
Utility model content
The purpose of this utility model is that in view of the deficiencies of the prior art, now providing one kind and being readily cleaned, be equally applicable to
Unprotect inhales the novel integrated distillation apparatus of the distillation of gas chemicals.
In order to solve the above technical problems, the technical solution adopted by the utility model is: a kind of novel integrated distillation apparatus, packet
Include shell, setting be provided with electric heating cover in the intracorporal multiple stove mouths of shell, cucurbit, returnable bottle and condensing bulb, the stove mouth,
Main control circuit is installed, the electric heating cover is connected with main control circuit, it is characterised in that: the distillation apparatus in the shell
It further include safe ball, chilled water unit built in the enclosure interior, the chilled water unit is connected with main control circuit, the shell
External side is equipped with observation window of liquid level, and multiple computer heating control switches corresponding with electric heating cover, heating are equipped on the shell
Indicator light is also equipped with display screen on the shell, and the shell upper end is equipped with fixed device, and the cucurbit is placed on electricity
In heating mantle, the cucurbit upper end is connected with safe ball, and the safe ball upper end is connected with condensing bulb, the condensing bulb connection
There is distillate effuser, suck-back device, the distillate outflow are installed on the distillate effuser close at condensing bulb
Pipe is connected with returnable bottle.
Further, the fixed device includes being fixedly mounted on the vertical support rod of shell upper end two sides and installing and erect
Two horizontal cross bars between allotment bar are fixed with vertical bar between the horizontal cross bar, are movably installed in the vertical bar
Fixing clamp A and fixed frame B, the safe ball and condensing bulb pass through fixing clamp A respectively and fixing clamp B is fixed.
Further, the cucurbit is the cylindrical bottle body that neck closes up, and the cucurbit bottom is circle, the steaming
It evaporates neck part and sealing-plug is installed.
Further, the safe ball includes elliposoidal body, the vertical outlet tube A for being fixed on body bottom and fixation
Outlet tube B, the outlet tube B curved one at the top of body is vertical pipe, and other end is bent towards inside safe ball, described to go out vertically
Liquid pipe A is inserted into inside sealing-plug.
Further, the condensing bulb includes the spiral cold-finger inside bottle body and bottle body, and the bottle body upper end offers
Steam inlet, lower end offer distillate outlet, and side offers cooling water inlet and cooling water outlet, the cooling water inlet
It is connected with chilled water unit with cooling water outlet.
The beneficial effects of the utility model are as follows:
(1) the utility model is in multiple cucurbits simultaneously in use, can be by multiple condensing bulb cooling water outlets and cooling water
Import connects, and the cooling water in condensing bulb is back to inside chilled water unit after repeatedly utilizing, and has saved water resource, and subtract
The quantity of distillation apparatus is lacked；
(2) the utility model is between cucurbit and condensing bulb by installing safe ball, and safe ball upper end outlet tube to
Bending inside safe ball, it is therefore prevented that be back between cucurbit in the distillate in distillation process in condensing bulb；
(3) the utility model replaces round bottom cucurbit to facilitate after use to cucurbit progress clearly with cylindrical cucurbit
It washes, reduces bringing into for the subsequent other product impurity of distillation；And cylindrical cucurbit bottleneck uses closing, distillation foam is not
It easily goes out, bottle is not pasted after heating；
(4) the utility model inhales device by installing to fall on distillate effuser, avoids the steaming inside returnable bottle
Distillate is back to inside condensing bulb.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model entirety；
Fig. 2 is the utility model principle structural schematic diagram；
Fig. 3 is the structural schematic diagram of the utility model cucurbit；
Fig. 4 is the structural schematic diagram of the utility model safe ball.
Specific embodiment
The embodiments of the present invention is illustrated by particular specific embodiment below, those skilled in the art can be by this
Content disclosed by specification understands other advantages and effect of the utility model easily.
As depicted in figs. 1 and 2, a kind of novel integrated distillation apparatus, including shell 1, the multiple stove mouths being arranged in shell 1
11, cucurbit 3, returnable bottle 2 and condensing bulb 5 are provided with electric heating cover 12 in stove mouth 11, are equipped with main control circuit in shell 1
13, electric heating cover 12 is connected with main control circuit 13, and distillation apparatus further includes safe ball 4, chilled water unit built in 1 inside of shell
14, chilled water unit 14 is connected with main control circuit 13, and observation window of liquid level 10 is equipped on the outside of shell 1, is equipped on shell 1 multiple
Computer heating control switch 15 corresponding with electric heating cover 12, heating lamp 16 are also equipped with display screen 9, shell 1 on shell 1
Upper end is equipped with fixed device 7, and fixed device 7 includes vertical support rod 71 and the installation for being fixedly mounted on 1 upper end two sides of shell
Two horizontal cross bars 72 between vertical pole are fixed with vertical bar 73 between horizontal cross bar 72, activity peace in vertical bar 73
Equipped with fixing clamp A74 and fixed frame B75, safe ball 4 and condensing bulb 5 are fixed by fixing clamp A74 and fixing clamp B75 respectively.
Cucurbit 3 is placed on electric heating cover 12, and 12 upper end of cucurbit is connected with safe ball 4, and 4 upper end of safe ball is connected with
Condensing bulb 5, condensing bulb 5 are connected with distillate effuser 8, are equipped with anti-suck dress on distillate effuser 8 close at condensing bulb 5
17 are set, distillate effuser 8 is connected with returnable bottle 2.
As shown in figure 3, cucurbit 3 is the cylindrical bottle body that neck closes up, 3 bottom of cucurbit is circle 32,3 neck of cucurbit
Portion is equipped with sealing-plug 6, replaces round bottom cucurbit with cylindrical bottle body, facilitates clean to cucurbit after use, reduces
It is subsequent to distill bringing into for other product impurity.
As shown in figure 4, safe ball 4 include elliposoidal body 41, be fixed on 41 bottom of body vertical outlet tube A42 and
It is fixed on the outlet tube B43 at 41 top of body, outlet tube B43 mono- is vertical pipe, and other end is bent towards inside safe ball, is gone out vertically
Liquid pipe A41 is inserted into inside sealing-plug 6, and outlet tube B43 mono- in 3 upper end of cucurbit connection 4 upper end of safe ball is internally curved
Song can prevent inside the liquid reflux to cucurbit 3 in condensing bulb 5.
Condensing bulb 5 includes the spiral cold-finger 52 inside bottle body 51 and bottle body 51, and 51 upper end of bottle body offers steam inlet
56, lower end offers distillate outlet 55, and side offers cooling water inlet 54 and cooling water outlet 55,54 He of cooling water inlet
Cooling water outlet 55 is connected with chilled water unit 13, is reduced distillation equipment integration by built-in recirculated cooling water device
The usage amount of equipment when distillation.
Working principle: the utility model is when being distilled, cucurbit 3, Backflow bottle 2, safe ball 4, condensing bulb 4 and cooling
Water installations 13 can be used separately as a set of distillation equipment, can also multiple cucurbits 3 distilled simultaneously, opened by computer heating control
The heating temperature for closing the 15 each electric jackets 12 of control, heats cucurbit 3, when multiple cucurbits 3 are carried out while being distilled,
Chilled water unit 13 is connect with first condensing bulb cooling water inlet 54, then first condensing bulb cooling water outlet 55 with under
The cooling water inlet 54 of one condensing bulb connects, and so on, to the last a condensing bulb cooling water outlet 55 return be connected to it is cold
But water installations 13, cooling water are back to inside chilled water unit 13 after repeatedly utilizing, and have saved water resource, and reduce steaming
The quantity for evaporating instrument is detected the water inside chilled water unit at any time by observation window of liquid level 10, added in time when insufficient.
Above-described embodiment is the preferred embodiment of the utility model, is not the limit to technical solutions of the utility model
System, as long as being regarded as falling into without the technical solution that creative work can be realized on the basis of the above embodiments
In the rights protection scope of the utility model patent.
Claims (1)
1. a kind of novel integrated distillation apparatus, including shell, setting are in the intracorporal multiple stove mouths of shell, cucurbit, returnable bottle and cold
Bottle is coagulated, electric heating cover is provided in the stove mouth, main control circuit, the electric heating cover and main control is installed in the shell
Circuit is connected, it is characterised in that: the distillation apparatus further includes safe ball, chilled water unit built in the enclosure interior, described cold
But water installations are connected with main control circuit, and the hull outside is equipped with observation window of liquid level, be equipped on the shell it is multiple with it is electric
Heating mantle corresponding computer heating control switch, heating lamp are also equipped with display screen, the shell upper end peace on the shell
Equipped with fixed device, the cucurbit is placed on electric heating cover, and the cucurbit upper end is connected with safe ball, the safe ball
Upper end is connected with condensing bulb, and the condensing bulb is connected with distillate effuser, on the distillate effuser close at condensing bulb
Suck-back device is installed, the distillate effuser is connected with returnable bottle；The fixed device includes being fixedly mounted on shell
Two horizontal cross bars between the vertical support rod and installation and vertical pole of upper end two sides are fixed between the horizontal cross bar
Vertical bar is movably installed with fixing clamp A and fixed frame B in the vertical bar, and the safe ball and condensing bulb pass through fixation respectively
Folder A and fixing clamp B is fixed；The cucurbit is the cylindrical bottle body that neck closes up, and the cucurbit bottom is circle, the steaming
It evaporates neck part and sealing-plug is installed；The safe ball includes elliposoidal body, the vertical outlet tube A for being fixed on body bottom and consolidates
Outlet tube B, the outlet tube B curved one at the top of body is scheduled on as vertical pipe, other end is bent towards inside safe ball, described vertical
Outlet tube A is inserted into inside sealing-plug；The condensing bulb includes the spiral cold-finger inside bottle body and bottle body, the bottle body upper end
Steam inlet is offered, lower end offers distillate outlet, and side offers cooling water inlet and cooling water outlet, the cooling
Water inlet and cooling water outlet are connected with chilled water unit.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820114150.9U CN208482027U (en) | 2018-01-24 | 2018-01-24 | A kind of novel integrated distillation apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820114150.9U CN208482027U (en) | 2018-01-24 | 2018-01-24 | A kind of novel integrated distillation apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208482027U true CN208482027U (en) | 2019-02-12 |
Family
ID=65255857
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820114150.9U Expired - Fee Related CN208482027U (en) | 2018-01-24 | 2018-01-24 | A kind of novel integrated distillation apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208482027U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109772487A (en) * | 2019-03-19 | 2019-05-21 | 长沙永乐康仪器设备有限公司 | A kind of full-automatic distillation apparatus |
| CN110404282A (en) * | 2019-09-10 | 2019-11-05 | 北京师范大学 | It is a kind of can an accurate quantitative analysis recycle the Rotary Evaporators of multiple solvents |
| CN110404283A (en) * | 2019-09-10 | 2019-11-05 | 北京师范大学 | It is a kind of can an accurate quantitative analysis Rotary Evaporators of multiple samples are concentrated |
-
2018
- 2018-01-24 CN CN201820114150.9U patent/CN208482027U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109772487A (en) * | 2019-03-19 | 2019-05-21 | 长沙永乐康仪器设备有限公司 | A kind of full-automatic distillation apparatus |
| CN110404282A (en) * | 2019-09-10 | 2019-11-05 | 北京师范大学 | It is a kind of can an accurate quantitative analysis recycle the Rotary Evaporators of multiple solvents |
| CN110404283A (en) * | 2019-09-10 | 2019-11-05 | 北京师范大学 | It is a kind of can an accurate quantitative analysis Rotary Evaporators of multiple samples are concentrated |
| CN110404282B (en) * | 2019-09-10 | 2024-03-22 | 北京师范大学 | Rotary evaporator capable of accurately and quantitatively recycling multiple solvents at one time |
| CN110404283B (en) * | 2019-09-10 | 2024-03-22 | 北京师范大学 | Rotary evaporator capable of accurately and quantitatively concentrating multiple samples at one time |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190212 Termination date: 20210124 |