CN208192128U - A kind of MEMS euthermic chip integrating multiple Pt film resistor temperature sensors - Google Patents

A kind of MEMS euthermic chip integrating multiple Pt film resistor temperature sensors Download PDF

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Publication number
CN208192128U
CN208192128U CN201820006194.XU CN201820006194U CN208192128U CN 208192128 U CN208192128 U CN 208192128U CN 201820006194 U CN201820006194 U CN 201820006194U CN 208192128 U CN208192128 U CN 208192128U
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substrate
mems
film resistor
temperature
temperature sensors
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韩熠
陈李
李廷华
李寿波
徐溢
吴俊�
朱东来
巩效伟
洪鎏
张霞
袁大林
陈永宽
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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Abstract

The utility model discloses a kind of MEMS euthermic chips for integrating multiple Pt film resistor temperature sensors, comprising: there is the microcavity body (2) of concave in the first substrate (1-1), front;There is the micro through hole (3) through the first substrate (1-1) in microcavity body (2);Second substrate (1-2), there is the miniflow channel array (4) perpendicular to its back side at its back side, front center region is equipped with perpendicular to its positive porous structure (5), and miniflow channel array (4) is connected to porous structure (5);Its front face surface has multiple Pt film resistor temperature sensors (6);The front of first substrate (1-1) is together with the back adhesive of the second substrate (1-2).The problems such as euthermic chip of the utility model can carry out real-time measurement to the temperature of euthermic chip, effectively prevent temperature measurement inaccuracy.

Description

A kind of MEMS euthermic chip integrating multiple Pt film resistor temperature sensors
Technical field
The utility model relates to electronic cigarette technical field, in particular to one kind integrates multiple Pt film resistor temperature sensors MEMS electronic cigarette euthermic chip.
Background technique
Most commercially available electronic cigarettes use heating wire for heater element, and under power supply state, heating wire is converted by electric heating and produced Raw high heat heating tobacco juice is allowed to be atomized.Due to helical structure and oil-guiding element the winding side on it of heating wire itself Formula, so that the phenomenon that localized hyperthermia inevitably occurs at work in heating wire.Tobacco juice ingredient, Oil Guide the material temperature excessively high in electronic cigarette The lower variation that physicochemical property can occur of degree, it is possible to create harmful pyrolysis product;Under high temperature, some fragrance components in tobacco juice can quilt It destroys, influences to inhale the rich of taste;The excessively high flue-gas temperature that atomization can also generated of electronic cigarette temperature is excessively high, may be to respiratory tract It causes to damage;In the case where tobacco juice insufficient supply, excessively high temperature can also burn atomization core (paste core), generate burning, suction Experience is deteriorated.
In order to improve disadvantages described above, in recent years, occurs temperature control technology in electronic cigarette.The basic principle of the temperature control technology Be: electronic cigarette temperature controlling chip passes through the resistance for reading heating wire, to monitor heating wire temperature.Heating wire is substantially resistance wire, When heating wire temperature increases, the Collision Number between heating wire internal metal ion increases therewith, and then the resistivity of metal can be with Temperature change, it is associated by temperature-coefficient of electrical resistance between temperature and resistance value.Specifically, electronic cigarette is built-in with heating wire resistance value Detection circuit allows user to like the maximum temperature of setting heating wire according to itself.The reference resistance of heating wire is surveyed at room temperature It is fixed, to determine correct temperature relevant to benchmark resistance value, then, resistance value and application when being started by METHOD FOR CONTINUOUS DETERMINATION electronic cigarette Resistance v. temperature formula estimates the operating temperature of electronic cigarette.By the special algorithm of temperature controlling chip, regulating cell output power, Heating wire resistance value is set to be no more than calculated value corresponding with user's set temperature.Currently used temp controlled heating silk type mainly has Nickel 200, titanium and 316 stainless steel wires etc..The advantage of the technology be heating wire will not overheat, will not dry combustion method, also while avoiding cigarette The peculiar smell and harmful substance generated under the excessively high evaporating temperature of liquid, is substantially improved the overall experience and safety in utilization of electronic cigarette.
Currently, " temperature control " that is applied to electronic cigarette is actually to converse corresponding temperature according to the resistance change of metal To realize so-called " temperature control ", finally still realized according to the resistance variations of heating wire.The temperature control mode is not logical Excess temperature sensor detects temperature, but calculates the change in resistance of heating wire by electronic cigarette host chip to converse temperature Information, so the temperature control of actually current electronic cigarette is using the change in resistance of heating wire as foundation, it is not with actual temperature Come what is judged, as a result, the accuracy of temperature is directly related to the accuracy of resistance value, and the initial resistance value as fruit chip detects is inaccurate Really, that would not be accurate according to the temperature that temperature-coefficient of electrical resistance calculates, if radix mistake, that entire calculated result is also Mistake.In addition, the temperature control mode still remains following problems: the resistance value of heating wire can only reflect whole temperature conditions, When generation local temperature is excessively high, cannot effectively it monitor;Secondly in use, heating wire can because high temperature ageing, The reasons such as oxidation lead to the variation of resistance, and it is increasing to will lead to temperature measurement error.
In numerous temp measuring methods, resistance temperature sensor (or thermometer resistor, usual abbreviation RTD) is most accurate side One of method, and advantage of the film resistor temperature sensor compared to tradition RTD is highly sensitive and rapid thermal response, this is because its Lesser size reduces the heat exchange between sensing element and environment.Metal platinum (Pt) is because of good response, the resistivity to heat Highly linear between temperature is positively correlated and long-term chemical durability at high temperature, and becomes Thin film resistive temperature and sense The preferred material of device.Currently, COMS (complementary metal oxide semiconductor) work can be used in majority Pt film resistor temperature sensor Skill or MEMS (MEMS) technique are prepared on silicon or metal substrate.Pt is used especially in MEMS device, is allowed Manufacture can have the structure of high resistance to plastic deformation when the temperature rises.
Utility model content
Utility model aims to solve existing electronic cigarette temperature control technology there are the problem of, using advanced MEMS Processing technology designs the MEMS electronic cigarette euthermic chip and its manufacturing method of integrated temperature sensor.It is passed by integrated temperature Sensor, real-time and accurately measures the temperature of MEMS euthermic chip, and cooperates external temperature controller, realizes MEMS euthermic chip It accurately controls, makes tobacco juice uniform atomizing.
The utility model first aspect discloses a kind of MEMS heat generating core for integrating multiple Pt film resistor temperature sensors Piece, comprising:
First substrate (1-1), in the form of sheets, front have the microcavity body (2) of concave;Have in the microcavity body (2) through institute State the micro through hole (3) of the first substrate (1-1);
Second substrate (1-2), in the form of sheets, the back side have the miniflow channel array (4) perpendicular to its back side, front center region Equipped with perpendicular to its positive porous structure (5), the miniflow channel array (4) is connected to porous structure (5);Its front face surface There are multiple Pt film resistor temperature sensors (6);
The front of first substrate (1-1) is together with the back adhesive of second substrate (1-2).
Preferably, the depth of the microcavity body (2) is 1 millimeter to 5 millimeters;The diameter of the micro through hole (3) is 500 microns To 1 millimeter.
Preferably, there is a metallic film in the front of second substrate (1-2), the metallic film with a thickness of 200~ 500nm;The metallic film material sputtered is one or more of Ti/Pt or Cr/Pt.
Preferably, the diameter of the fluid channel of the miniflow channel array (4) is 10 microns to 500 microns, the fluid channel Depth is the 1/2~3/4 of the second substrate (1-2) height.
Preferably, the aperture of the porous structure (5) is 100 nanometers to 1000 nanometers.
Preferably, first substrate is made of glass or high resistant monocrystalline silicon, and the resistivity of the high resistant monocrystalline silicon is greater than 10Ω·cm。
Preferably, second substrate is made of low-resistance single crystal silicon, and the resistivity of the low-resistance single crystal silicon is less than 0.01 Ω·cm。
A kind of MEMS heat generating core for integrating multiple Pt film resistor temperature sensors of the second disclosure of the invention of the utility model The preparation method of piece, comprising the following steps:
The preparation of first substrate (1-1):
(1) microcavity body figure is lithographically formed in the front of the high resistance monocrystalline silicon wafer of sheet glass or resistivity greater than 10 Ω cm Then shape corrodes microcavity body (2) out using etchant solution;
(2) photoetching is carried out to the obtained sheet glass of step (1) or the high resistance monocrystalline silicon wafer back side, then uses etchant solution Corrode the micro through hole (3) for running through the sheet glass or high resistance monocrystalline silicon wafer out;Obtain first substrate (1-1);
The preparation of second substrate (1-2):
(a) fluid channel array of figure is lithographically formed less than the back side of the silicon wafer of the low-resistivity of 0.01 Ω cm in resistivity Shape;
(b) back side of the low-resistivity silicon wafer of step (a) is performed etching using deep reaction ion etching technique, is formed micro- Runner array (4);
(c) using low-pressure chemical vapor deposition process to the front deposition one of the obtained low-resistivity silicon wafer of step (b) Layer silicon nitride;
(d) photoetching is carried out to the front of the obtained low-resistivity silicon wafer of step (c), is gone using reactive ion etching process Except the exposed silicon nitride layer in middle part;
(e) porous knot is gone out to the front etch of the obtained low-resistivity silicon wafer of step (d) using electrochemical corrosive process Structure (5) is connected to porous structure with the miniflow channel array at the back side;
(f) to the obtained low-resistivity silicon wafer of step (e) in positive photoetching, magnetron sputtering deposits to form metallic film;
(g) photoetching of spin coating photoresist, formation temperature are carried out in the front side of silicon wafer of the obtained sputtered metal film of step (f) Sensor pattern;
(h) metallic film exposed using dry etch step (g), leaves required metal thin-film pattern;
(i) the remaining photoresist of the surface step (h) institute is removed with acetone,;
(j) the front side of silicon wafer surface that photoresist is removed in (i) sputters alumina layer;
(K) in the described alumina layer surface (j) aluminium oxide that the photoetching of spin coating photoresist and use dry etching expose again Layer;
(l) after removing (k) remaining photoresist with acetone, as described second substrate (1-2)
Integrate the preparation of the MEMS euthermic chip of multiple Pt film resistor temperature sensors:
The front of first substrate (1-1) and the back side of second substrate (1-2) are in close contact by (first), by strong Technique is closed to be bonded together;
(second) carries out scribing using the chip that scribing machine obtains step (first);
(the third) high temperature sintering after the second substrate face silver paste bonding conducting wire for the chip scribing for obtaining step (second) Cooled to room temperature is afterwards to get to the MEMS euthermic chip for integrating multiple Pt film resistor temperature sensors.
Preferably, corrosive liquid described in step (1) or (2), wherein the corrosive liquid of sheet glass is hydrofluoric acid solution, high resistant list The corrosive liquid of crystal silicon chip is one of potassium hydroxide solution or tetramethyl ammonium hydroxide solution.
Preferably, the metallic film material that step (f) is sputtered is one or more of Ti/Pt or Cr/Pt.
Preferably, high temperature described in step (third) is 300~700 DEG C, and sintering time is 10~20 minutes.
The beneficial outcomes of the utility model:
(1) the utility model sends out electronic cigarette using the MEMS euthermic chip for integrating multiple Pt film resistor temperature sensors The temperature of hot chip carries out real-time measurement, and temperature measurement is accurate, and sensor life-time length, reliable operation effectively prevent existing electricity Sub- cigarette fever temperature measurement inaccuracy, heater aging lead to problems such as temperature detecting resistance constantly change;Chip can be carried out real Shi Wendu control, first is that avoiding overheating;Second is that temperature adjusting can be carried out according to user demand, thus change atomization quantity, tobacco juice point It is good to dissipate effect, homogeneous heating can effectively improve heat utilization efficiency, improve atomizing effect.
(2) can multiple platinum resistance temperature sensors be arranged according to actual needs in the utility model, to chip surface temperature Distributed measurement is carried out, the Temperature Distribution of chip different zones is obtained, avoidable existing method leads to not measure heater office The problem of portion's temperature.
Detailed description of the invention
Fig. 1 is the side, sectional of the MEMS euthermic chip for integrating multiple Pt film resistor temperature sensors of the utility model Figure;
Fig. 2 is the first side of substrate of the utility model cross-sectional view;
Fig. 3 the second side of substrate cross-sectional view;
Fig. 4 the second substrate face top view;
Fig. 5 the second substrate back top view.
Appended drawing reference are as follows: 1-1, the first substrate;1-2, the second substrate;2, microcavity body;3, micro through hole;4, fluid channel displays; 5, porous structure;6, Pt temperature sensor;7, silicon nitride layer;8,Al2O3Layer.
Specific embodiment
The utility model first aspect discloses a kind of MEMS heat generating core for integrating multiple Pt film resistor temperature sensors Piece, comprising:
First substrate (1-1), in the form of sheets, front have the microcavity body (2) of concave;Have in the microcavity body (2) through institute State the micro through hole (3) of the first substrate (1-1);
Second substrate (1-2), in the form of sheets, the back side have the miniflow channel array (4) perpendicular to its back side, front center region Equipped with perpendicular to its positive porous structure (5), the miniflow channel array (4) is connected to porous structure (5);Its front face surface There are multiple Pt film resistor temperature sensors (6);
The front of first substrate (1-1) is together with the back adhesive of second substrate (1-2).
The depth of the microcavity body (2) is 3 millimeters;The diameter of the micro through hole (3) is 750 microns.
There is a metallic film in the front of second substrate (1-2), the metallic film with a thickness of 350nm;The metal The material of film is Ti/Pt/Au.
The diameter of the fluid channel of the miniflow channel array (4) is 35 microns, and the depth of the fluid channel is second lining The 1/2 of bottom (1-2) height.
The aperture of the porous structure (5) is 500 nanometers.
First substrate is made of glass or high resistant monocrystalline silicon, and the resistivity of the high resistant monocrystalline silicon is 20 Ω cm.
Second substrate is made of low-resistance single crystal silicon, and the resistivity of the low-resistance single crystal silicon is 0.005 Ω cm.
A kind of preparation method step for the MEMS euthermic chip integrating multiple Pt film resistor temperature sensors are as follows:
The preparation of first substrate (1-1):
(1) it is lithographically formed microcavity volume graphic in the front for the high resistance monocrystalline silicon wafer that resistivity is 20 Ω cm, then used Corrosive liquid is that potassium hydroxide solution corrodes microcavity body (2) out;
(2) photoetching is carried out to the obtained high resistance monocrystalline silicon wafer back side of step (1), then uses corrosive liquid for potassium hydroxide Solution corrosion goes out the micro through hole (3) of the sheet glass or high resistance monocrystalline silicon wafer that run through described;Obtain the first substrate (1- 1);
The preparation of second substrate (1-2):
(a) fluid channel array pattern is lithographically formed at the back side of the silicon wafer for the low-resistivity that resistivity is 0.005 Ω cm;
(b) back side of the low-resistivity silicon wafer of step (a) is performed etching using deep reaction ion etching technique, is formed micro- Runner array (4);
(c) using low-pressure chemical vapor deposition process to the front deposition one of the obtained low-resistivity silicon wafer of step (b) Layer silicon nitride;
(d) photoetching is carried out to the front of the obtained low-resistivity silicon wafer of step (c), is gone using reactive ion etching process Except the exposed silicon nitride layer in middle part;
(e) porous knot is gone out to the front etch of the obtained low-resistivity silicon wafer of step (d) using electrochemical corrosive process Structure (5) is connected to porous structure with the miniflow channel array at the back side;
(f) to the obtained low-resistivity silicon wafer of step (e) in positive photoetching, magnetron sputtering deposits to form Ti/Pt metal Film;
(g) there is the front side of silicon wafer of metallic film to carry out the photoetching of spin coating photoresist in obtained sputter of step (f), form temperature Spend sensor pattern;
(h) metallic film exposed using dry etch step (g), leaves required metal thin-film pattern;
(i) the remaining photoresist of the surface step (h) institute is removed with acetone,;
(j) the front side of silicon wafer surface that photoresist is removed in (i) sputters alumina layer;
(K) in the described alumina layer surface (j) aluminium oxide that the photoetching of spin coating photoresist and use dry etching expose again Layer;
(l) after removing (k) remaining photoresist with acetone, as described second substrate (1-2)
Integrate the preparation of the MEMS euthermic chip of multiple Pt film resistor temperature sensors:
The front of first substrate (1-1) and the back side of second substrate (1-2) are in close contact by (first), by strong Technique is closed to be bonded together;
(second) carries out scribing using the chip that scribing machine obtains step (first);
(the third) 600 DEG C of burnings after the second substrate face silver paste bonding conducting wire for the chip scribing for obtaining step (second) Knot after ten minutes cooled to room temperature to get to the MEMS heat generating core for integrating multiple Pt film resistor temperature sensors Piece.

Claims (5)

1. a kind of MEMS euthermic chip for integrating multiple Pt film resistor temperature sensors characterized by comprising
First substrate (1-1), in the form of sheets, front have the microcavity body (2) of concave;Have in the microcavity body (2) through described the The micro through hole (3) of one substrate (1-1);First substrate is made of glass or high resistant monocrystalline silicon, the electricity of the high resistant monocrystalline silicon Resistance rate is greater than 10 Ω cm;
Second substrate (1-2), in the form of sheets, the back side have the miniflow channel array (4) perpendicular to its back side, and front center region is equipped with Perpendicular to its positive porous structure (5), the miniflow channel array (4) is connected to porous structure (5);Its front face surface has multiple Pt film resistor temperature sensor (6);Second substrate is made of low-resistance single crystal silicon, and the resistivity of the low-resistance single crystal silicon is small In 0.01 Ω cm;
The front of first substrate (1-1) is together with the back adhesive of second substrate (1-2).
2. the MEMS euthermic chip according to claim 1 for integrating multiple Pt film resistor temperature sensors, feature exist In the depth of the microcavity body (2) is 1 millimeter to 5 millimeters;The diameter of the micro through hole (3) is 500 microns to 1 millimeter.
3. the MEMS euthermic chip according to claim 1 for integrating multiple Pt film resistor temperature sensors, feature exist Have a metallic film in, the front of second substrate (1-2), the metallic film with a thickness of 200~500nm;The metal The material of film is one or more of Ti/Pt/Au, TiW/Au, Al, Cr or Pt/Au.
4. the MEMS euthermic chip according to claim 1 for integrating multiple Pt film resistor temperature sensors, feature exist It is 10 microns to 500 microns in the diameter of, the fluid channel of the miniflow channel array (4), the depth of the fluid channel is described the The 1/2~3/4 of two substrates (1-2) height.
5. the MEMS euthermic chip according to claim 1 for integrating multiple Pt film resistor temperature sensors, feature exist In the aperture of the porous structure (5) is 100 nanometers to 1000 nanometers.
CN201820006194.XU 2018-01-03 2018-01-03 A kind of MEMS euthermic chip integrating multiple Pt film resistor temperature sensors Active CN208192128U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108158039A (en) * 2018-01-03 2018-06-15 云南中烟工业有限责任公司 A kind of MEMS euthermic chips and its manufacturing method for integrating multiple Pt temperature sensors
CN110430625A (en) * 2019-06-10 2019-11-08 深圳桐源科技有限公司 Aerosol generating system, heating module, temperature checking method and device
CN112345111A (en) * 2020-09-28 2021-02-09 中国电子科技集团公司第二十九研究所 High-power heat source chip and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108158039A (en) * 2018-01-03 2018-06-15 云南中烟工业有限责任公司 A kind of MEMS euthermic chips and its manufacturing method for integrating multiple Pt temperature sensors
CN110430625A (en) * 2019-06-10 2019-11-08 深圳桐源科技有限公司 Aerosol generating system, heating module, temperature checking method and device
CN112345111A (en) * 2020-09-28 2021-02-09 中国电子科技集团公司第二十九研究所 High-power heat source chip and preparation method thereof

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