CN208032536U - Glycine betaine production column reactor - Google Patents
Glycine betaine production column reactor Download PDFInfo
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- CN208032536U CN208032536U CN201721864521.7U CN201721864521U CN208032536U CN 208032536 U CN208032536 U CN 208032536U CN 201721864521 U CN201721864521 U CN 201721864521U CN 208032536 U CN208032536 U CN 208032536U
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- mixing chamber
- reative cell
- heating
- mouth
- channel
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- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 title claims abstract description 54
- 229960003237 betaine Drugs 0.000 title claims abstract description 52
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 30
- 238000002156 mixing Methods 0.000 claims abstract description 156
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 98
- 238000010438 heat treatment Methods 0.000 claims abstract description 92
- 238000001816 cooling Methods 0.000 claims abstract description 61
- 238000006243 chemical reaction Methods 0.000 claims abstract description 15
- 238000010079 rubber tapping Methods 0.000 claims description 9
- 238000004821 distillation Methods 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 4
- 210000004027 cell Anatomy 0.000 description 107
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 16
- FDRCDNZGSXJAFP-UHFFFAOYSA-M sodium chloroacetate Chemical compound [Na+].[O-]C(=O)CCl FDRCDNZGSXJAFP-UHFFFAOYSA-M 0.000 description 10
- 239000000243 solution Substances 0.000 description 10
- 239000002994 raw material Substances 0.000 description 9
- 235000017550 sodium carbonate Nutrition 0.000 description 8
- 229910000029 sodium carbonate Inorganic materials 0.000 description 8
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 8
- 230000004060 metabolic process Effects 0.000 description 5
- 239000003925 fat Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 235000019197 fats Nutrition 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000036528 appetite Effects 0.000 description 2
- 235000019789 appetite Nutrition 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000001727 in vivo Methods 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 239000012047 saturated solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- 241000143060 Americamysis bahia Species 0.000 description 1
- 235000019737 Animal fat Nutrition 0.000 description 1
- 208000004930 Fatty Liver Diseases 0.000 description 1
- 206010019708 Hepatic steatosis Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 208000034189 Sclerosis Diseases 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 235000019730 animal feed additive Nutrition 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
- 208000010706 fatty liver disease Diseases 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000002440 hepatic effect Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 230000002101 lytic effect Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 210000003470 mitochondria Anatomy 0.000 description 1
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- 239000002736 nonionic surfactant Substances 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 238000009304 pastoral farming Methods 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 229960002668 sodium chloride Drugs 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 231100000240 steatosis hepatitis Toxicity 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
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- 229940045997 vitamin a Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
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Abstract
The utility model discloses a kind of glycine betaine production column reactor, inlet port and outlet port are provided in cylindrical body, mixing chamber, reative cell and distillery, mixing chamber is arranged inside cylindrical body is connected with feed inlet, and mixing component is provided in mixing chamber；The side wall of reative cell is provided with dosing mouth, and multiple heating tubes are provided in distillery, and multiple heating tubes are vertically arranged, and the upper end side wall of distillery is provided with hot water outlet；Temperature control channel be arranged cylindrical body madial wall and mixing chamber, reative cell and distillery side wall between, temperature control channel includes heating channel and cooling channel, the side wall of mixing chamber and reative cell is both provided with heating mouth and cooling mouth, heating mouth is connected with heating channel, cooling mouth is connected with cooling channel, and opening mechanism is both provided on heating mouth and cooling mouth.Reactor provided by the utility model can be adjusted the temperature of each reaction process of glycine betaine by a temperature control channel.
Description
Technical field
The utility model is related to glycine betaine production technical fields, are reacted with pillar more particularly to a kind of glycine betaine production
Device.
Background technology
The chemical name of glycine betaine is betaine.It is one of main alkaloid.Glycine betaine has mild
Pharmacological action, participate in fat metabolism, improve mitochondria in triglyceride content, remove liver in superabundant fats, have improving eyesight,
The effects that preventing fatty liver, hepatic sclerosis, liver made to get well, protecting kidney.Glycine betaine, which is one kind again in vivo, most to be had
The infiltration lytic agent of effect has important metabolism effect.It can promote animal protein and fat metabolism, mitigate emergent, tune
Osmotic pressure is saved, is improved a poor appetite, stable vitamin participates in preventing globidiosis.Methyl is very unstable in vivo, in animal body again
It itself cannot synthesize, food supply can only be relied on.Glycine betaine as methyl donor participate in several metabolism, especially protein and
The metabolism of fat.Glycine betaine can increase appetite of livestock and poultry as feed addictive, improve vitamin A, K, B, B6 etc. in feed
In stability.When glycine betaine is for aquatic animal feed additives such as fish, shrimps, the palatability of feed can be improved, it is dynamic to aquatic products
Object smell and the sense of taste have preferable temptation, to improve its grazing rate, promote its growth and development.Glycine betaine is as nonionic
Surfactant is also widely used for the industries such as daily use chemicals, printing and dyeing.Therefore glycine betaine has a vast market foreground.
In the production process of glycine betaine, the different stages, required temperature was inconsistent, however existing glycine betaine closes
It is reacted using stacked at reaction, during the reaction its centralized head load of reactor, each stage is heated consistent, and it is anti-to influence the synthesis
Rate and conversion ratio are answered, often occurs reacting halfway problem.If being respectively provided with temperature control equipment, cost in each stage
It is higher and safeguard get up it is more complicated, result in waste of resources.
Utility model content
The purpose of this utility model is to provide a kind of glycine betaine production column reactor, with solve it is in the prior art not
Foot place.
To achieve the goals above, the utility model provides the following technical solutions：
A kind of glycine betaine production column reactor, including cylindrical body are provided in the cylindrical body at least one
Feed inlet and at least one discharge port, the feed inlet are arranged at the top of the cylindrical body, and the discharge port is arranged in institute
State the bottom of cylindrical body；Mixing chamber, the mixing chamber are arranged inside the cylindrical body, the mixing chamber and the charging
Mouth is connected, and the side wall of the mixing chamber is additionally provided with water inlet, and mixing component is provided in the mixing chamber；Reative cell, institute
It states reative cell to be arranged in the inside of the cylindrical body and positioned at the lower section of the mixing chamber, the upper end of the reative cell passes through company
It connects road with the mixing chamber to be connected, the side wall of the reative cell is provided with dosing mouth；Position is arranged in distillery, the distillery
It is connected by tapping channel in the lower section of the mixing chamber and with the mixing chamber, multiple heating is provided in the distillery
Pipe, multiple heating tubes are vertically arranged, and fluid course, the upper end side wall of the distillery are formed between each heating tube
It is provided with hot water outlet；Temperature control channel, the temperature control channel setting are mixed in the cylindrical body madial wall with described
It closes between room, reative cell and the side wall of distillery, the temperature control channel includes heating channel and cooling channel, the mixing
The side wall of room and reative cell is both provided with heating mouth and cooling mouth, and the heating mouth is connected with the heating channel, the drop
Warm mouth is connected with the cooling channel, and opening mechanism is both provided on the heating mouth and cooling mouth.
Above-mentioned glycine betaine production column reactor, the heating channel include hot-water cavity and heating chamber, the hot water
Chamber is arranged between the madial wall and the lateral wall of the distillation chamber of the cylindrical body, and the hot-water cavity is connected with hot water outlet
Logical, the hot-water cavity is connected with the mixing chamber and reative cell respectively by the connecting tube.
Madial wall and institute in the cylindrical body is arranged in above-mentioned glycine betaine production column reactor, the heating chamber
It states between mixing chamber and the madial wall of reative cell, heating device is provided in the heating chamber, the mixing chamber and reative cell are logical
The heating mouth is crossed with the heating chamber to be connected.
Above-mentioned glycine betaine production column reactor, the cooling channel include cold water cavity and cooling chamber, the cold water
Chamber is arranged between the madial wall and the lateral wall of the distillation chamber of the cylindrical body, and the cold water cavity is logical with the hot-water cavity
It crosses connecting tube to be connected, the cold water cavity is connected with the mixing chamber and reative cell respectively by the connecting tube.
Madial wall and institute in the cylindrical body is arranged in above-mentioned glycine betaine production column reactor, the cold water cavity
It states between mixing chamber and the madial wall of reative cell, heat sink is provided in the cold water cavity, the mixing chamber and reative cell are logical
The cooling mouth is crossed with the cold water cavity to be connected.
Above-mentioned glycine betaine production column reactor is provided with vertical clapboard, the vertical clapboard in the mixing chamber
The mixing chamber is separated into left mixing chamber and right mixing chamber, the charging is both provided on the left mixing chamber and right mixing chamber
Mouth, water inlet, cooling mouth and heating mouth.
Above-mentioned glycine betaine production column reactor is provided with horizontal baffle, the horizontal baffle in the reative cell
The reative cell is divided into upper reative cell and lower reative cell, is connected between the upper reative cell and lower reative cell, it is described on
Dosing mouth, cooling mouth and heating mouth are both provided on reative cell and lower reative cell.
Above-mentioned glycine betaine production column reactor, the left mixing chamber, right mixing chamber, upper reative cell and lower reative cell
It is connected with the hot-water cavity and cold water cavity by the connecting tube.
Above-mentioned glycine betaine production column reactor, the mixing chamber, reative cell, distillery, cooling channel and heating
It is both provided with temperature inductor in channel, autocontrol valve is both provided in the interface channel, tapping channel and connecting tube.
In the above-mentioned technical solutions, glycine betaine production column reactor provided by the utility model is set in cylindrical body
It is equipped at least one feed inlet and at least one discharge port, cylindrical body is internally provided with mixing chamber, reative cell and distillery,
Cylindrical body madial wall and mixing chamber, reative cell and distillery side wall between be provided with temperature control channel, temperature control is logical
Road includes heating channel and cooling channel, and the side wall of mixing chamber and reative cell is both provided with heating mouth and cooling mouth, heating mouth with
Heating channel is connected, and cooling mouth is connected with cooling channel, opening mechanism is both provided on heating mouth and cooling mouth, by beating
Opening mechanism can open corresponding heating mouth and cooling mouth so passes through to adjust the temperature of corresponding mixing chamber and reative cell
One temperature control channel can meet the temperature requirement of each reaction process of glycine betaine.
Description of the drawings
In order to illustrate the technical solutions in the embodiments of the present application or in the prior art more clearly, below will be to institute in embodiment
Attached drawing to be used is needed to be briefly described, it should be apparent that, the accompanying drawings in the following description is only described in the utility model
Some embodiments, for those of ordinary skill in the art, other drawings may also be obtained based on these drawings.
Fig. 1 is the structural schematic diagram for the glycine betaine production column reactor that the utility model embodiment provides.
Reference sign：
1, cylindrical body；1.1, feed inlet；1.2, discharge port；2, mixing chamber；2.1, vertical clapboard；2.2, left mixing chamber；
2.3, right mixing chamber；2.4, water inlet；2.5, mixing component；2.6, interface channel；3, reative cell；3.1 horizontal baffle；3.2, on
Reative cell；3.3, lower reative cell；3.4, tapping channel；4, distillery；4.1, heating tube；4.2, hot water outlet；4, heating channel；
4.1, heat up mouth；4.2, heating device；4.3, hot-water cavity；5, cool down channel；5.1, cool down mouth；5.2, heat sink；5.3, cold
Water cavity；6, connecting tube；7, opening mechanism；8, temperature inductor；9, autocontrol valve.
Specific implementation mode
In order to make those skilled in the art more fully understand the technical solution of the utility model, below in conjunction with attached drawing pair
The utility model is further detailed.
As shown in Figure 1, a kind of glycine betaine production column reactor that the utility model embodiment provides, including column sheet
Body 1, at least one feed inlet 1.1 and at least one discharge port 1.2 are provided in cylindrical body 1, and feed inlet 1.1 is arranged in column
The top of ontology 1, discharge port 1.2 are arranged in the bottom of cylindrical body 1；Mixing chamber 2, mixing chamber 2 are arranged in cylindrical body 1
Portion, mixing chamber 2 are connected with feed inlet 1.1, and the side wall of mixing chamber 2 is additionally provided with the first water inlet 2.4, is arranged in mixing chamber 2
There is mixing component 2.5；Reative cell 3, reative cell 3 are arranged in the inside of cylindrical body 1 and positioned at the lower section of mixing chamber 2, reative cell 3
Upper end be connected with mixing chamber 2 by interface channel 2.6, the side wall of reative cell 3 is provided with dosing mouth；Distillery 4, distillery
4 settings by tapping channel 3.4 are connected positioned at the lower section of mixing chamber 2 and with mixing chamber 2, and multiple add is provided in distillery 4
Heat pipe 4.1, multiple heating tubes 4.1 are vertically arranged, and fluid course, the upper end of distillery 4 are formed between each heating tube 4.1
Side wall is provided with hot water outlet 4.2；Temperature control channel, temperature control channel are arranged in 1 madial wall of cylindrical body and mixing chamber
2, between reative cell 3 and the side wall of distillery 4, temperature control channel includes heating channel 4 and cooling channel 5, mixing chamber 2 and anti-
The side wall of room 3 is answered to be both provided with heating mouth 4.1 and cooling mouth 5.1, heating mouth 4.1 is connected with heating channel 4, and cool down mouth 5.1
It is connected with cooling channel 5, opening mechanism 7 is both provided on heating mouth 4.1 and cooling mouth 5.1.
Specifically, cylindrical body 1 is the main body mechanism of reactor, mixing chamber 2, reative cell 3, distillery 4 and temperature control
Channel is arranged inside cylindrical body 1, and at least one feed inlet 1.1 and at least one discharge port are provided in cylindrical body 1
1.2, feed inlet 1.1 and discharge port 1.2 can be one, can also be multiple, while feed inlet 1.1 can design as needed
At feeding-in solid body mouth 1.1 and liquid inlet opening 1.1, feed inlet 1.1 is arranged at the top of cylindrical body 1, can by feed inlet 1.1
With the transferring raw material into cylindrical body 1, discharge port 1.2 is arranged at the top of cylindrical body 1, what discharge port 1.2 was used to produce
Aqueous solutions of betaine exports, and the upper position in cylindrical body 1 is arranged in mixing chamber 2, and mixing chamber 2 can be one, can also root
It is two or more according to needing to be designed to, by mixing chamber 2 to produce glycine betaine raw material mix, when need to raw material carry out
When mixing respectively, it can be mixed by designing the mixing chamber 2 of different numbers, feed inlet 1.1 is respectively provided on each mixing chamber 2,
Multiple mixing chambers 2 can be set up in parallel, can also be setting up and down, for example be raw material by sodium carbonate, monoxone and trimethylamine
When, it is provided with two mixing chambers 2 arranged side by side in cylindrical body 1, agitating device, agitating device are both provided in each mixing chamber 2
Including stirring motor, agitating shaft and stirring blade, feed inlet 1.1 and water inlet 2.4 are both provided on each mixing chamber 2, at one
Sodium carbonate and water are added in mixing chamber 2, is sufficiently stirred under the action of agitating device and soda ash solution is made, in another mixing chamber
Monoxone and water are added in 2, is stirred under the action of agitating device and monoxone saturated solution is made, set in the lower section of mixing chamber 2
It is equipped with reative cell 3, reative cell 3 is connected with mixing chamber 2 by interface channel 2.6, and reative cell 3 is according to the process and need of reaction
It wants, one or more can be designed, multiple reative cells 3, which are formed, generates the multiple intermediate reaction objects of glycine betaine and end reaction object,
It is also provided with dosing mouth and filler in the side wall of reative cell 3, reaction can be added into reative cell 3 by dosing mouth needs
The raw material wanted is provided with tapping channel 3.4 in the bottom of reative cell 3, and tapping channel 3.4 is connected with distillery 4, by reative cell
Reactant after 3 reactions is exported to distillery 4, multiple heating tubes 4.1 is provided in distillery 4, heating tube 4.1 is along vertical side
To setting, fluid course is formed between each heating tube 4.1, the upper end side wall of distillery 4 is provided with hot water outlet 4.2, heating tube
Heating chamber is connected on 4.1, reactant is heated by heating tube 4.1, hot steam is exported by hot water outlet 4.2, is left
Reactant exported by discharge port 1.2, the processing such as be then filtered, dry and obtaining final glycine betaine.
In the present embodiment, during glycine betaine produces, mixing chamber 2, reative cell 3 and distillery 4 are required to different
Temperature, and when mixing chamber 2 and reative cell 3 have multiple, each mixing chamber 2 and reative cell 3 are required to different temperature, if
It is both provided with temperature-adjusting device in each mixing chamber 2 and reative cell 3, then increases cost and difficult in maintenance, the present embodiment is in column
The madial wall and mixing chamber 2 of shape ontology 1 are provided with temperature control channel, temperature control between reative cell 3 and the side wall of distillery 4
Channel processed includes mutually independent heating channel 4 and cooling channel 5, and heating mouth is both provided in the side wall of mixing chamber 2 and reative cell 3
4.1 and cooling mouth 5.1, heating mouth 4.1 and cooling mouth 5.1 have it is multiple, multiple heating mouths 4.1 with heat up channel 4 be connected, it is more
A cooling mouth 5.1 is connected with cooling channel 5, is both provided with opening mechanism 7 on heating mouth 4.1 and cooling mouth 5.1, passes through opening
The opening and closing of heating mouth 4.1 and the mouth 5.1 that cools down may be implemented in mechanism 7, when the temperature in mixing chamber 2 or reative cell 3 is less than
Or when higher than specified temperature, by opening corresponding heating mouth 4.1 or cooling mouth 5.1, to mixing chamber 2 or reative cell
Control is adjusted in temperature in 3, so realizes through heat up channel 4 and the channel 5 that cools down to each mixing chamber 2 and reative cell 3
Temperature is adjusted, and avoids the need for being required to setting temperature control device in each mixing chamber 2 and reative cell 3.
In the present embodiment, 2 He of mixing chamber of different numbers is arranged in the raw material and reaction process that can be generated according to glycine betaine
Reative cell 3, is both provided with temperature inductor 8 in each mixing chamber 2 and reative cell 3, and temperature inductor 8 detects 2 He of each mixing chamber
The temperature of reative cell 3, and the temperature of detection is delivered to controller, controller control corresponding opening mechanism 7 open and
It closes, to which the temperature in each mixing chamber 2 and reative cell 3 be adjusted, so that the temperature in mixing chamber 2 and reative cell 3
Degree is constantly in OK range.
The glycine betaine production column reactor that the utility model embodiment provides is provided at least one in cylindrical body 1
A feed inlet 1.1 and at least one discharge port 1.2, cylindrical body 1 are internally provided with mixing chamber 2, reative cell 3 and distillery 4,
Temperature control channel, temperature control are provided between 1 madial wall of cylindrical body and mixing chamber 2, reative cell 3 and the side wall of distillery 4
Channel processed includes heating channel 4 and cooling channel 5, and the side wall of mixing chamber 2 and reative cell 3 is both provided with heating mouth 4.1 and cooling
Mouth 5.1, heating mouth 4.1 are connected with heating channel 4, and cooling mouth 5.1 is connected with cooling channel 5, and heat up mouth 4.1 and cooling mouth
It is both provided with opening mechanism 7 on 5.1, corresponding heating mouth 4.1 and cooling mouth 5.1 can be opened by opening mechanism 7, to adjust
The temperature of corresponding mixing chamber 2 and reative cell 3 so can meet respectively reacting for glycine betaine by a temperature control channel
The temperature requirement of journey.
In the present embodiment, it is preferred that heating channel 4 includes hot-water cavity 4.3 and heating chamber, and hot-water cavity 4.3 is arranged in column
Between the madial wall of ontology 1 and the lateral wall for distilling chamber, hot-water cavity 4.3 is connected with hot water outlet 4.2, and hot-water cavity 4.3 passes through
Connecting tube 6 is connected with mixing chamber 2 and reative cell 3 respectively；Heating chamber be arranged madial wall in cylindrical body 1 and mixing chamber 2 and
Be provided between the madial wall of reative cell 3, in heating chamber heating device 4.2, mixing chamber 2 and reative cell 3 by heat up mouth 4.1 with
Heating chamber is connected.Hot water and steam after being distilled by heating tube 4.1 in distillery 4 is delivered to hot water by hot water outlet 4.2
The water that distillation generates can be continued on to mixing chamber 2 and reative cell 3 by chamber 4.3, the storage in hot-water cavity 4.3, hot-water cavity 4.3
Water in hot-water cavity 4.3 is delivered to by recycling when the temperature in mixing chamber 2 or reative cell 3 is relatively low and needs that water is added
Mixing chamber 2 or reative cell 3 pass through device for opening when the temperature in mixing chamber 2 or reative cell 3 is relatively low but water need not add water
Open heating mouth 4.1 so that heating mouth 4.1 is connected with heating channel 4, and heating channel 4 is to corresponding mixing chamber 2 and reative cell
3 heat up so that the temperature in mixing chamber 2 or reative cell 3 reaches requirement.
In the present embodiment, it is preferred that cooling channel 5 includes cold water cavity 5.3 and cooling chamber, and cold water cavity 5.3 is arranged in column
Between the madial wall of ontology 1 and the lateral wall for distilling chamber, cold water cavity 5.3 is connected with hot-water cavity 4.3 by connecting tube 6, cold water
Chamber 5.3 is connected with mixing chamber 2 and reative cell 3 respectively by connecting tube 6；The madial wall in cylindrical body 1 is arranged in cold water cavity 5.3
Between mixing chamber 2 and the madial wall of reative cell 3, heat sink 5.2, mixing chamber 2 and reative cell 3 are provided in cold water cavity 5.3
By cooling down, mouth 5.1 is connected with cold water cavity 5.3.Cold water cavity 5.3 is connected by connecting tube 6 with hot-water cavity 4.3, and hot-water cavity is worked as
The temperature of water is too low or when water is more in 4.3, and the water in hot-water cavity 4.3 is delivered to cold water cavity 5.3 by connecting tube 6
It is interior.Simultaneously when the temperature in mixing chamber 2 or reative cell 3 is higher and needs that water is added, the water in cold water cavity 5.3 is delivered to mixed
It closes room 2 or reative cell 3 is beaten when the temperature in mixing chamber 2 or reative cell 3 is higher but water need not add water by device for opening
Open cooling mouth 5.1 so that cooling mouth 5.1 is connected with cooling channel 5, and cooling channel 5 is to corresponding mixing chamber 2 and reative cell 3
Carry out cooling processing so that be down to suitable range at the temperature in mixing chamber 2 or reative cell 3.
In the present embodiment, it is preferred that be provided with vertical clapboard 2.1 in mixing chamber 2, vertical clapboard 2.1 separates mixing chamber 2
At left mixing chamber 2.2 and right mixing chamber 2.3, feed inlet 1.1, water inlet are both provided on left mixing chamber 2.2 and right mixing chamber 2.3
2.4, cool down mouth 5.1 and heating mouth 4.1；Horizontal baffle 3.1 is provided in reative cell 3, horizontal baffle 3.1 separates reative cell 3
For upper reative cell 3.2 and lower reative cell 3.3, it is connected between upper reative cell 3.2 and lower reative cell 3.3, upper reative cell 3.2 is under
Dosing mouth, cooling mouth 5.1 and heating mouth 4.1 are both provided on reative cell 3.3.It, can be according to glycine betaine when producing glycine betaine
The raw material and reaction process of production are arranged the mixing chamber 2 and reative cell 3 of different numbers, for example, by sodium carbonate, monoxone and
When trimethylamine is raw material, vertical clapboard 2.1 is set in the mixing chamber 2 of cylindrical body 1, vertical clapboard 2.1 separates mixing chamber 2
At left mixing chamber 2.2 and right mixing chamber 2.3 arranged side by side, agitating device, left mixing chamber 2.2 and the right side are both provided in each mixing chamber 2
It is both provided with feed inlet 1.1 and water inlet 2.4 on mixing chamber 2.3, sodium carbonate and water are added in left mixing chamber 2.2, is stirring
It is sufficiently stirred under the action of device and soda ash solution is made, monoxone and water are added in right mixing chamber 2.3, in the work of agitating device
Monoxone saturated solution is made with lower stirring, horizontal baffle 3.1 is set in reative cell 3, and horizontal baffle 3.1 divides reative cell 3
It is divided into reaction and lower reative cell 3.3, the sodium carbonate liquor and monoxone that left mixing chamber 2.2 and right mixing chamber 2.3 are mixed to get
Solution is delivered in reative cell 3.2, and sodium chloroacetate solution is made after placing response in upper reative cell 3.2, then will be upper anti-
It answers sodium chloroacetate solution made of room 3.2 to be delivered in lower reative cell 3.3, and is added by dosing mouth in reative cell 3.3 downwards
Trimethylamine, placing response obtain glycine betaine and sodium-chloride water solution, are then sent to the processing of distillery 4.Not office in the present embodiment
Be limited to be made glycine betaine using sodium carbonate, monoxone and trimethylamine, those skilled in the art can according to other raw materials and
Reaction process designs the mixing chamber 2 and reative cell 3 of the different numbers met the requirements.
In the present embodiment, it is preferred that left mixing chamber 2.2, right mixing chamber 2.3, upper reative cell 3.2 and lower reative cell 3.3 are equal
It is connected with hot-water cavity 4.3 and cold water cavity 5.3 by connecting tube 6, mixing chamber 2, reative cell 3, distillery 4, cooling channel 5 and liter
It is both provided with temperature inductor 8 in warm channel 4, automatic control is both provided in interface channel 2.6, tapping channel 3.4 and connecting tube 6
Valve 9 processed.When the temperature of left mixing chamber 2.2, right mixing chamber 2.3, upper reative cell 3.2 or lower reative cell 3.3 is relatively low or higher and needs
When adding water, hot water or hot water adjusting can be added to corresponding mixing chamber 2 or reative cell 3 by hot-water cavity 4.3 or cold water cavity 5.3
Temperature, when the temperature of left mixing chamber 2.2, right mixing chamber 2.3, upper reative cell 3.2 or lower reative cell 3.3 is relatively low or higher but is not required to
When adding water, corresponding heating mouth 4.1 or cooling mouth 5.1 are opened by device for opening, to logical by heating channel 4 or cooling
Road 5 cools down to it.Temperature inductor 8 detects the temperature of each mixing chamber 2 and reative cell 3, and the temperature of detection is delivered to
Controller, controller control corresponding opening mechanism 7 and are opened and closed, to the temperature in each mixing chamber 2 and reative cell 3
Degree is adjusted.
Above certain exemplary embodiments that the utility model is only described by way of explanation, undoubtedly, for
Those skilled in the art can be with a variety of different without departing from the spirit and scope of the utility model
Mode is modified described embodiment.Therefore, above-mentioned attached drawing and description are regarded as illustrative in nature, and should not be construed as
Limitation to the utility model claims protection domain.
Claims (9)
1. a kind of glycine betaine production column reactor, which is characterized in that including
Cylindrical body is provided at least one feed inlet and at least one discharge port in the cylindrical body, and the feed inlet is set
It sets at the top of the cylindrical body, the discharge port is arranged in the bottom of the cylindrical body；
Mixing chamber, the mixing chamber are arranged inside the cylindrical body, and the mixing chamber is connected with the feed inlet, described
The side wall of mixing chamber is additionally provided with water inlet, and mixing component is provided in the mixing chamber；
Reative cell, the reative cell are arranged in the inside of the cylindrical body and positioned at the lower section of the mixing chamber, the reaction
The upper end of room is connected by interface channel with the mixing chamber, and the side wall of the reative cell is provided with dosing mouth；
Distillery, the distillery setting by tapping channel are connected positioned at the lower section of the mixing chamber and with the mixing chamber
It is logical, multiple heating tubes are provided in the distillery, multiple heating tubes are vertically arranged, and are formed between each heating tube
The upper end side wall of fluid course, the distillery is provided with hot water outlet；
Temperature control channel, the temperature control channel are arranged in the cylindrical body madial wall and the mixing chamber, reative cell
Between the side wall of distillery, the temperature control channel includes heating channel and cool down channel, the mixing chamber and reative cell
Side wall be both provided with heating mouth and cooling mouth, the heating mouth is connected with the heating channel, the cooling mouth with it is described
Cooling channel is connected, and opening mechanism is both provided on the heating mouth and cooling mouth.
2. glycine betaine production column reactor according to claim 1, which is characterized in that the heating channel includes heat
Water cavity and heating chamber, the hot-water cavity are arranged between the madial wall and the lateral wall of the distillation chamber of the cylindrical body, institute
It states hot-water cavity with hot water outlet to be connected, the hot-water cavity is connected with the mixing chamber and reative cell respectively by connecting tube.
3. glycine betaine production column reactor according to claim 2, which is characterized in that the heating chamber is arranged in institute
It states between the madial wall of cylindrical body and the mixing chamber and the madial wall of reative cell, heating dress is provided in the heating chamber
It sets, the mixing chamber and reative cell are connected by the heating mouth with the heating chamber.
4. glycine betaine production column reactor according to claim 2, which is characterized in that the cooling channel includes cold
Water cavity and cooling chamber, the cold water cavity are arranged between the madial wall and the lateral wall of the distillation chamber of the cylindrical body, institute
Cold water cavity is stated with the hot-water cavity to be connected by connecting tube, the cold water cavity by the connecting tube respectively with the mixing chamber
It is connected with reative cell.
5. glycine betaine production column reactor according to claim 4, which is characterized in that the cold water cavity is arranged in institute
It states between the madial wall of cylindrical body and the mixing chamber and the madial wall of reative cell, cooling dress is provided in the cold water cavity
It sets, the mixing chamber and reative cell are connected by the cooling mouth with the cold water cavity.
6. glycine betaine production column reactor according to claim 2, which is characterized in that be provided in the mixing chamber
The mixing chamber is separated into left mixing chamber and right mixing chamber by vertical clapboard, the vertical clapboard, and the left mixing chamber and the right side are mixed
It closes and is both provided with the feed inlet, water inlet, cooling mouth and heating mouth on room.
7. glycine betaine production column reactor according to claim 6, which is characterized in that be provided in the reative cell
The reative cell is divided into upper reative cell and lower reative cell by horizontal baffle, the horizontal baffle, the upper reative cell and lower anti-
It answers and is connected between room, dosing mouth, cooling mouth and heating mouth are both provided on the upper reative cell and lower reative cell.
8. glycine betaine production column reactor according to claim 7, which is characterized in that the left mixing chamber, the right side are mixed
Room, upper reative cell and lower reative cell is closed to be connected with the hot-water cavity and cold water cavity by the connecting tube.
9. glycine betaine production column reactor according to claim 2, which is characterized in that the mixing chamber, reative cell,
It is both provided with temperature inductor in distillery, cooling channel and heating channel, in the interface channel, tapping channel and connecting tube
It is both provided with autocontrol valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721864521.7U CN208032536U (en) | 2017-12-27 | 2017-12-27 | Glycine betaine production column reactor |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721864521.7U CN208032536U (en) | 2017-12-27 | 2017-12-27 | Glycine betaine production column reactor |
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| CN208032536U true CN208032536U (en) | 2018-11-02 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113893566A (en) * | 2021-10-20 | 2022-01-07 | 杭州三隆新材料有限公司 | Preparation system and purification method of neopentyl glycol copolymer |
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2017
- 2017-12-27 CN CN201721864521.7U patent/CN208032536U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113893566A (en) * | 2021-10-20 | 2022-01-07 | 杭州三隆新材料有限公司 | Preparation system and purification method of neopentyl glycol copolymer |
| CN113893566B (en) * | 2021-10-20 | 2023-01-06 | 杭州三隆新材料有限公司 | Preparation system and purification method of neopentyl glycol copolymer |
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