CN206642691U - A kind of process units of fatty acid acylamino acid surfactant - Google Patents

A kind of process units of fatty acid acylamino acid surfactant Download PDF

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Publication number
CN206642691U
CN206642691U CN201720209912.9U CN201720209912U CN206642691U CN 206642691 U CN206642691 U CN 206642691U CN 201720209912 U CN201720209912 U CN 201720209912U CN 206642691 U CN206642691 U CN 206642691U
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China
Prior art keywords
storage tank
pump
solid content
road
branch pipe
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Expired - Fee Related
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CN201720209912.9U
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Chinese (zh)
Inventor
曾小君
严宇
杨高文
付任重
吴晓发
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Changshu Institute of Technology
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Changshu Institute of Technology
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Abstract

A kind of process units of fatty acid acylamino acid surfactant, belong to the process units technical field of surfactant.Including continuous feeding device, reaction unit, solid content adjusting means and storage device, described continuous feeding device is fed respectively by feed pump into reaction unit from three raw material storage tanks, a water storage tank;Described reaction unit is composed in series respectively by circulating pump and pipeline by three stirred autoclaves;Described solid content adjusting means is that the material after reacted device reaction enters in regulation kettle, and regulation of the water into solid content is added into regulation kettle by feed pump from water storage tank;Described storage device is to store the product obtained by solid content adjusting means.It is simple in construction, with short production cycle, production cost is low, can operate continuously, and considerably reduce labour input quantity, improve production efficiency, extend the time between overhauls(TBO), be applicable to the requirement of industrial amplification production.

Description

A kind of process units of fatty acid acylamino acid surfactant
Technical field
The utility model belongs to the process units technical field of surfactant, and in particular to a kind of fatty acyl group amino The process units of acid surfaces activating agent.
Background technology
The surfactant of " industrial monosodium glutamate " is described as, due to a variety of good performances, obtaining in the industrial production Extensive use.Development with Green Chemistry and the attention to chemical producting safety, with come from natural reproducible raw material prepare Surfactant prepared by surfactant substitution petroleum-based feedstock turns into a kind of trend.By natural acid and it is natural or Industrially prepared amino acid be Material synthesis fatty acid acylamino acid class surfactant, due to good water solubility, The performance such as excellent emulsification and soil release performance, good foaming foam stability, makes it obtained extensively in daily use chemicals, food and medicine and other fields General application.
At present, a variety of fatty acid acylamino acid surfactants have industrialized, preparation of industrialization fatty acid acylamino acid The process units of surfactant, be typically made up of multiple conventional reactors, regulation kettle, configuration kettle etc., this process units its The annexation not being mutually communicated between all kinds of kettles, i.e., actual production operation is intermittently operated, production cycle length, work be present Sequence is complicated, labour's input quantity is more, low production efficiency, the short time between overhauls(TBO) the problems such as.
In view of above-mentioned prior art, it is necessary to the structure of the process units of existing fatty acid acylamino acid surfactant Reasonably improved.Therefore, the applicant has made actively effectively to explore, technology described below is formd finally Scheme.
The content of the invention
The purpose of this utility model be to provide for one kind can operate continuously, be simple in construction, be with short production cycle, production cost it is low Fatty acid acylamino acid class surfactant process units.
The purpose of this utility model is such to what is reached, a kind of production dress of fatty acid acylamino acid class surfactant Put, it is characterised in that:Including continuous feeding device, reaction unit, solid content adjusting means and storage device, described continuously enters Expect that device is fed respectively by feed pump into reaction unit from three raw material storage tanks, a water storage tank;Described reaction dress Put is composed in series respectively by circulating pump and pipeline by three stirred autoclaves;Described solid content adjusting means is reacted Material after device reaction enters in regulation kettle, and adds water into regulation kettle by feed pump from water storage tank and enter solid content Regulation;Described storage device is to store the product obtained by solid content adjusting means.
In a specific embodiment of the present utility model, three raw material storage tanks in the continuous feeding device include For contain the first raw material storage tank of fatty acid chloride, the second raw material storage tank for containing glycine, glutamic acid or methyl amimoacetic acid, For containing the 3rd raw material storage tank of liquid caustic soda;Three stirred autoclaves in the reaction unit include the first stirred autoclave, Second stirred autoclave and the 3rd stirred autoclave;Described solid content adjusting means includes at least one solid content regulation kettle; Described storage device includes at least one product storage tank.
In another specific embodiment of the present utility model, the first described raw material storage tank is connected to first by the road Feedstock pump intake, the first described feedstock pump discharge are connected to the first described stirred autoclave through the first branch pipe, The second described raw material storage tank is connected to the second feedstock pump intake by the road, and the second described feedstock pump discharge is through Two branch pipes are connected to the first described stirred autoclave, and the 3rd described raw material storage tank is connected to the 3rd feedstock pump by the road Entrance, the 3rd described feedstock pump are connected to the first described stirred autoclave, described water storage tank warp through the 3rd branch pipe Pipeline is connected to the 4th charging pump intake, and the described the 4th charging pump discharge is connected to the first described stirring instead through the 4th branch pipe Answer kettle.
In another specific embodiment of the present utility model, the first described stirred autoclave is connected to by the road One pump entry, described first circulation pump discharge are connected to the second described stirred autoclave by the road, and described second Stirred autoclave is connected to second circulation pump intake by the road, and described second circulation pump discharge is connected to described the by the road Three stirred autoclaves, the 3rd described stirred autoclave are connected to the 3rd pump entry, the 3rd described circulating pump by the road Outlet is connected to described solid content regulation kettle by the road, and described water storage tank is connected to the 5th charging pump intake, institute by the road The 5th charging pump discharge stated is connected to described solid content through the 5th branch pipe and adjusts kettle.
In an of the present utility model and then specific embodiment, the first described branch pipe, the second branch pipe, the 3rd First flow control valve, second flow control valve, the 3rd flow control valve are respectively arranged with pipe, the 4th branch pipe and the 5th branch pipe With the 4th flow control valve and the 5th flow control valve.
Of the present utility model more and in a specific embodiment, described solid content regulation kettle is connected to the by the road Four pump entries, the 4th described circulating-pump outlet are connected to described product storage tank by the road.
The utility model is due to using after said structure, having the advantage that:Simple in construction, with short production cycle, production Cost is low, can operate continuously, and considerably reduces the quantity of labour's input, improves production efficiency, extends maintenance week Phase, it is applicable to the requirement of industrial amplification production.By the device, qualified product can be obtained, and multiple types can be produced The amino acid surfactant product of type.
Brief description of the drawings
Fig. 1 is the structural representation of the embodiment of the utility model one.
In figure:1. the first raw material storage tank;2. the second raw material storage tank;3. the 3rd raw material storage tank;4. water storage tank;5. the first raw material Feed pump;6. the second feedstock pump;7. the 3rd feedstock pump;8. the 4th feed pump;9. the 5th feed pump;It is 10. first-class Control valve;11. second flow control valve;12. the 3rd flow control valve;13. the 4th flow control valve;14. the 5th stream Control valve;15. the first branch pipe;16. the second branch pipe;17. the 3rd branch pipe;18. the 4th branch pipe;19. the 5th branch pipe;20. first Stirred autoclave;21. the second stirred autoclave;22. the 3rd stirred autoclave;23. first circulation pump;24. second circulation pump; 25. the 3rd circulating pump;26. solid content adjusts kettle;27. the 4th circulating pump;28. product storage tank.
Embodiment
The utility model is further described below below in conjunction with the accompanying drawings.
Referring to Fig. 1, a kind of process units of fatty acid acylamino acid class surfactant is the utility model is related to, including Continuous feeding device, reaction unit, solid content adjusting means and storage device, described continuous feeding device are by three raw materials Storage tank, a water storage tank are fed by feed pump into reaction unit respectively;Described reaction unit is by three stirring reactions Kettle is composed in series by circulating pump and pipeline respectively;Described solid content adjusting means is that the material after reacted device reaction enters Enter to adjust in kettle, and regulation of the water into solid content is added into regulation kettle by feed pump from water storage tank;Described storage dress Put is to store the product obtained by solid content adjusting means.
Specifically, three raw material storage tanks in the continuous feeding device include being used for the first original for containing fatty acid chloride Material storage tank 1, the second raw material storage tank 2 for containing the amino acid such as glycine, glutamic acid or methyl amimoacetic acid, for contain liquid caustic soda the Three raw material storage tanks 3;Three stirred autoclaves in the reaction unit include the first stirred autoclave 20, the second stirred autoclave 21 and the 3rd stirred autoclave 22, three stirred autoclaves be used to continuously prepare fatty acid acylamino acid class surfactant.
Wherein, the first raw material storage tank 1 is connected to the entrance of the first feedstock pump 5 by the road, and the first feedstock pump 5 exports The first stirred autoclave 20 is connected to through the first branch pipe 15, first flow control valve 10 is provided with the first branch pipe 15;Second is former Material storage tank 2 is connected to the entrance of the second feedstock pump 6 by the road, and the second feedstock pump 6 exports to be connected to through the second branch pipe 16 First stirred autoclave 20, second flow control valve 11 is provided with the second branch pipe 16;3rd raw material storage tank 3 is connected to by the road The entrance of 3rd feedstock pump 7, the 3rd feedstock pump 7 exports is connected to the first stirred autoclave 20 through the 3rd branch pipe 17, 3rd branch pipe 17 is provided with the 3rd flow control valve 12;Water storage tank 4 is connected to the entrance of feed pump 8, the outlet of feed pump 8 warp by the road 4th branch pipe 18 is connected to the first stirred autoclave 20, and the 4th flow control valve 13 is provided with the 4th branch pipe 18.
First stirred autoclave 20 is connected to the entrance of first circulation pump 23 by the road, and first circulation pump 23 exports to be connected by the road The second stirred autoclave 21 is connected to, the second stirred autoclave 21 is connected to the entrance of second circulation pump 24, second circulation pump by the road 24 outlets are connected to the 3rd stirred autoclave 22 by the road.
In order to obtain different solid content products, described solid content adjusting means includes at least one solid content regulation kettle 26, described solid content regulation kettle 26 is used to adjust product solid content, and the 3rd stirred autoclave 22 is connected to the 3rd and followed by the road The entrance of ring pump 25, the 3rd circulating pump 25 exports is connected to solid content regulation kettle 26 by the road, and water storage tank 4 is connected to the 5th by the road The entrance of feed pump 9, the 5th feed pump 9 exports is connected to solid content regulation kettle 26 through the 5th branch pipe 19, is set on the 5th branch pipe 19 There is the 5th flow control valve 14.
In order to store product, described storage device includes at least one product storage tank 28, and solid content adjusts kettle 26 through pipe Road is connected to the entrance of the 4th circulating pump 27, and the 4th circulating pump 27 exports is connected to product storage tank 28 by the road.
Above embodiment is only that preferred embodiment of the present utility model is described, not to of the present utility model Scope is defined, and under the premise of not departing from and the utility model is related to spirit, those of ordinary skill in the art are to the utility model The various modifications and improvement that technical scheme is made, the protection domain that claims of the present utility model determine all should be fallen into.

Claims (7)

  1. A kind of 1. process units of fatty acid acylamino acid surfactant, it is characterised in that:Including continuous feeding device, reaction Device, solid content adjusting means and storage device, described continuous feeding device are by three raw material storage tanks, a water storage tank point Do not fed by feed pump into reaction unit;Described reaction unit be by three stirred autoclaves respectively by circulating pump and Pipeline is composed in series;Described solid content adjusting means is that the material after reacted device reaction enters in regulation kettle, and by water Storage tank adds the regulation that water enters solid content by feed pump into regulation kettle;Described storage device is will to be adjusted by solid content The product that device obtains stores.
  2. A kind of 2. process units of fatty acid acylamino acid surfactant according to claim 1, it is characterised in that institute Stating three in continuous feeding device raw material storage tanks includes being used to contain the first raw material storage tank (1) of fatty acid chloride, for containing Fill the second raw material storage tank (2), the 3rd raw material storage tank (3) for containing liquid caustic soda of glycine, glutamic acid or methyl amimoacetic acid;It is described anti- Three stirred autoclaves in device are answered to include the first stirred autoclave (20), the second stirred autoclave (21) and the 3rd stirring anti- Answer kettle (22);Described solid content adjusting means includes at least one solid content regulation kettle (26);Described storage device includes At least one product storage tank (28).
  3. A kind of 3. process units of fatty acid acylamino acid surfactant according to claim 2, it is characterised in that institute The first raw material storage tank (1) stated is connected to first feedstock pump (5) entrance, the first described feedstock pump (5) by the road Outlet is connected to described the first stirred autoclave (20) through the first branch pipe (15), and described the second raw material storage tank (2) is by the road Second feedstock pump (6) entrance is connected to, the second described feedstock pump (6) outlet is connected to institute through the second branch pipe (16) The first stirred autoclave (20) stated, the 3rd described raw material storage tank (3) are connected to the 3rd feedstock pump (7) and entered by the road Mouthful, the 3rd described feedstock pump (7) is connected to described the first stirred autoclave (20) through the 3rd branch pipe (17), described Water storage tank (4) is connected to the 4th feed pump (8) entrance by the road, and the 4th described feed pump (8) is exported through the 4th branch pipe (18) It is connected to described the first stirred autoclave (20).
  4. A kind of 4. process units of fatty acid acylamino acid surfactant according to claim 2, it is characterised in that institute The first stirred autoclave (20) stated is connected to first circulation pump (23) entrance, the outlet of described first circulation pump (23) by the road Described the second stirred autoclave (21) is connected to by the road, and described the second stirred autoclave (21) is connected to second by the road Circulating pump (24) entrance, the outlet of described second circulation pump (24) are connected to the 3rd described stirred autoclave (22) by the road, The 3rd described stirred autoclave (22) is connected to the 3rd circulating pump (25) entrance by the road, and the 3rd described circulating pump (25) goes out Mouth is connected to described solid content regulation kettle (26) by the road, and described water storage tank (4) is connected to the 5th feed pump (9) by the road Entrance, the 5th described feed pump (9) outlet are connected to described solid content through the 5th branch pipe (19) and adjust kettle (26).
  5. A kind of 5. process units of fatty acid acylamino acid surfactant according to claim 3, it is characterised in that institute The first branch pipe (15) for stating, the second branch pipe (16), the 3rd branch pipe (17), first flow control is respectively arranged with the 4th branch pipe (18) Valve (10), second flow control valve (11), the 3rd flow control valve (12) and the 4th flow control valve (13) processed.
  6. A kind of 6. process units of fatty acid acylamino acid surfactant according to claim 4, it is characterised in that institute The 5th flow control valve (14) is provided with the 5th branch pipe (19) stated.
  7. A kind of 7. process units of fatty acid acylamino acid surfactant according to claim 2, it is characterised in that institute The solid content regulation kettle (26) stated is connected to the 4th circulating pump (27) entrance, the 4th described circulating pump (27) outlet warp by the road Pipeline is connected to described product storage tank (28).
CN201720209912.9U 2017-03-06 2017-03-06 A kind of process units of fatty acid acylamino acid surfactant Expired - Fee Related CN206642691U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108993355A (en) * 2018-07-13 2018-12-14 广州泰道安医疗科技有限公司 A kind of system producing stable antiseptic solution

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108993355A (en) * 2018-07-13 2018-12-14 广州泰道安医疗科技有限公司 A kind of system producing stable antiseptic solution
CN108993355B (en) * 2018-07-13 2021-02-19 广州泰道安医疗科技有限公司 System for producing stable sterilization and disinfection solution

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Granted publication date: 20171117

Termination date: 20210306