CN207950748U - Epoxychloropropane chromatographs tank and epoxychloropropane tomographic system - Google Patents
Epoxychloropropane chromatographs tank and epoxychloropropane tomographic system Download PDFInfo
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- CN207950748U CN207950748U CN201721825086.7U CN201721825086U CN207950748U CN 207950748 U CN207950748 U CN 207950748U CN 201721825086 U CN201721825086 U CN 201721825086U CN 207950748 U CN207950748 U CN 207950748U
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- epoxychloropropane
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- chromatography
- deflector
- chromatographs
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Abstract
The utility model is related to commercial plant technical fields, and in particular to a kind of epoxychloropropane chromatography tank and epoxychloropropane tomographic system.The epoxychloropropane chromatographs tank, including chromatography tank body, and chromatography tank body opens up epoxychloropropane aqueous solution feed pipe, and chromatography tank interior is obliquely installed deflector, and deflector is equipped with baffle, and deflector lower part is equipped with baffle, and baffle is arranged for vertical direction；Epoxychloropropane tomographic system includes epoxychloropropane chromatography tank, storage of waste water tank, epoxychloropropane crude product holding vessel, wherein epoxychloropropane chromatography tank is respectively connected with storage of waste water tank, epoxychloropropane crude product holding vessel.The utility model improves separating effect, reduces the loss of epoxychloropropane crude product, reduces operation difficulty, reduces control error.The utility model is easy to operate, saves resource, improves work efficiency, time saving and energy saving.
Description
Technical field
The utility model is related to commercial plant technical fields, and in particular to a kind of epoxychloropropane chromatography tank and epoxy chloropropionate
Alkane tomographic system.
Background technology
Currently, the processing method of epoxychloropropane aqueous solution is that epoxychloropropane aqueous solution is directly added into chromatography tank,
It is voluntarily detached, lower layer's epoxychloropropane is controlled by regulating valve and produced, and Interface Control is adjusted by level meters registration, is grasped
The extraction by observing interface meter registration control epoxychloropropane crude product is needed as personnel.This method has a defect that chromatography tank
Level fluctuation is big, easily leads to level meters registration and beats repeatedly, and operation is relatively difficult, and dcs control difficulty is big, and
And waste water is detached with epoxychloropropane crude product and is not thorough, and causes the loss of epoxychloropropane crude product big.
Therefore, in order to solve problem above, it is a kind of easy to operate that there is an urgent need for research and development, the epoxychloropropane chromatography of good separating effect
Tank and epoxychloropropane tomographic system.
Utility model content
The purpose of this utility model is to provide a kind of easy to operate, the good epoxychloropropane chromatography tank of chromatographic effect, this reality
With novel while providing epoxychloropropane tomographic system.
The technical solution adopted by the utility model to solve its technical problems is that：
Epoxychloropropane described in the utility model chromatographs tank, including chromatography tank body, and chromatography tank body opens up epoxychloropropane
Aqueous solution feed pipe, chromatography tank interior are obliquely installed deflector, and deflector lower part is equipped with baffle, and baffle sets for vertical direction
It sets.
Wherein：
The deflector tilts down setting, and the angle with horizontal plane is 20-40 °, and the number of plies of deflector is 3-4 layers,
The quantity of every layer of deflector overhead gage is 2-3；Deflector side is fixed on the side wall of chromatography tank interior, and deflector is another
Side extend to chromatography tank body inside, adjacent two layers deflector downwardly-inclined direction on the contrary, adjacent two layers deflector extension
Line has intersection point.
On the basis of chromatographing top of the tank, epoxychloropropane aqueous solution feed pipe is located at 3/7ths of chromatography tank body height
Place.
Distributor is set on the epoxychloropropane aqueous solution feed pipe.
Level meters are equipped on the outside of the chromatography tank body, level meters one end is connect with chromatography tank body top, and the other end passes through ball
Valve is connect with chromatography tank base.
Epoxychloropropane tomographic system described in the utility model, including epoxychloropropane chromatography tank, storage of waste water tank, ring
Oxygen chloropropane crude product holding vessel, epoxychloropropane chromatography tank are respectively connected with storage of waste water tank, epoxychloropropane crude product holding vessel.
Wherein：
The epoxychloropropane chromatography tank is connected with epoxychloropropane crude product holding vessel by inverted U bend pipe, inverted U bend pipe
Upper setting barometric pipe, barometric pipe are also connected with epoxychloropropane chromatography tank.
Preferably, the epoxychloropropane chromatography pot bottom passes through inverted U bend pipe phase with epoxychloropropane crude product holding vessel
Even, barometric pipe is also connected with epoxychloropropane chromatography tank top.
The top that the storage of waste water tank chromatographs tank with epoxychloropropane is connect.
The beneficial effects of the utility model are as follows：
The utility model is equipped with deflector in chromatography tank body, and deflector is equipped with baffle, and the setting of baffle, which increases, to rub
Power is wiped, is conducive to the cyclic oxygen chloropropane phase of epoxychloropropane aqueous solution chromatography and water phase, improves epoxychloropropane aqueous solution
Chromatographic effect reduces the residual quantity of epoxychloropropane in waste water, is conducive to the separation of epoxychloropropane and waste water；This practicality is new
Inverted U bend pipe is equipped in the epoxychloropropane tomographic system of type, inverted U bend pipe utilizes the density of epoxychloropropane phase and water phase
Difference, control epoxychloropropane crude product voluntarily produce, improve separating effect, reduce the loss of epoxychloropropane crude product, reduce
Operation difficulty, reduces control error.The utility model is easy to operate, saves resource, improves work efficiency, time saving province
Power.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model；
In figure：1, storage of waste water tank；2, epoxychloropropane aqueous solution feed pipe；3, tank body is chromatographed；4, deflector；5, it is distributed
Device；6, level meters；7, barometric pipe；8, inverted U bend pipe；9, epoxychloropropane crude product holding vessel；10, ball valve；11, baffle.
Specific implementation mode
The utility model is described further with reference to embodiments.
Embodiment 1
As shown in Figure 1, epoxychloropropane described in the utility model chromatographs tank, including chromatography tank body 3, chromatography tank body 3 is opened
If epoxychloropropane aqueous solution feed pipe 2, deflector 4 is arranged in chromatography 3 inner inclination of tank body, and 4 lower part of deflector is equipped with baffle 11,
Baffle 11 is arranged for vertical direction.
Wherein：
The deflector 4 tilts down setting, and the angle with horizontal plane is 30 °, and the number of plies of deflector 4 is 4 layers, every layer
The quantity of 4 overhead gage 11 of deflector is 3；4 side of deflector is fixed on the side wall inside chromatography tank body 3, and deflector 4 is another
Side extends to the inside of chromatography tank body 3, and 4 downwardly-inclined direction of adjacent two layers deflector is on the contrary, adjacent two layers deflector 4 prolongs
Long line has intersection point.
On the basis of chromatographing 3 top of tank body, epoxychloropropane aqueous solution feed pipe 2 is located at seven points of chromatography 3 height of tank body
Three at.
Distributor 5 is set on the epoxychloropropane aqueous solution feed pipe 2.
3 outside of the chromatography tank body is equipped with level meters 6, and 6 one end of level meters is connect with 3 top of chromatography tank body, and the other end is logical
Ball valve 10 is crossed to connect with 3 bottom of chromatography tank body.
Epoxychloropropane tomographic system described in the utility model, as shown in Figure 1, including epoxychloropropane chromatography tank, giving up
Water store tank 1, epoxychloropropane crude product holding vessel 9, wherein epoxychloropropane chromatographs tank and storage of waste water tank 1, epoxychloropropane
Crude product holding vessel 9 is respectively connected with.
Wherein：
The epoxychloropropane chromatography pot bottom is connected with epoxychloropropane crude product holding vessel 9 by inverted U bend pipe 8, U
Barometric pipe 7 is set on type bend pipe 8, and barometric pipe 7 is also connected with epoxychloropropane chromatography tank top.
The top that the storage of waste water tank 1 chromatographs tank with epoxychloropropane is connect.
The course of work of epoxychloropropane tomographic system described in the utility model is as follows：
Epoxychloropropane aqueous solution enters from epoxychloropropane aqueous solution feed pipe 2 in epoxychloropropane chromatography tank, through dividing
Cloth device 5 is dispersed in epoxychloropropane chromatography tank.Since epoxychloropropane is different from the density of waste water, epoxychloropropane with
Waste water is layered, and upper layer is waste water, and lower layer is epoxychloropropane crude product.Epoxychloropropane chromatographs the deflector 4 in tank and is equipped with gear
The setting of plate 11, baffle 11 increases frictional force, is conducive to the cyclic oxygen chloropropane phase of epoxychloropropane aqueous solution chromatography and water phase,
The top that waste water chromatographs tank from epoxychloropropane enters in storage of waste water tank 1, and epoxychloropropane crude product is chromatographed from epoxychloropropane
The bottom of tank is flowed out, and is entered in epoxychloropropane crude product holding vessel 9 through inverted U bend pipe 8, realizes epoxychloropropane crude product and waste water
Separation.
Embodiment 2
Epoxychloropropane aqueous solution enters epoxychloropropane from epoxychloropropane aqueous solution feed pipe 2 with 5t/h flow velocitys and chromatographs
In tank, it is dispersed in epoxychloropropane chromatography tank through distributor 5, by deflector 4 and baffle 11, realizes epoxychloropropane
Crude product is detached with waste water, and upper layer waste water outflow to storage of waste water tank 1, lower layer's epoxychloropropane crude product is by inverted U bend pipe 8 to overflow
Stream mode produces, into epoxychloropropane crude product holding vessel 9；Waste water and epoxychloropropane crude product is taken to be measured respectively, waste water
COD value be 562mg/L, epoxychloropropane crude product water content 0.90g/L.
Embodiment 3
Epoxychloropropane aqueous solution enters epoxychloropropane from epoxychloropropane aqueous solution feed pipe 2 with 6t/h flow velocitys and chromatographs
In tank, it is dispersed in epoxychloropropane chromatography tank through distributor 5, by deflector 4 and baffle 11, realizes epoxychloropropane
Crude product is detached with waste water, and upper layer waste water outflow to storage of waste water tank 1, lower layer's epoxychloropropane crude product is by inverted U bend pipe 8 to overflow
Stream mode produces, into epoxychloropropane crude product holding vessel 9；Waste water and epoxychloropropane crude product is taken to be measured respectively, waste water
COD value be 573mg/L, epoxychloropropane crude product water content 0.92g/L.
Embodiment 4
Epoxychloropropane aqueous solution enters epoxychloropropane layer with 5.5t/h flow velocitys from epoxychloropropane aqueous solution feed pipe 2
It analyses in tank, is dispersed in epoxychloropropane chromatography tank through distributor 5, by deflector 4 and baffle 11, realizes epoxy chloropropionate
Alkane crude product is detached with waste water, upper layer waste water outflow to storage of waste water tank 1, lower layer's epoxychloropropane crude product by inverted U bend pipe 8 with
Overflow manner produces, into epoxychloropropane crude product holding vessel 9；It takes waste water and epoxychloropropane crude product to be measured respectively, gives up
The COD value of water is 541mg/L, epoxychloropropane crude product water content 0.89g/L.
The content of water is 1.5g/L in epoxychloropropane aqueous solution, and COD value 2000mg/L passes through the layer of the utility model
Analysis system realizes the separation of epoxychloropropane crude product and waste water, and after separation, the COD value of waste water is reduced to 540-580mg/L, epoxy
The content of water is reduced to 0.89-0.93g/L in chloropropane crude product.The utility model is equipped with deflector 4, deflector in chromatographing tank
4 are equipped with baffle 11, and the setting of baffle 11 increases frictional force, are conducive to the cyclic oxygen chloropropane of epoxychloropropane aqueous solution chromatography
Phase and water phase, improve the chromatographic effect of epoxychloropropane aqueous solution, reduce the residual quantity of epoxychloropropane in waste water；This reality
With inverted U bend pipe 8 is additionally provided in novel, inverted U bend pipe 8 controls epoxy chlorine using the density contrast of epoxychloropropane phase and water phase
Propane crude product voluntarily produces, and reduces operation difficulty, reduces control error, reduces the loss of epoxychloropropane crude product.
Claims (9)
1. a kind of epoxychloropropane chromatographs tank, including chromatography tank body（3）, chromatograph tank body（3）Open up epoxychloropropane aqueous solution into
Expects pipe（2）, it is characterised in that：Chromatograph tank body（3）Deflector is arranged in inner inclination（4）, deflector（4）Lower part is equipped with baffle
（11）, baffle（11）It is arranged for vertical direction；
The deflector（4）Setting is tilted down, the angle with horizontal plane is 20-40 °, deflector（4）The number of plies be 3-4
Layer, deflector（4）Side is fixed on chromatography tank body（3）On internal side wall, deflector（4）The other side extends to chromatography tank body
（3）Inside, adjacent two layers deflector（4）Downwardly-inclined direction is on the contrary, adjacent two layers deflector（4）Extended line have friendship
Point.
2. epoxychloropropane according to claim 1 chromatographs tank, it is characterised in that：The baffle（11）Quantity be 2-3
It is a.
3. epoxychloropropane according to claim 1 chromatographs tank, it is characterised in that：To chromatograph tank body（3）On the basis of top,
Epoxychloropropane aqueous solution feed pipe（2）Positioned at chromatography tank body（3）At 3/7ths of height.
4. epoxychloropropane according to claim 1 chromatographs tank, it is characterised in that：The epoxychloropropane aqueous solution charging
Pipe（2）Upper setting distributor（5）.
5. epoxychloropropane according to claim 1 chromatographs tank, it is characterised in that：The chromatography tank body（3）Outside is equipped with
Level meters（6）.
6. epoxychloropropane according to claim 5 chromatographs tank, it is characterised in that：The level meters（6）One end and chromatography
Tank body（3）Top connects, and the other end passes through ball valve（10）With chromatography tank body（3）Bottom connects.
7. a kind of epoxychloropropane tomographic system chromatographing tank using any epoxychloropropane of claim 1-6, special
Sign is：Including epoxychloropropane chromatography tank, storage of waste water tank（1）, epoxychloropropane crude product holding vessel（9）, wherein epoxy chlorine
Propane chromatographs tank and storage of waste water tank（1）, epoxychloropropane crude product holding vessel（9）It is respectively connected with.
8. epoxychloropropane tomographic system according to claim 7, it is characterised in that：Epoxychloropropane chromatography tank with
Epoxychloropropane crude product holding vessel（9）Pass through inverted U bend pipe（8）It is connected, inverted U bend pipe（8）Upper setting barometric pipe（7）,
Barometric pipe（7）Also it is connected with epoxychloropropane chromatography tank.
9. epoxychloropropane tomographic system according to claim 8, it is characterised in that：The epoxychloropropane chromatographs tank bottom
Portion and epoxychloropropane crude product holding vessel（9）Pass through inverted U bend pipe（8）It is connected, barometric pipe（7）Also with epoxychloropropane layer
Tank top is analysed to be connected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721825086.7U CN207950748U (en) | 2017-12-22 | 2017-12-22 | Epoxychloropropane chromatographs tank and epoxychloropropane tomographic system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721825086.7U CN207950748U (en) | 2017-12-22 | 2017-12-22 | Epoxychloropropane chromatographs tank and epoxychloropropane tomographic system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207950748U true CN207950748U (en) | 2018-10-12 |
Family
ID=63729852
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721825086.7U Active CN207950748U (en) | 2017-12-22 | 2017-12-22 | Epoxychloropropane chromatographs tank and epoxychloropropane tomographic system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207950748U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114942227A (en) * | 2022-07-21 | 2022-08-26 | 东营市俊源石油技术开发有限公司 | Quick detection device of decoloration degree in food level white oil preparation process |
-
2017
- 2017-12-22 CN CN201721825086.7U patent/CN207950748U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114942227A (en) * | 2022-07-21 | 2022-08-26 | 东营市俊源石油技术开发有限公司 | Quick detection device of decoloration degree in food level white oil preparation process |
| CN114942227B (en) * | 2022-07-21 | 2022-10-21 | 东营市俊源石油技术开发有限公司 | Quick detection device of degree of decolorization in food level white oil preparation process |
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|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: No.227, Changguo East Road, chemical industry park, Zhangdian District, Zibo City, Shandong Province Patentee after: Shandong MINJI New Material Technology Co.,Ltd. Address before: 255000 Shandong city of Zibo province Zhangdian two road Hutian Road on the north side of cross East Chemical Industrial Zone Patentee before: SHANDONG MINJI CHEMICAL Co.,Ltd. |