CN207446258U - A kind of kettle equipment of triazole crystallization - Google Patents
A kind of kettle equipment of triazole crystallization Download PDFInfo
- Publication number
- CN207446258U CN207446258U CN201721533882.3U CN201721533882U CN207446258U CN 207446258 U CN207446258 U CN 207446258U CN 201721533882 U CN201721533882 U CN 201721533882U CN 207446258 U CN207446258 U CN 207446258U
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- CN
- China
- Prior art keywords
- autoclave body
- triazole
- kettle
- kettle equipment
- wall
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model is related to a kind of triazole crystallization kettle equipment, comprising：Autoclave body, crown center position are fixed with male flange；Agitating device, it is arranged in autoclave body crown center position and is coaxially fixed on above-mentioned male flange, including being arranged on the driving device of autoclave body top outer, axis connection and stirring shaft, the anchor formula paddle for the stirring shaft one side being disposed far from the top of autoclave body inside autoclave body being exported with driving device；Wall is scraped, be set to one or is spaced apart multiple, is connected setting on the outside of one side and the anchor formula paddle, opposite side contacts setting with autoclave body madial wall.The utility model is simple in structure, Binding can be avoided to generate big ingot on kettle wall and prevent its ingot from blocking outlet.
Description
Technical field
The utility model is related to a kind of crystallizer, more particularly to a kind of kettle equipment of triazole crystallization.
Background technology
At present, there are two types of methods for triazole crystallization.Method one：Material is disposably placed into crystallizing pond and crystallizes, this side
The shortcomings that method is that crystalline solid can form harder ingot, crushes difficulty, substantial amounts of manpower is spent when broken, and is being operated
When be lost it is more, and due to after broken material be in solid-like, it is impossible to the water being wherein mingled with using the drying of full automatic centrifuge
Divide and sundries, production automation degree are low；Method two：It is crystallized in crystallization kettle, product is in a large amount of mother liquors by cold in chuck
But liquid achievees the purpose that crystallisation by cooling with forming heat exchange by chuck wall in material.The shortcomings that being crystallized in crystallization kettle is three
Crystal is easily adhered on kettle wall when nitrogen azoles forms crystal in a large amount of mother liquors, and the cooling water in chuck is just difficult shape with material in kettle
It is very long when causing to crystallize into heat exchange, it is unfavorable for being carried out continuously for production.To improve the deficiency in the second method for crystallising,
Design a kind of kettle equipment suitable for triazole crystallization.
Utility model content
The purpose of the utility model is to overcome defect in the prior art, provide it is a kind of it is simple in structure, can keep away
Exempt from the kettle equipment that Binding generates the triazole crystallization of big ingot on kettle wall.
To achieve the above object, the technical solution of the utility model is to provide a kind of kettle equipment of triazole crystallization, including：
Autoclave body, crown center position are fixed with male flange；
Agitating device is arranged in autoclave body crown center position and is coaxially fixed on above-mentioned male flange, including being arranged on kettle
The driving device of body top outer, the stirring shaft with driving device output axis connection and inside autoclave body are disposed far from kettle
The anchor formula paddle of stirring shaft one side at the top of body；
Wall is scraped, be set to one or is spaced apart multiple, setting, opposite side are connected on the outside of one side and the anchor formula paddle
Setting is contacted with autoclave body madial wall.
It is connected to make to scrape wall with anchor formula paddle, preferred technical solution is that the wall of scraping includes being fixed at anchor formula
Connector on paddle is connected with connector by pin and contact the scraper plate of setting with autoclave body madial wall.
It is engaged in order to avoid scraping when wall is rotated with agitating device with tank skin, preferred technical solution is that the scraper plate is set to
Elastic construction, upper and lower ends of the scraper plate away from autoclave body tank skin one side are respectively equipped with journal stirrup, bar shaped are equipped on the journal stirrup
Hole, one side of the scraper plate away from tank skin are additionally provided with spring mounting hole, spring are equipped in the spring mounting hole.
It is come into full contact with to make to scrape between wall and tank skin, preferred technical solution is that the connector is stirred away from anchor formula
The one side of leaf is equipped with through hole, and the one end of the connector away from anchor formula paddle is equipped with to be arranged in spring and be nested in spring and install
Column in hole；Spring is equipped between the scraper plate and connector, after being installed to avoid agitating device in autoclave body, scrapes wall
It is not bonded with tank skin.
Air is entered in kettle by the gap between driving device and male flange and influences outside kettle during in order to avoid vacuumizing
Material reaction, preferred technical solution, which are that the kettle equipment is further included, to be coaxially fixed on male flange and is arranged by bolt
In the sealing device on stirring shaft.
In order to solve the axial movement of agitating device, damage when avoiding stirring shaft double swerve to driving device is excellent
The technical solution of choosing is that the agitating device bottom is also coaxially provided with Auxiliary support, and the Auxiliary support includes being sheathed on stirring
The installing plate that the axle sleeve of shaft bottom, axle sleeve bottom are also fixed with annulus, are sheathed on axle sleeve and are fixed on annulus upper surface,
The Auxiliary support is fixedly connected by leg with autoclave body, and the sleeve lining, which is equipped with to match somebody with somebody to merge with axle sleeve, is sheathed on stirring shaft
On tetrafluoro set；The tetrafluoro set can to avoid between metal axle sleeve and metal stirring shaft rotate when metal between be engaged, shadow
Ring mixing effect.
In order to reduce leakage face, preferred technical solution is that the driving device includes motor, is connected with motor output shaft
The speed reducer of setting, the rack being connected with deceleration motor spindle, the bottom of the frame mounting surface are set to hollow structure, the rack set
On sealing device and pass through bolt and be connected with male flange.
In order to which the material after being stirred in kettle preferably is delivered to discharging pipeline, preferred technical solution is the autoclave body
Bottom among be equipped with spiral discharge device.
In order to transport material in kettle, measure material temperature in kettle, to being vacuumized in kettle, preferred technical solution
It is that temperature sensor, manhole, pressure vacuum gauge, vacuum orifice, drain, feed inlet, spare is additionally provided at the top of the autoclave body
Mouthful, the temperature sensor, which is taken over to be arranged in autoclave body and pass through connector, to be fixed on autoclave body inner cavity and is contacted with material.
In order to facilitate the situation of material in observation kettle, preferred technical solution is that the manhole is set to opening soon with visor
Formula manhole.
In order to be heated or be cooled down to material in kettle, preferred technical solution, which is that the kettle equipment further includes, to be arranged
Chuck on the outside of autoclave body is respectively equipped with inlet and outlet on the chuck, electrically-controlled valve is equipped in the inlet and outlet.
In order to be evenly heated in kettle material or uniformly cool down, preferred technical solution is that spiral shell is equipped in the chuck
Curl up the spiral deflector on autoclave body outer wall.
Technical solutions of the utility model have the following advantages that：
1. a kind of kettle equipment of triazole crystallization provided by the utility model, equipped with wall is scraped, can avoid Binding in kettle
Big ingot is generated on wall and prevents its ingot from blocking outlet so as to influence the heat of material in cooling water and kettle in chuck
It exchanges；
2. a kind of kettle equipment of triazole crystallization provided by the utility model, the wall of scraping, can be with equipped with spring, bar hole
Scraper plate is made to be slided in the active force of spring, after agitating device is avoided to be installed in autoclave body, wall is scraped and is not bonded with tank skin；
3. a kind of kettle equipment of triazole crystallization provided by the utility model, bottom of the frame mounting surface are set to hollow devices simultaneously
Sealing device is directly fixed on male flange, reduces leakage face；When sealing device is installed on rack lower surface, rack
Endless hermetically sealed generate is revealed between mounting surface and male flange mounting surface.
Description of the drawings
It, below will be right in order to illustrate more clearly of specific embodiment of the present invention or technical solution of the prior art
Specific embodiment or attached drawing needed to be used in the description of the prior art are briefly described, it should be apparent that, it describes below
In attached drawing be the utility model some embodiments, for those of ordinary skill in the art, do not paying creativeness
On the premise of work, other attached drawings are can also be obtained according to these attached drawings.
Fig. 1 is the kettle device structure schematic diagram of the triazole crystallization provided in the utility model embodiment；
Fig. 2 is the explosive view that wall construction is scraped in Fig. 1；
Fig. 3 is the structure diagram of Auxiliary support in Fig. 1.
In figure：1：Autoclave body；2：Agitating device；3：Spiral discharge device；4：Scrape wall；5：Sealing device；6：Auxiliary support；7：
Chuck；1-1：Male flange；1-2：Temperature sensor；2-1：Driving device；2-2：Stirring shaft；2-3：Anchor formula paddle；2-
11：Motor；2-12：Speed reducer；2-13：Rack；4-1：Connector；4-2：Scraper plate；4-3：Pin；4-11：Through hole；4-12：Column；
4-21：Journal stirrup；4-22：Bar hole；4-23：Spring mounting hole；4-24：Spring；6-1：Axle sleeve；6-2：Annulus；6-3：Installing plate；
6-4：Leg；6-5：Tetrafluoro set；7-1：Spiral deflector.
Specific embodiment
The technical solution of the utility model is clearly and completely described below in conjunction with attached drawing, it is clear that described
Embodiment is the utility model part of the embodiment, instead of all the embodiments.Based on the embodiment in the utility model, sheet
Field those of ordinary skill all other embodiments obtained without making creative work, belong to this practicality
Novel protected scope.
As shown in Figure 1 to Figure 3, the kettle equipment of a kind of triazole crystallization provided by the utility model, including：
Autoclave body 1, crown center position are fixed with male flange 1-1；
Agitating device 2 is arranged in 1 crown center position of autoclave body and is coaxially fixed on above-mentioned male flange 1-1, including setting
Driving device 2-1 and driving device 2-1 output axis connections in 1 top outer of autoclave body and the stirring shaft inside autoclave body 1
2-2, the anchor formula paddle 2-3 for the stirring shaft 2-2 one sides being disposed far from the top of autoclave body 1；
Wall 4 is scraped, be set to one or is spaced apart multiple, is connected setting on the outside of one side and the anchor formula paddle 2-3, separately
One side contacts setting with 1 madial wall of autoclave body.
It is connected to make to scrape wall with anchor formula paddle, the preferred scheme of the utility model is that the wall 4 of scraping includes fixing
Connector 4-1 on anchor formula paddle 2-3, set by pin 4-3 and connector 4-1 connections and being contacted with 1 madial wall of autoclave body
The scraper plate 4-2 put.
It is engaged in order to avoid scraping when wall is rotated with agitating device with tank skin, the preferred scheme of the utility model is, described to scrape
Plate 4-2 is set to elastic construction, and upper and lower ends of the scraper plate 4-2 away from 1 tank skin one side of autoclave body are respectively equipped with journal stirrup 4-21, described
Bar hole 4-22 is equipped on journal stirrup 4-21, the one sides of the scraper plate 4-2 away from tank skin is additionally provided with spring mounting hole 4-23, institute
It states and spring 4-24 is equipped in spring mounting hole 4-23.
It is come into full contact with to make to scrape between wall and tank skin, the preferred scheme of the utility model is that the connector 4-1 is separate
The one side of anchor formula paddle 2-3 is equipped with equipped with the one end of through hole 4-11, the connector 4-1 away from anchor formula paddle 2-3 and wears
In spring 4-24 and the column 4-12 that is nested in spring mounting hole 4-23；Spring is equipped between the scraper plate and connector, it can
After being installed to avoid agitating device in autoclave body, scrape wall and be not bonded with tank skin.
Air is entered in kettle by the gap between driving device and male flange and influences outside kettle during in order to avoid vacuumizing
Material reaction, the preferred scheme of the utility model, which are that the kettle equipment is further included, is coaxially fixed on male flange 1-1 by bolt
It goes up and is sheathed on the sealing device 5 on stirring shaft 2-2.
In order to solve the axial movement of agitating device, damage when avoiding stirring shaft double swerve to driving device, this
The preferred scheme of utility model is that 2 bottom of agitating device is also coaxially provided with Auxiliary support 6, and the Auxiliary support 6 includes set
Axle sleeve 6-1, axle sleeve 6-1 bottoms arranged on stirring shaft 2-2 bottoms are also fixed with annulus 6-2, are sheathed on axle sleeve 6-1 simultaneously
The installing plate 6-3 of annulus 6-2 upper surfaces is fixed on, the Auxiliary support 6 is fixedly connected by leg 6-4 with autoclave body 1, the axis
Set 6-1 inner walls are equipped with the tetrafluoro for matching somebody with somebody with axle sleeve 6-1 and merging and being sheathed on stirring shaft 2-2 and cover 6-5；The tetrafluoro set can be kept away
It is engaged when exempting to rotate between metal axle sleeve and metal stirring shaft between metal, influences mixing effect.
In order to reduce leakage face, the preferred scheme of the utility model is, the driving device 2-1 include motor 2-11, with
Speed reducer 2-12, the rack 2-13, the rack 2- being connected with speed reducer 2-12 bottoms that motor 2-11 output axis connections are set
13 bottom mounting surfaces are set to hollow structure, and the rack 2-13 is sheathed on sealing device 5 and passes through bolt and male flange 1-1
Connection.
In order to which the material after being stirred in kettle preferably is delivered to discharging pipeline, the preferred scheme of the utility model is institute
It states and spiral discharge device 3 is equipped among the bottom of autoclave body 1.
In order to transport material in kettle, measure material temperature in kettle, to being vacuumized in kettle, the utility model is preferred
Scheme be, 1 top of the autoclave body be additionally provided with temperature sensor 1-2, manhole, pressure vacuum gauge, vacuum orifice, drain, into
Material mouth, spare mouth, the temperature sensor 1-2, which takes over to be arranged in autoclave body 1 and pass through connector, is fixed on 1 inner cavity of autoclave body and and object
Material contact.
In order to facilitate the situation of material in observation kettle, the preferred scheme of the utility model is that the manhole is set to band visor
Fast open type manhole.
In order to be heated or be cooled down to material in kettle, the preferred scheme of the utility model is that the kettle equipment is also wrapped
The chuck 7 for being sheathed on 1 outside of autoclave body is included, inlet and outlet is respectively equipped on the chuck 7, electrically-controlled valve is equipped in the inlet and outlet.
In order to be evenly heated in kettle material or uniformly cool down, the preferred scheme of the utility model is, in the chuck 7
The spiral deflector 7-1 on 1 outer wall of autoclave body is arranged on equipped with spiral winding.
It is pressed from both sides for the work for controlling agitating device and by temperature sensor feedback temperature signal to controller so as to control
The electrically-controlled valve selection of set inlet and outlet is heated or cooled down to material in kettle, and the preferred scheme of the utility model is described three
The kettle equipment of nitrogen azoles crystallization further includes controller, the controller respectively with driving device 2-1, temperature sensor 1-2, vacuum pressure
Power table, electrically-controlled valve are electrically connected.
Example is only intended to clearly illustrate, and is not intended to limit the embodiments.For the general of fields
For logical technical staff, other different forms of changes or modifications may be made based on the above description.Here need not
Also all embodiments can not be exhaustive.And the obvious changes or variations thus extended out is still in this reality
Among protection domain with new creation.
Claims (10)
1. a kind of kettle equipment of triazole crystallization, which is characterized in that including：
Autoclave body (1), crown center position are fixed with male flange (1-1)；
Agitating device (2) is arranged in autoclave body (1) crown center position and is coaxially fixed on above-mentioned male flange (1-1), including
Driving device (2-1) and driving device (2-1) arranged on autoclave body (1) top outer export axis connection and arranged on autoclave body (1) inside
Stirring shaft (2-2), the anchor formula paddle (2-3) of stirring shaft (2-2) one side being disposed far from the top of autoclave body (1)；
Wall (4) is scraped, be set to one or is spaced apart multiple, is connected setting on the outside of one side and the anchor formula paddle (2-3), separately
One side contacts setting with autoclave body (1) madial wall.
2. the kettle equipment of triazole crystallization according to claim 1, which is characterized in that the wall (4) of scraping includes fixed set
In on anchor formula paddle (2-3) connector (4-1), be connected with connector (4-1) by pin (4-3) and on the inside of autoclave body (1)
The scraper plate (4-2) that wall contact is set.
3. the kettle equipment of triazole crystallization according to claim 2, which is characterized in that the scraper plate (4-2) is set to elasticity
Structure, upper and lower ends of the scraper plate (4-2) away from autoclave body (1) tank skin one side are respectively equipped with journal stirrup (4-21), the journal stirrup (4-
21) bar hole (4-22) is equipped on, one side of the scraper plate (4-2) away from tank skin is additionally provided with spring mounting hole (4-23), institute
It states and spring (4-24) is equipped in spring mounting hole (4-23).
4. the kettle equipment of triazole crystallization according to claim 2, which is characterized in that the connector (4-1) is away from anchor
The one side of formula paddle (2-3) is equipped with through hole (4-11), and the one end of the connector (4-1) away from anchor formula paddle (2-3) is set
There is the column (4-12) for being arranged in spring (4-24) and being nested in spring mounting hole (4-23).
5. the kettle equipment of triazole crystallization according to claim 1, which is characterized in that the kettle equipment, which further includes, passes through spiral shell
Bolt is coaxially fixed on male flange (1-1) and is sheathed on the sealing device (5) on stirring shaft (2-2).
6. the kettle equipment of triazole crystallization according to claim 1, which is characterized in that agitating device (2) bottom is also
Auxiliary support (6) is coaxially provided with, the Auxiliary support (6) includes being sheathed on the axle sleeve (6-1), axis of stirring shaft (2-2) bottom
The installation that set (6-1) bottom is also fixed with annulus (6-2), is sheathed on axle sleeve (6-1) and is fixed on annulus (6-2) upper surface
Plate (6-3), the Auxiliary support (6) are fixedly connected by leg (6-4) with autoclave body (1), axle sleeve (6-1) inner wall be equipped with
Axle sleeve (6-1) is sheathed on the tetrafluoro set (6-5) on stirring shaft (2-2) with merging.
7. the kettle equipment of triazole crystallization according to claim 1, which is characterized in that the driving device (2-1) includes
Motor (2-11) is connected with the speed reducer (2-12) of motor (2-11) output axis connection setting, with speed reducer (2-12) bottom
Rack (2-13), rack (2-13) bottom mounting surfaces are set to hollow structure, and the rack (2-13) is sheathed on sealing device
(5) on and pass through bolt and be connected with male flange (1-1).
8. the kettle equipment of triazole crystallization according to claim 1, which is characterized in that among the bottom of the autoclave body (1)
Equipped with spiral discharge device (3).
9. the kettle equipment of triazole crystallization according to claim 1, which is characterized in that further include and be sheathed on autoclave body (1) outside
The chuck (7) of side is respectively equipped with inlet and outlet on the chuck (7), electrically-controlled valve is equipped in the inlet and outlet.
10. the kettle equipment of triazole crystallization according to claim 9, which is characterized in that spiral is equipped in the chuck (7)
The spiral deflector (7-1) being set around on autoclave body (1) outer wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721533882.3U CN207446258U (en) | 2017-11-16 | 2017-11-16 | A kind of kettle equipment of triazole crystallization |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721533882.3U CN207446258U (en) | 2017-11-16 | 2017-11-16 | A kind of kettle equipment of triazole crystallization |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207446258U true CN207446258U (en) | 2018-06-05 |
Family
ID=62280247
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721533882.3U Expired - Fee Related CN207446258U (en) | 2017-11-16 | 2017-11-16 | A kind of kettle equipment of triazole crystallization |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207446258U (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109173325A (en) * | 2018-09-30 | 2019-01-11 | 蔡素真 | A kind of Chemical Manufacture crystallization kettle |
| CN110115855A (en) * | 2019-06-14 | 2019-08-13 | 浙江农林大学 | A kind of gibberellin plant growth regulator special-purpose crystallization pot |
| CN110773094A (en) * | 2019-11-25 | 2020-02-11 | 河北省环保产品质量监督检验研究院 | Reaction kettle stirrer suitable for reaction of viscous substances |
| CN110960882A (en) * | 2019-12-26 | 2020-04-07 | 临海市泰通医化设备有限公司 | Clean crystallization kettle |
| CN111672440A (en) * | 2020-06-29 | 2020-09-18 | 河北诺达化工设备有限公司 | Agitating unit and crystallization reaction cauldron |
| CN111905401A (en) * | 2020-08-18 | 2020-11-10 | 萍乡市利升科技有限公司 | Kettle type crystallization equipment and application thereof in potassium permanganate production |
| CN113750564A (en) * | 2021-09-30 | 2021-12-07 | 江苏筑美科技有限公司 | Crystallization kettle |
-
2017
- 2017-11-16 CN CN201721533882.3U patent/CN207446258U/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109173325A (en) * | 2018-09-30 | 2019-01-11 | 蔡素真 | A kind of Chemical Manufacture crystallization kettle |
| CN109173325B (en) * | 2018-09-30 | 2021-05-18 | 黄山友谊南海新材料有限公司 | Crystallization kettle for chemical production |
| CN110115855A (en) * | 2019-06-14 | 2019-08-13 | 浙江农林大学 | A kind of gibberellin plant growth regulator special-purpose crystallization pot |
| CN110115855B (en) * | 2019-06-14 | 2021-02-19 | 浙江农林大学 | Special crystallizer of gibberellin plant growth regulator |
| CN110773094A (en) * | 2019-11-25 | 2020-02-11 | 河北省环保产品质量监督检验研究院 | Reaction kettle stirrer suitable for reaction of viscous substances |
| CN110960882A (en) * | 2019-12-26 | 2020-04-07 | 临海市泰通医化设备有限公司 | Clean crystallization kettle |
| CN111672440A (en) * | 2020-06-29 | 2020-09-18 | 河北诺达化工设备有限公司 | Agitating unit and crystallization reaction cauldron |
| CN111905401A (en) * | 2020-08-18 | 2020-11-10 | 萍乡市利升科技有限公司 | Kettle type crystallization equipment and application thereof in potassium permanganate production |
| CN113750564A (en) * | 2021-09-30 | 2021-12-07 | 江苏筑美科技有限公司 | Crystallization kettle |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180605 Termination date: 20201116 |