CN110773094A - Reaction kettle stirrer suitable for reaction of viscous substances - Google Patents

Reaction kettle stirrer suitable for reaction of viscous substances Download PDF

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CN110773094A
CN110773094A CN201911161843.9A CN201911161843A CN110773094A CN 110773094 A CN110773094 A CN 110773094A CN 201911161843 A CN201911161843 A CN 201911161843A CN 110773094 A CN110773094 A CN 110773094A
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reactor body
reactor
reaction
wall
fixed
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张蓓
吕晓飞
赵慧
肖军
李晨曦
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Hebei Institute Of Quality Supervision And Inspection Of Environmental Protection Products
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers

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Abstract

本发明公开了一种适合黏性物质反应的反应釜搅拌器,包括设有进料口和出料口的反应釜本体、固设于反应釜本体外壁上用于注入加热液体进行加热的夹套、固设于反应釜本体外壁且一端延伸至反应釜本体内部的测温装置、固设于反应釜本体上的传动装置、固设于传动装置上并位于反应釜本体内腔的锚式桨叶和用于控制传动装置的控制装置,所述锚式桨叶为与反应釜本体内壁相匹配的片状结构,所述锚式桨叶的外边缘上固设有用于将反应釜本体内壁上的黏性物质刮下来的多个硅胶片。本发明结构简单,易于操作,搅拌均匀,不会产生挂壁现象,有利于传热和维持曝气的条件,适用于所有反应釜搅拌器。

Figure 201911161843

The invention discloses a reactor agitator suitable for the reaction of viscous substances. , a temperature measuring device fixed on the outer wall of the reactor body and one end extending into the inside of the reactor body, a transmission device fixed on the reactor body, an anchor paddle fixed on the transmission device and located in the inner cavity of the reactor body and The control device used to control the transmission device, the anchor paddle is a sheet-like structure that matches the inner wall of the reactor body, and the outer edge of the anchor paddle is fixed with a sticker for attaching the adhesive on the inner wall of the reactor body. Multiple pieces of silicone scraped off of sexual substances. The invention has the advantages of simple structure, easy operation, uniform stirring, no wall hanging phenomenon, favorable heat transfer and maintenance of aeration conditions, and is suitable for all reactor agitators.

Figure 201911161843

Description

适合黏性物质反应的反应釜搅拌器Reactor Stirrers for Viscous Reactions

技术领域technical field

本发明属于有机合成材料处理领域,涉及一种反应釜搅拌器,具体地说是一种适合黏性物质反应的反应釜搅拌器。The invention belongs to the field of organic synthetic material processing, and relates to a reaction kettle agitator, in particular to a reaction kettle agitator suitable for the reaction of viscous substances.

背景技术Background technique

目前按照GB/T 19277.1-208《受控堆肥条件下材料最终需氧生物分解能力的测定采用测定释放的二氧化碳的方法 第1部分:通用方法》进行检测的堆肥降解设备,通常采用大型水浴或夹套的方式进行加热,保持降解温度为(58±2)℃,由于反应温度较高,堆肥混合物的湿度为50%左右,很容易结块,不利于维持曝气条件。At present, the compost degradation equipment tested in accordance with GB/T 19277.1-208 "Determination of the final aerobic biodegradability of materials under controlled composting conditions adopts the method for the determination of released carbon dioxide Part 1: General method", usually large water baths or clamps are used. The composting mixture is heated in a way to keep the degradation temperature at (58±2) °C. Due to the high reaction temperature, the humidity of the compost mixture is about 50%, which is easy to agglomerate, which is not conducive to maintaining aeration conditions.

现有技术中堆肥降解反应釜的搅拌通常采用手动搅拌或推进式搅拌桨进行搅拌,手动搅拌需要打开反应釜进行,影响反应釜中气流情况,且开盖时异味大,操作繁琐。推进式搅拌桨往往不易搅开结块的反应物,且物料挂壁现象严重,黏性较大时,推进式搅拌桨剪切力不够,还会存在转不动的现象,且不利于传热和维持曝气条件。In the prior art, manual stirring or propelling stirring paddles are usually used to stir the compost degradation reactor. Manual stirring needs to open the reactor, which affects the airflow in the reactor, and the peculiar smell is large when the lid is opened, and the operation is cumbersome. The propelling paddle is often difficult to stir up the agglomerated reactants, and the material hanging on the wall is serious. When the viscosity is large, the shearing force of the propelling paddle is not enough, and there will be a phenomenon that it cannot rotate, which is not conducive to heat transfer. and maintain aeration conditions.

专利号为:ZL201810748427.8,名称为:“一种不锈钢反应釜”的专利文献中公开了一种反应釜,其锚式搅拌器为棍棒形,它的缺点是:锚式搅拌器与反应物的接触面积较小,只能搅拌锚式搅拌器转动的圆周方向上的反应物,且当反应物附着于反应釜的内壁上时,需要打开反应釜的上封头,人工进行清理,清洗麻烦且造成了原料的浪费。The patent number is: ZL201810748427.8, and the patent document titled: "a stainless steel reaction kettle" discloses a reaction kettle, and its anchor stirrer is in the shape of a stick. Its shortcomings are: the anchor stirrer and the reactant The contact area of the reactor is small, and it can only stir the reactants in the circumferential direction of the rotation of the anchor stirrer, and when the reactants are attached to the inner wall of the reactor, it is necessary to open the upper head of the reactor and clean it manually, which is troublesome to clean. And caused a waste of raw materials.

发明内容SUMMARY OF THE INVENTION

为解决现有技术中存在的以上不足,本发明旨在提供一种适合黏性物质反应的反应釜搅拌器,以达到反应釜内壁不产生挂壁现象、搅拌均匀的目的。In order to solve the above deficiencies in the prior art, the present invention aims to provide a reactor agitator suitable for the reaction of viscous substances, so as to achieve the purpose of uniform stirring without wall hanging on the inner wall of the reactor.

为实现上述目的,本发明所采用的技术方案如下:一种适合黏性物质反应的反应釜搅拌器,包括设有进料口和出料口的反应釜本体、固设于反应釜本体外壁上用于注入加热液体进行加热的夹套、固设于反应釜本体外壁且一端延伸至反应釜本体内部的测温装置、固设于反应釜本体上的传动装置、固设于传动装置上并位于反应釜本体内腔的锚式桨叶和用于控制传动装置的控制装置,所述锚式桨叶为与反应釜本体内壁相匹配的片状结构,所述锚式桨叶的外边缘上固设有用于将反应釜本体内壁上的黏性物质刮下来的多个硅胶片。In order to achieve the above purpose, the technical scheme adopted in the present invention is as follows: a reactor agitator suitable for the reaction of viscous substances, comprising a reactor body provided with a feed port and a discharge port, fixed on the outer wall of the reactor body A jacket for injecting heating liquid for heating, a temperature measuring device fixed on the outer wall of the reactor body and one end extending into the inside of the reactor body, a transmission device fixed on the reactor body, fixed on the transmission device and located in the An anchor paddle in the inner cavity of the reactor body and a control device for controlling the transmission device, the anchor paddle is a sheet-like structure that matches the inner wall of the reactor body, and the outer edge of the anchor paddle is fixed on the outer edge. There are multiple silica gel sheets for scraping off the sticky substances on the inner wall of the reactor body.

作为对本发明的限定:所述锚式桨叶为U型。As a limitation of the present invention: the anchor paddle is U-shaped.

作为对本发明的进一步限定:所述硅胶片均匀间隔设置,且未连接锚式桨叶的一端与反应釜本体内壁接触。As a further limitation of the present invention, the silica gel sheets are evenly spaced, and the end not connected to the anchor paddle is in contact with the inner wall of the reactor body.

作为对本发明的再进一步限定:所述传动装置包括固设于反应釜本体外壁上的基座、固设于基座上的减速器、与减速器的输入端连接的电机和与减速器输出端连接的转轴,所述锚式桨叶固设于转轴未连接减速器的一端。As a further limitation of the present invention: the transmission device includes a base fixed on the outer wall of the reactor body, a reducer fixed on the base, a motor connected to the input end of the reducer, and an output end of the reducer The connected rotating shaft, the anchor blade is fixed on the end of the rotating shaft that is not connected to the reducer.

作为对本发明的更进一步限定:所述反应釜本体上设有人孔,所述人孔上设有密封盖。As a further limitation of the present invention: the reactor body is provided with a manhole, and the manhole is provided with a sealing cover.

作为对本发明的一种限定:所述进料口设于反应釜本体的上部,所述出料口设于反应釜本体的底部。As a limitation of the present invention, the feed port is provided at the upper part of the reactor body, and the discharge port is provided at the bottom of the reactor body.

作为对本发明的另一种限定:所述反应釜本体上设有机架。As another limitation of the present invention: the reactor body is provided with a frame.

由于采用了上述技术方案,本发明与现有技术相比,所取得的有益效果在于:Owing to adopting the above-mentioned technical scheme, compared with the prior art, the present invention has the following beneficial effects:

(1)本发明的锚式桨叶上设置有硅胶片,硅胶片有助于刮下反应釜内壁上的反应物,同时与反应釜的内壁间隙较小,保证了反应釜内的物料能得到充分的搅拌,提高了搅拌效率和质量,硅胶片为硅胶材质,具有良好的弹性,不会因为长期的搅拌损伤反应釜内壁,使锚式桨叶转动平稳,噪声小,制造与维护方便,成本低;(1) The anchor paddle of the present invention is provided with a silica gel sheet. The silica gel sheet helps to scrape off the reactants on the inner wall of the reactor, and at the same time, the gap with the inner wall of the reactor is small, which ensures that the materials in the reactor can be obtained. Sufficient stirring improves the stirring efficiency and quality. The silica gel sheet is made of silica gel and has good elasticity. It will not damage the inner wall of the reactor due to long-term stirring, so that the anchor paddle rotates smoothly, with low noise, convenient manufacturing and maintenance, and low cost. Low;

(2)本发明的锚式桨叶为U型的片状结构,增加了与反应物料接触的面积,有利于传热和维持曝气的条件,U型结构使其更好的与反应釜本体内壁贴合,使其搅拌更加均匀;(2) The anchor blade of the present invention has a U-shaped sheet structure, which increases the contact area with the reaction material, which is conducive to heat transfer and maintaining aeration conditions, and the U-shaped structure makes it better with the reactor body. The inner wall is attached to make the stirring more uniform;

(3)本发明的硅胶片均匀间隔设置,既能将反应釜本体内壁上的反应物刮下来,又不会增大锚式桨叶与反应釜内壁之间的摩擦力,且反应釜本体上设有机架,能保证锚式桨叶搅拌过程中反应釜本体更加稳定;(3) The silica gel sheets of the present invention are evenly spaced, which not only can scrape off the reactants on the inner wall of the reactor body, but also does not increase the friction between the anchor blade and the inner wall of the reactor body. Equipped with a frame, which can ensure that the reactor body is more stable during the stirring process of the anchor paddle;

(4)本发明的电机连接减速器,能增大剪切力,有助于黏性物质散开,使其搅拌更加均匀;(4) The motor of the present invention is connected to the reducer, which can increase the shear force, help the viscous material to disperse, and make the stirring more uniform;

(5)本发明的的进料口设于反应釜本体的上部,使加入的料反应更加彻底,出料口设于反应釜本体的底部,保证反应后不留残液。(5) The feed port of the present invention is arranged on the upper part of the reactor body, so that the added material reacts more thoroughly, and the discharge port is arranged at the bottom of the reactor body to ensure that no residual liquid is left after the reaction.

综上所述,本发明结构简单,易于操作,搅拌均匀,不会产生挂壁现象,有利于传热和维持曝气的条件,适用于所有反应釜搅拌器。To sum up, the invention has simple structure, easy operation, uniform stirring, no wall hanging phenomenon, favorable heat transfer and maintenance of aeration conditions, and is suitable for all reactor agitators.

附图说明Description of drawings

下面结合附图及具体实施例对本发明作更进一步详细说明。The present invention will be described in further detail below with reference to the accompanying drawings and specific embodiments.

图1为本发明实施例的透视结构示意图。FIG. 1 is a perspective structural schematic diagram of an embodiment of the present invention.

图中:1-反应釜本体,1.1-筒体,1.2-上封头,1.3-下封头,2-传动装置,21-转轴,22-基座,23-减速器,24-电机,3-锚式桨叶,4-硅胶片,5-人孔,6-密封盖,7-机架,8-夹套,8.1-进液口,8.2-出液口,9-进料口,10-出料口,11-测温装置。In the picture: 1-Reaction kettle body, 1.1-Cylinder body, 1.2-Upper head, 1.3-Lower head, 2-Transmission device, 21-Rotary shaft, 22-Base, 23-Reducer, 24-Motor, 3 -Anchor paddle, 4-silicone sheet, 5-manhole, 6-sealing cover, 7-frame, 8-jacket, 8.1-liquid inlet, 8.2-liquid outlet, 9-feed inlet, 10 - Discharge port, 11- Temperature measuring device.

具体实施方式Detailed ways

以下结合附图对本发明的优选实施例进行说明。应当理解,此处所描述的适合黏性物质反应的反应釜搅拌器为优选实施例,仅用于说明和解释本发明,并不构成对本发明的限制。The preferred embodiments of the present invention will be described below with reference to the accompanying drawings. It should be understood that the reactor agitator suitable for the reaction of viscous substances described here is a preferred embodiment, which is only used to illustrate and explain the present invention, and does not constitute a limitation of the present invention.

实施例 适合黏性物质反应的反应釜搅拌器Example Reactor agitator suitable for viscous substance reaction

本实施例如图1所示,一种适合黏性物质反应的反应釜搅拌器,包括设有进料口9和出料口10的反应釜本体1、固设于反应釜本体1外壁上用于注入加热液体进行加热的夹套8、固设于反应釜本体1外壁且一端延伸至反应釜本体1内部的测温装置11、固设于反应釜本体1上的传动装置2、固设于传动装置2上并位于反应釜本体1内的锚式桨叶3和用于控制传动装置2的控制装置,所述反应釜本体1包括筒体、固设于筒体上端(图1上端)的上封头1.2、固设于筒体下端(图1下端)的下封头1.3,所述下封头1.3的周向圆弧过渡,使反应釜本体1的底部(图1底部)相对较低,有利于反应物从出料口10流出,防止残留在反应釜本体1内;所述进料口9设于反应釜本体1的上封头1.2上,所述出料口10设于反应釜本体1下封头1.3的底部;所述上封头1.2上设有用于人观察反应状态的人孔5,所述人孔5上设有密封盖6;所述反应釜本体1上设有用于将反应釜本体1固定牢固的机架7;所述夹套8采用现有技术,所述夹套8上设有进液口8.1和出液口8.2,所述进液口8.1设于夹套的左下方(图1左下方),所述出液口8.2设于夹套8的右上方(图1的右上方);所述测温装置11采用现有技术中的测温管,所述测温管的上端固设于反应釜本体1的上封头1.2上,所述测温管的另一端延伸至反应釜本体1的内腔中,用于测定反应过程的温度。The present embodiment is shown in FIG. 1 , a reactor agitator suitable for the reaction of viscous substances, including a reactor body 1 provided with a feed port 9 and a discharge port 10, and a reactor body 1 fixed on the outer wall of the reactor body 1 for use. The jacket 8 is injected into the heating liquid for heating, the temperature measuring device 11 fixed on the outer wall of the reactor body 1 and one end extending into the inside of the reactor body 1, the transmission device 2 fixed on the reactor body 1, and the transmission device The anchor blade 3 and the control device for controlling the transmission device 2 are located on the device 2 and located in the reactor body 1. The reactor body 1 includes a cylinder, and an upper The head 1.2, the lower head 1.3 fixed at the lower end of the cylinder (the lower end of Figure 1), the circumferential arc of the lower head 1.3 transitions, so that the bottom of the reactor body 1 (the bottom of Figure 1) is relatively low, which is beneficial to The reactant flows out from the discharge port 10 to prevent it from remaining in the reactor body 1; the feed port 9 is set on the upper head 1.2 of the reactor body 1, and the discharge port 10 is set under the reactor body 1 The bottom of the head 1.3; the upper head 1.2 is provided with a manhole 5 for people to observe the reaction state, and the manhole 5 is provided with a sealing cover 6; The main body 1 is firmly fixed to the frame 7; the jacket 8 adopts the prior art, and the jacket 8 is provided with a liquid inlet 8.1 and a liquid outlet 8.2, and the liquid inlet 8.1 is provided at the lower left of the jacket (lower left in Figure 1 ), the liquid outlet 8.2 is located at the upper right of the jacket 8 (upper right in Figure 1 ); the temperature measurement device 11 adopts the temperature measurement tube in the prior art, and the temperature measurement tube The upper end of the temperature measuring tube is fixed on the upper sealing head 1.2 of the reactor body 1, and the other end of the temperature measuring tube extends into the inner cavity of the reactor body 1 for measuring the temperature of the reaction process.

所述传动装置2包括固设于反应釜本体1外壁上的基座22、与减速器23的输入端连接的电机24和与减速器23输出端连接的转轴21,所述转轴21穿过反应釜本体1的位置设有轴封装置,所述轴封装置采用现有技术,防止反应釜本体1内的温度或气流流失;所述控制装置控制传动装置2运动,即控制电机24正反转动,使反应釜本体1内的物料反应充分,有助于黏性物质散开,不会产生结块现象。The transmission device 2 includes a base 22 fixed on the outer wall of the reactor body 1, a motor 24 connected with the input end of the reducer 23, and a rotating shaft 21 connected with the output end of the reducer 23. The rotating shaft 21 passes through the reaction vessel. The position of the kettle body 1 is provided with a shaft sealing device. The shaft sealing device adopts the prior art to prevent the loss of temperature or airflow in the reactor body 1; the control device controls the movement of the transmission device 2, that is, controls the motor 24 to rotate forward and reverse , so that the material in the reactor body 1 reacts sufficiently, which helps the viscous substances to disperse and does not cause agglomeration.

所述转轴21未连接减速器23的一端固设有锚式桨叶3,所述锚式桨叶3为与反应釜本体1内壁相匹配的片状结构,所述锚式桨叶3为U型。所述锚式桨叶3的外边缘上固设有用于将反应釜本体1内壁上的黏性物质刮下来的多个硅胶片4,所述硅胶片4通过螺栓可拆卸的设于锚式桨叶3上,所述硅胶片4沿锚式桨叶3的外边缘均匀间隔设置,且硅胶片4未连接锚式桨叶3的一端与反应釜本体1内壁接触。An anchor paddle 3 is fixed at one end of the rotating shaft 21 that is not connected to the reducer 23 . The anchor paddle 3 is a sheet-like structure that matches the inner wall of the reactor body 1 , and the anchor paddle 3 is U-shaped. type. A plurality of silica gel sheets 4 for scraping off the viscous substances on the inner wall of the reactor body 1 are fixed on the outer edge of the anchor paddle 3, and the silica gel sheets 4 are detachably arranged on the anchor paddle through bolts. On the blade 3 , the silica gel sheets 4 are evenly spaced along the outer edge of the anchor paddle 3 , and the end of the silica gel sheet 4 not connected to the anchor paddle 3 is in contact with the inner wall of the reactor body 1 .

使用本实施例时,将物料放入反应釜本体1内,调节到合适的反应条件,同时启动传动装置2,使锚式桨叶3随着转轴21转动,锚式桨叶3上的硅胶片4与反应釜本体1的内壁接触,将黏在反应釜内壁上的反应物刮下来。When using this embodiment, the material is put into the reactor body 1, adjusted to suitable reaction conditions, and the transmission device 2 is started at the same time, so that the anchor paddle 3 rotates with the rotating shaft 21, and the silica gel sheet on the anchor paddle 3 rotates. 4. Contact with the inner wall of the reactor body 1, and scrape off the reactant sticking to the inner wall of the reactor.

Claims (7)

1.一种适合黏性物质反应的反应釜搅拌器,包括设有进料口和出料口的反应釜本体、固设于反应釜本体外壁上用于注入加热液体进行加热的夹套、固设于反应釜本体外壁且一端延伸至反应釜本体内部的测温装置、固设于反应釜本体上的传动装置、固设于传动装置上并位于反应釜本体内腔的锚式桨叶和用于控制传动装置的控制装置,其特征在于:所述锚式桨叶为与反应釜本体内壁相匹配的片状结构,所述锚式桨叶的外边缘上固设有用于将反应釜本体内壁上的黏性物质刮下来的多个硅胶片。1. A reactor agitator suitable for the reaction of viscous substances, comprising a reactor body provided with a feed port and a discharge port, a jacket fixed on the outer wall of the reactor body for injecting heating liquid for heating, a solid A temperature measuring device arranged on the outer wall of the reactor body and one end extending into the inside of the reactor body, a transmission device fixed on the reactor body, an anchor paddle fixed on the transmission device and located in the inner cavity of the reactor body, and a The control device for controlling the transmission device is characterized in that: the anchor-type paddle is a sheet-like structure that matches the inner wall of the reactor body, and the outer edge of the anchor-type paddle is fixed on the inner wall of the reactor body. The sticky substance scraped off multiple silicone sheets. 2.根据权利要求1所述的适合黏性物质反应的反应釜搅拌器,其特征在于:所述锚式桨叶为U型。2. The reactor agitator suitable for the reaction of viscous substances according to claim 1, characterized in that: the anchor paddle is U-shaped. 3.根据权利要求2所述的适合黏性物质反应的反应釜搅拌器,其特征在于:所述硅胶片均匀间隔设置,且未连接锚式桨叶的一端与反应釜本体内壁接触。3 . The reactor agitator suitable for the reaction of viscous substances according to claim 2 , wherein the silica gel sheets are evenly spaced, and the end not connected to the anchor paddle is in contact with the inner wall of the reactor body. 4 . 4.根据权利要求1-3中任意一项所述的适合黏性物质反应的反应釜搅拌器,其特征在于:所述传动装置包括固设于反应釜本体外壁上的基座、固设于基座上的减速器、与减速器的输入端连接的电机和与减速器输出端连接的转轴,所述锚式桨叶固设于转轴未连接减速器的一端。4. The reactor agitator suitable for the reaction of viscous substances according to any one of claims 1-3, characterized in that: the transmission device comprises a base fixed on the outer wall of the reactor body, fixed on the The speed reducer on the base, the motor connected with the input end of the speed reducer, and the rotating shaft connected with the output end of the speed reducer, the anchor blade is fixed on the end of the rotating shaft that is not connected to the speed reducer. 5.根据权利要求4所述的适合黏性物质反应的反应釜搅拌器,其特征在于:所述反应釜本体上设有人孔,所述人孔上设有密封盖。5 . The reactor agitator suitable for the reaction of viscous substances according to claim 4 , wherein the reactor body is provided with a manhole, and the manhole is provided with a sealing cover. 6 . 6.根据权利要求5所述的适合黏性物质反应的反应釜搅拌器,其特征在于:所述进料口设于反应釜本体的上部,所述出料口设于反应釜本体的底部。6 . The reactor agitator suitable for the reaction of viscous substances according to claim 5 , wherein the feed port is arranged on the upper part of the reactor body, and the discharge port is arranged on the bottom of the reactor body. 7 . 7.根据权利要求1-3、5、6中任意一项所述的适合黏性物质反应的反应釜搅拌器,其特征在于:所述反应釜本体上设有机架。7. The reactor agitator suitable for the reaction of viscous substances according to any one of claims 1-3, 5 and 6, wherein the reactor body is provided with a frame.
CN201911161843.9A 2019-11-25 2019-11-25 Reaction kettle stirrer suitable for reaction of viscous substances Pending CN110773094A (en)

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Application publication date: 20200211