CN207280675U - A kind of quartz tube device for detecting vacuum glass vacuum - Google Patents

A kind of quartz tube device for detecting vacuum glass vacuum Download PDF

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Publication number
CN207280675U
CN207280675U CN201721025612.1U CN201721025612U CN207280675U CN 207280675 U CN207280675 U CN 207280675U CN 201721025612 U CN201721025612 U CN 201721025612U CN 207280675 U CN207280675 U CN 207280675U
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vacuum
glass
quartz
graduation mark
tube device
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卢雁鹏
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Rainbow Group New Energy Ltd By Share Ltd
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Rainbow Group New Energy Ltd By Share Ltd
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Abstract

A kind of quartz tube device for detecting vacuum glass vacuum, includes the cylindric quartz ampoule of one end open, and the wire that can be moved freely is equipped with quartz ampoule, has the graduation mark of mark vacuum degree in quartz ampoule high temperature of outer surface of high sintering;When detecting vacuum using the device, between quartz tube device first is placed in two blocks of glass, vacuumizes and sealed at high temperature after sealing-in, when temperature drops to room temperature, contrast whether wire present position is at second group of graduation mark, judge whether vacuum degree meets necessary requirement with this;Due to having placed the present apparatus in advance in vacuum glass, so the detection of vacuum can be completed using high temperature when vacuumizing, without individually being heated to glass, thus plenty of time and energy consumption cost can be saved;In addition, when using the vacuum glass containing the present apparatus, vacuum degree can be read at any time, is detected so professional institution need not be sent to, can save detection, the expense of maintenance indirectly.

Description

A kind of quartz tube device for detecting vacuum glass vacuum
Technical field
The utility model belongs to vacuum glass production detection technique field, and in particular to one kind detection vacuum glass vacuum Quartz tube device.
Background technology
Vacuum glass belongs to one kind of energy-saving glass, is widely used at present in Passive low-energy building, and vacuum Degree becomes one of important indicator of evaluation vacuum glass quality.
The method of detection vacuum is that first upper strata glass is heated at present, by air thin among two glass by heat Amount conduction, when two pieces of glass temperatures are equal, record the spent time, two pieces of glass is estimated by the time to lower floor's glass Vacuum values between glass, this method need about 5 it is small when, time length, cost is higher;Other detection methods further include photoelastic method and move State method, but since to the more demanding of equipment, personnel and environment, operation difficulty is larger in actual production process.
The content of the invention
For overcome the deficiencies in the prior art, the purpose of this utility model is to provide a kind of detection vacuum glass vacuum Quartz tube device, can reduce testing cost, shorten detection time, and have the advantages that to operate easy, visual result.
To achieve these goals, the technical solution of the utility model is:
A kind of quartz tube device for detecting vacuum glass vacuum, includes the cylindric quartz ampoule of one end open, in quartz The wire that can be moved freely is equipped with pipe, has the graduation mark of mark vacuum degree in quartz ampoule high temperature of outer surface of high sintering.
Further, the overall diameter 3mm of the quartz ampoule, 1.82~1.84mm of interior diameter, long 65~80mm.
Further, the wire is long 5mm, the steel wire of 1.79~1.81mm of diameter.
Further, the graduation mark is divided into three groups:First group of graduation mark is one, arranged on away from 4.4~5.4mm of tube bottom it Between;Second group of graduation mark has three, is spaced 1mm successively and is arranged at away between 26.6~32.6mm of tube bottom;3rd group of graduation mark has Four, 1mm is spaced successively and is arranged at away between 44.5~64.5mm of tube bottom.
A kind of method using quartz tube device detection vacuum glass vacuum, comprises the following steps:
(1) under room temperature condition of normal pressure, between the quartz tube device equipped with wire is put into two blocks of glass, quartz ampoule dress It is in diagonal position to put with the aspirating hole of glass edge, then two pieces of glass edge gaps are used glass powder materials 500~600 Sealing-in processing is carried out under DEG C high temperature;
(2) two blocks of glass are exhausted at a temperature of 300~380 DEG C and vacuumized, make pressure be down to -0.02~- 0.08MPa, in the process, wire are more than the other end away from the pressure that the close one end of tube bottom is subject to, under the differential pressure action of both ends, It is moved near the 3rd group of graduation mark from tube bottom;Glass aspirating hole is then subjected to thawing cut-out, is fully sealed with reaching;
(3) when temperature is down to room temperature, wire is moved about at second group of graduation mark from the 3rd group of graduation mark, is shown The vacuum of the vacuum glass reaches required value;If not reaching at second group of graduation mark, need to readjust step (2) Evacuated pressure value, untill reaching requirement.
The beneficial effects of the utility model:
Due to just enclosing quartz tube device when producing vacuum glass, it is possible to high temperature when being vacuumized using exhaust Condition completes the detection of vacuum at the same time, without individually being heated to glass with conventional method, thus can save a large amount of Time and energy consumption cost;With the exception of this, vacuum glass often as some devices part, in use, when this A little devices break down when needing detection, since the vacuum degree in glass shown by quartz tube device can be directly read, and then Judge foregoing failure whether because vacuum glass vacuum caused by, without vacuum glass is unloaded and is sent to professional institution It is detected, detection, the expense of maintenance can be saved indirectly.
Brief description of the drawings
Fig. 1 is quartz tube device structure diagram;
Fig. 2 is placement perspective view of the quartz tube device in vacuum glass;
In figure, 1, quartz ampoule, 2, the 3rd groups of graduation marks, 3, second groups of graduation marks, 4, steel wire, 5, first groups of graduation marks, 6, Aspirating hole, 7, glass.
Embodiment
The utility model is described in detail with reference to the accompanying drawings and examples.
Embodiment 1:
As shown in Figure 1, a kind of quartz tube device for detecting vacuum glass vacuum, the cylindrical shape for including one end open is quartzy Pipe 1, the overall diameter 3mm of the quartz ampoule 1, interior diameter 1.82mm, long 70mm, are equipped with what can be moved freely in quartz ampoule 1 Steel wire 4, the steel wire 4 long 5mm, diameter 1.80mm, have the graduation mark of mark vacuum degree in 1 high temperature of outer surface of high of quartz ampoule sintering, The graduation mark is divided into three groups, and first group of graduation mark 5 is one, at away from tube bottom 5.4mm;Second group of graduation mark 3 has three, Interval 1mm is arranged at away between 28.6~31.6mm of tube bottom successively, and the 3rd group of graduation mark 2 has four articles, is spaced 1mm successively and is arranged at Away between 56.0~60.0mm of tube bottom.
A kind of method using quartz tube device detection vacuum glass vacuum, comprises the following steps:
(1) as shown in Fig. 2, under room temperature condition of normal pressure, by the quartz tube device equipped with steel wire 4 be put into two blocks of glass 7 it Between, quartz tube device and the aspirating hole 6 of 7 edge of glass are in diagonal position, then two pieces of 7 edge slots of glass are used glass dust Material carries out sealing-in processing under 500 DEG C of high temperature;
(2) two blocks of glass 7 are exhausted at a temperature of 320 DEG C and vacuumized, pressure is down to -0.02MPa, herein mistake Cheng Zhong, steel wire 4 are more than the other end away from the pressure that the close one end of tube bottom is subject to, and under the differential pressure action of both ends, it is moved to from tube bottom At 56.5mm, i.e., near the 3rd group of graduation mark 2;Glass aspirating hole 6 is then subjected to thawing cut-out, is fully sealed with reaching;
(3) when temperature is down to room temperature, graduation mark 2 is attached is moved at 29.6mm from the 3rd group for steel wire 4, i.e. second group of scale At line 3, show that the vacuum of the vacuum glass reaches required value, detection operation is completed.
Embodiment 2:
As shown in Figure 1, a kind of quartz tube device for detecting vacuum glass vacuum, the cylindrical shape for including one end open is quartzy Pipe 1, the overall diameter 3mm of the quartz ampoule 1, interior diameter 1.83mm, long 75mm, are equipped with what can be moved freely in quartz ampoule 1 Steel wire 4, the steel wire 4 long 5mm, diameter 1.81mm, have the graduation mark of mark vacuum degree in 1 high temperature of outer surface of high of quartz ampoule sintering, The graduation mark is divided into three groups, and first group of graduation mark 5 is one, at away from tube bottom 5.4mm;Second group of graduation mark 3 has three, Interval 1mm is arranged at away between 29.5~32.5mm of tube bottom successively, and the 3rd group of graduation mark 2 has four articles, is spaced 1mm successively and is arranged at Away between 59.5~63.5mm of tube bottom.
A kind of method using quartz tube device detection vacuum glass vacuum, comprises the following steps:
(1) as shown in Fig. 2, under room temperature condition of normal pressure, by the quartz tube device equipped with steel wire 4 be put into two blocks of glass 7 it Between, quartz tube device and the aspirating hole 6 of 7 edge of glass are in diagonal position, then two pieces of 7 edge slots of glass are used glass dust Material carries out sealing-in processing under 550 DEG C of high temperature;
(2) two blocks of glass 7 are exhausted at a temperature of 350 DEG C and vacuumized, pressure is down to -0.08MPa, herein mistake Cheng Zhong, steel wire 4 are more than the other end away from the pressure that the close one end of tube bottom is subject to, and under the differential pressure action of both ends, it is moved to from tube bottom At 60.5mm, i.e., near the 3rd group of graduation mark 2;Glass aspirating hole 6 is then subjected to thawing cut-out, is fully sealed with reaching;
(3) when temperature is down to room temperature, graduation mark 2 is attached is moved at 31.5mm from the 3rd group for steel wire 4, i.e. second group of scale At line 3, show that the vacuum of the vacuum glass reaches required value, detection operation is completed.
Pass through both examples above, in the range of common vacuum glass vacuum (- 0.02~-0.08MPa), sheet Device testing result is satisfied by requiring.
The scale and testing principle of quartz tube device:
The utility model mainly realizes the inspection to vacuum using the thermal expansion and contraction principle and gas-dynamic equation of gas Survey.
(1) wire of 5mm long is fitted at first in quartz ampoule group of graduation mark at room temperature, then first group of graduation mark It is away from the air quality in tube bottom region:M=ρ * V=1.293*h* π r2
Wherein:ρ atmospheric density, V are area's volume, and h is the section length, and r is quartz ampoule cross sectional radius;
The Ideal-Gas Equation is:P*V=n*R*T
Wherein:P is that perfect gas pressure, V are that perfect gas volume, n are that the amount of perfect gas material, R are perfect gases Constant 8.31441, T are perfect gas thermodynamic temperature (273.15+t);
(2) when temperature vacuumizes the glass exhaust equipped with quartz ampoule at 300~380 DEG C, by following relation:
When exhaust is evacuated down to P0(such as P0=-0.02MPa) when, due in glass and quartzy one section of tube opening is in Vacuum state, and first group of graduation mark is away from high temperature action is subject at the same time in tube bottom region, the air expansion in the area, both are common Under effect, wire can be moved to quartz ampoule open at one end, but due to the area space is limited, air capacity is less, when being expanded into After certain volume, active force will significantly weaken, and then make wire both ends stress equal, reach equilbrium position, at this time,
P0=-0.02MPa=n*R*T/V, n=m/M, V=π r2*h’
M is gaseous mass, M is air molal weight M=28.959, and h ' is distance of the equilbrium position away from tube bottom.
It is various more than to obtain:
H'=[m*R* (273.15+t)]/[M* π r2*P0]
=[8.31441* (273.15+t) * m]/[28.959*3.14*r2*P0]
(3) as temperature drops to room temperature (24 DEG C), due to first group of graduation mark away from tube bottom regional air shrink, wire from Equilbrium position h ' places originally are moved to tube bottom direction, untill new equilbrium position h ".
Pass through h ' and h " respectively with the vacuum degree under respective corresponding temperature, go out the 3rd group of graduation mark in quartz ampoule high scale With second group of graduation mark.
Calculating and scale by above-mentioned three step, have obtained wire position under certain temperature, certain vacuum angle value (h ' and h ") and the relation of vacuum, is finally detected, and sentence according to the vacuum of this other vacuum glass of scale relation pair It is disconnected whether to reach required vacuum requirement.

Claims (4)

  1. A kind of 1. quartz tube device for detecting vacuum glass vacuum, it is characterised in that:Cylindrical shape quartz including one end open Pipe (1), is equipped with the wire that can be moved freely in quartz ampoule (1), has mark very in quartz ampoule (1) high temperature of outer surface of high sintering The graduation mark of reciprocal of duty cycle value.
  2. A kind of 2. quartz tube device for detecting vacuum glass vacuum as claimed in claim 1, it is characterised in that:The quartz Manage overall diameter 3mm, the 1.82~1.84mm of interior diameter of (1), long 65~80mm.
  3. A kind of 3. quartz tube device for detecting vacuum glass vacuum as claimed in claim 1, it is characterised in that:The metal Silk is long 5mm, the steel wire (4) of 1.79~1.81mm of diameter.
  4. A kind of 4. quartz tube device for detecting vacuum glass vacuum as claimed in claim 1, it is characterised in that:The scale Line is divided into three groups, and first group of graduation mark (5) is one, arranged on away between 4.4~5.4mm of tube bottom;Second group of graduation mark (3) has three Bar, is spaced 1mm and is arranged at away between 26.6~32.6mm of tube bottom, the 3rd group of graduation mark (2) has four articles, is spaced 1mm successively successively It is arranged at away between 44.5~64.5mm of tube bottom.
CN201721025612.1U 2017-08-16 2017-08-16 A kind of quartz tube device for detecting vacuum glass vacuum Active CN207280675U (en)

Priority Applications (1)

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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107449549A (en) * 2017-08-16 2017-12-08 彩虹集团新能源股份有限公司 A kind of quartz tube device and its detection method for detecting vacuum glass vacuum

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107449549A (en) * 2017-08-16 2017-12-08 彩虹集团新能源股份有限公司 A kind of quartz tube device and its detection method for detecting vacuum glass vacuum

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