CN207002287U - A kind of cupric oxide comprehensive hot water circulatory system - Google Patents
A kind of cupric oxide comprehensive hot water circulatory system Download PDFInfo
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- CN207002287U CN207002287U CN201720486728.9U CN201720486728U CN207002287U CN 207002287 U CN207002287 U CN 207002287U CN 201720486728 U CN201720486728 U CN 201720486728U CN 207002287 U CN207002287 U CN 207002287U
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- Prior art keywords
- water
- inlet
- kettle
- cistern
- hot water
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 130
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 229960004643 cupric oxide Drugs 0.000 title claims abstract description 24
- 239000002002 slurry Substances 0.000 claims abstract description 24
- 238000005406 washing Methods 0.000 claims abstract description 8
- 238000004891 communication Methods 0.000 claims description 11
- 238000007599 discharging Methods 0.000 claims description 6
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract description 12
- 229910052802 copper Inorganic materials 0.000 abstract description 12
- 239000010949 copper Substances 0.000 abstract description 12
- 230000003647 oxidation Effects 0.000 abstract description 12
- 238000007254 oxidation reaction Methods 0.000 abstract description 12
- 239000012535 impurity Substances 0.000 abstract description 5
- 238000010276 construction Methods 0.000 abstract description 3
- 238000005530 etching Methods 0.000 description 6
- 239000002699 waste material Substances 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 125000004122 cyclic group Chemical group 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
Landscapes
- Treatment Of Water By Oxidation Or Reduction (AREA)
Abstract
This application discloses a kind of cupric oxide comprehensive hot water circulatory system, it includes cistern, reactor and filter press, reactor include kettle, hollow clamping sleeve and, coil pipe, the bottom of kettle is provided with discharge port, hollow clamping sleeve is provided with overfall, water inlet and discharge outlet, and water inlet connects the outlet of coil pipe, and overfall and discharge outlet are respectively communicated with cistern, the entrance of coil pipe is provided with three-way pipe, and three-way pipe includes cold water inlet, steam inlet and compressed air inlet；Filter press is provided with wash water entrance and slurry inlet, and its bottom is provided with washing water outlet, and slurry inlet connects the discharge port of kettle, wash water entrance connection cistern.The cupric oxide comprehensive hot water circulatory system of the application cleans oxidation copper slurry by using hot water, impurity is accelerated dissolving, and wash time is saved while improving solubility, simple in construction, easy to operate, makes full use of the heat energy of system, saves resource, energy-conserving and environment-protective.
Description
Technical field
The application belongs to circulating utilization device technical field, specifically, is related to a kind of cupric oxide comprehensive hot water cyclic system
System.
Background technology
During the processing of assist side etching waste liquor, the basic copper chloride in etching waste liquor can circulate profit by processing
With.In etching waste liquor injection reactor, basic copper chloride therein generates cupric oxide sediment by chemically reacting, but due to erosion
The complicated component of waste liquid in itself is carved, while regenerating cupric oxide sediment, however it remains plurality of impurities so that cupric oxide precipitates
The purity of thing is not high.In order to improve the purity of cupric oxide, by injecting cold water into reactor, by cold water by solubility it is miscellaneous
Matter dissolves and discharged, final to obtain the higher cupric oxide sediment of purity.Such a processing method is time-consuming longer, and cleans not thorough
Bottom can not realize energy-conserving and environment-protective, it is necessary to additionally use a large amount of clear water.
Utility model content
For the problems of the prior art, the purpose of this utility model is to provide a kind of cupric oxide comprehensive hot water cyclic system
System.
In order to solve the above-mentioned technical problem, this application discloses a kind of cupric oxide comprehensive hot water circulatory system, it includes：
Cistern；
Reactor, reactor include kettle, the hollow clamping sleeve being sheathed on the outside of kettle and the disk for being wound in kettle lateral wall
Pipe, the bottom of kettle are provided with discharge port, and the side of hollow clamping sleeve is provided with overfall, and the bottom of hollow clamping sleeve is provided with water inlet and row
The mouth of a river, water inlet are respectively communicated with cistern by the outlet of pipeline communication coil pipe, overfall and discharge outlet by pipeline, coil pipe
Entrance is provided with three-way pipe, and three-way pipe includes cold water inlet, steam inlet and compressed air inlet；And
Filter press, the top of filter press are provided with wash water entrance and slurry inlet, and its bottom is provided with washing water outlet, slurry inlet
Connect the discharge port of kettle, wash water entrance connection cistern.
According to the embodiment of the application, in addition to the first water pump, the first feeding mouth connection kettle of the first water pump unloads
Material mouth, the slurry inlet of the first discharging opening connection filter press of the first water pump.
According to the embodiment of the application, in addition to the second water pump, the second feeding mouth of the second water pump connects cistern, the
The second discharging opening connection wash water entrance of two water pumps.
According to the embodiment of the application, above-mentioned three-way pipe is provided with the first valve, the second valve and the 3rd valve, the first valve
The corresponding steam inlet of door, the second valve correspond to cold water inlet, and the 3rd valve corresponds to compressed air inlet.
According to the embodiment of the application, in addition to water diversion tank, the water inlet connection cistern of water diversion tank, water diversion tank goes out
The mouth of a river connects the second feeding mouth of the second water pump.
Compared with prior art, the utility model can be obtained including following technique effect：
The cupric oxide comprehensive hot water circulatory system of the application passes through pipeline communication reactor, filter press and cistern, reaction
Oxidation copper slurry in kettle is evacuated in filter press, and the clear water heat for cooling down reactor becomes hot water and is collected to cistern, then from
Cistern is evacuated to cleaning oxidation copper slurry in filter press, cleans oxidation copper slurry by hot water, impurity is accelerated dissolving, improve molten
Wash time is saved while solution is spent, it is simple in construction, it is easy to operate, the heat energy of system is made full use of, saves resource, energy-saving ring
Protect.
Brief description of the drawings
Accompanying drawing described herein is used for providing further understanding of the present application, forms the part of the application, this Shen
Schematic description and description please is used to explain the application, does not form the improper restriction to the application.In the accompanying drawings：
Fig. 1 is the schematic diagram of the cupric oxide comprehensive hot water circulatory system of the embodiment of the application one.
Embodiment
Multiple embodiments of the application, as clearly stated, the details in many practices will be disclosed with schema below
It will be explained in the following description.It should be appreciated, however, that the details in these practices is not applied to limit the application.Also
It is to say, in some embodiments of the application, the details in these practices is non-essential.In addition, for the sake of simplifying schema,
Some known usual structures will illustrate it in a manner of simply illustrative in the drawings with component.
On its " first " used herein, " second " etc., the meaning of order or cis-position is not especially censured, also non-use
To limit the application, it is just for the sake of difference with the component of constructed term description or operation.
Referring to Fig. 1, it is the schematic diagram of the cupric oxide comprehensive hot water circulatory system of the embodiment of the application one, as schemed institute
Show, the cupric oxide comprehensive hot water circulatory system of the application includes cistern 1, reactor 2 and filter press 3, and cistern 1 is respectively communicated with
Reactor 2 and filter press 3, reactor 2 connect filter press 3.Wherein reactor 2 includes kettle 21, is sheathed on outside kettle 21
The hollow clamping sleeve 22 of side and the coil pipe 23 for being wound in the lateral wall of kettle 21, the bottom of kettle 21 are provided with discharge port 211, hollow clamping sleeve
22 side is provided with overfall 221, and the bottom of hollow clamping sleeve 22 is provided with water inlet 222 and discharge outlet 223, and water inlet 222 passes through
The outlet 232 of pipeline communication coil pipe 23, overfall 221 and discharge outlet 223 are respectively communicated with cistern 2 by pipeline, coil pipe 23
Entrance 231 is provided with three-way pipe 2311, and three-way pipe 2311 includes cold water inlet 23111, steam inlet 23112 and compressed air inlet
23113.The top of filter press 3 is provided with wash water entrance 31 and slurry inlet 32, and its bottom is provided with washing water outlet 33, slurry inlet 32
The discharge port 211 of kettle 21 is connected, wash water entrance 31 connects cistern 1.
Further, in order to which smoothly the oxidation copper slurry in the kettle 21 of reactor 2 is pumped into filter press 3, peace is passed through
The oxidation copper slurry in the first water pump 4 extraction kettle 21 is filled, the first feeding mouth 41 of the first water pump 4 passes through pipeline communication kettle 2
Discharge port 211, the slurry inlet 32 that the first discharging opening 42 of the first water pump 4 passes through pipeline communication filter press 3.When cupric oxide is starched
Cupric oxide is washed, it is necessary to which the hot water in cistern 1 is pumped into filter press 3 after expecting in from reactor 2 into filter press 3, is passed through
Second water pump 5 is installed and extracts hot water in cistern 1, the second feeding mouth 51 of the second water pump 5 by pipeline communication cistern 1,
The wash water entrance 31 that second discharging opening 52 of the second water pump 5 passes through pipeline communication filter press 3；To prevent the water level in cistern 1
The second water pump 5 is caused not draw water less than the height of the second water pump 5, in the second feeding mouth 51 and cistern 1 of the second water pump 5
Between water diversion tank 6 is installed, i.e. the water inlet 61 of water diversion tank 6 passed through by pipeline communication cistern 1, the delivery port 62 of water diversion tank 6
Second feeding mouth 51 of the second water pump of pipeline communication 5, the volume of water diversion tank 6 are less than the volume of cistern 1, and water diversion tank 6 stores in advance
Water, it can be ensured that the water level in water diversion tank 6 is higher than the height of the second water pump 5.
In actual applications, etching waste liquor is added into reactor 2, basic copper chloride and sodium hydroxide in etching waste liquor
Solution reaction.The three-way pipe 2311 of the entrance 231 of the coil pipe 23 of the lateral wall of kettle 21 is provided with the first valve 23114, the second valve
23115 and the 3rd valve 23116, the corresponding cold water inlet 23111 of the first valve 23114,23115 corresponding steam inlet of the second valve
23112, the corresponding compressed air inlet 23113 of the 3rd valve 23116.The second valve 23115 is now opened, closes other valves,
High-temperature steam is passed through to steam inlet 23112, high-temperature steam moves along coil pipe 23.High-temperature steam makes kettle 21 by heat transfer
Temperature rise, so as to promote the reaction in kettle 21 to accelerate.High-temperature steam flows out from the outlet 232 of coil pipe 23, along pipeline from
The water inlet 222 of hollow clamping sleeve 22 enters, and after high-temperature steam enters hollow clamping sleeve 22, persistently kettle 21 is heated, high-temperature steam
Cooling is condensed into water during heat is changed.After the reaction in kettle 21 terminates, the second valve 23115 is closed, is opened
Valve at overfall 221 and discharge outlet 223, high-temperature steam are expelled to cistern 1 from overfall 221, and condensed water is from discharge outlet
223 are expelled to cistern 1.Heated by high-temperature steam, the temperature of kettle 21 is very high, it is necessary to cool.Now close the first valve
Valve at door 23114 and discharge outlet 223, the second valve 23115 is opened, cold water is passed through to cold water inlet 23111.Cold water is along disk
Pipe 23 flows, and takes away the heat that steam leaves, and while coil pipe 23 cools, the rise of cold water endothermic temperature, cold water is from coil pipe 23
Outlet 232 flow out, then enter the water inlet 222 of hollow clamping sleeve 22 along pipeline, and be full of hollow clamping sleeve 22, it is hollow so as to absorb
The heat of the steam of residual in chuck 22, during heat transfer, the heat exchange of kettle 21 and hollow clamping sleeve 22 is to cold
In water, the temperature of kettle 21 and hollow clamping sleeve 22 reduces, and the temperature of cold water further raises and becomes hot water.Hot water is from overfall
221 outflows, flowed into along pipeline standby in cistern 1.After cooling, the second valve 23115 is closed, stopping pours into cold water, beaten
The valve at the 3rd valve 23116 and discharge outlet 223 is opened, is passed through compressed air to compressed air inlet 23113, compressed air is entered
Enter coil pipe 23, then flow in hollow clamping sleeve 22, the water in coil pipe 23 and hollow clamping sleeve 23 is blown by compressed air and drained only, is
Heating is ready next time, and compressed air finally flows out from the discharge outlet 223 and overfall 221 of hollow clamping sleeve 22.Cool down
Bi Hou, reactant are discharged from the discharge port 211 of the bottom of kettle 21.The discharge port 211 of the bottom of kettle 21 is opened, starts the first water pump
4, the oxidation copper slurry in kettle 21 is extracted out, entered from the slurry inlet 32 at the top of filter press 3 in filter press 3.Charging finishes
Afterwards, the first water pump 4 is closed, opens the second water pump 5, the hot water in cistern 1 is extracted out, hot water enters in water diversion tank 6, then edge pipe
The wash water entrance 31 at road from the top of filter press 3 enters in filter press 3, and hot water flows washing oxidation copper slurry from top to bottom, solvable
Property impurity accelerates to dissolve in the hot water.After washing, hot water is discharged from the washing water outlet 33 of the bottom of filter press 3, and filter press 3 enters
The moisture of one step extruding oxidation copper slurry, compression make it become filter cake, and the hot water after washing contains the ion needed for etching solution, can
As follow-up formula raw material, make full use of, it is cost-effective.
In summary, in one or more embodiments of the application, the cupric oxide comprehensive hot water circulatory system of the application
By pipeline communication reactor, filter press and cistern, the oxidation copper slurry in reactor is evacuated in filter press, cools down reactor
Clear water heat become hot water and be collected to cistern, then be evacuated in filter press cleaning oxidation copper slurry from cistern, pass through heat
Water cleaning oxidation copper slurry, makes impurity accelerate dissolving, saves wash time while improving solubility, simple in construction, operation side
Just, the heat energy of system is made full use of, saves resource, energy-conserving and environment-protective.
Some preferred embodiments of the present utility model have shown and described in described above, but as previously described, it should be understood that this
Utility model is not limited to form disclosed herein, is not to be taken as the exclusion to other embodiment, and available for various
Other combinations, modification and environment, and above-mentioned teaching or association area can be passed through in utility model contemplated scope described herein
Technology or knowledge be modified.And the change and change that those skilled in the art are carried out do not depart from spirit of the present utility model and model
Enclose, then all should be in the protection domain of the appended claims for the utility model.
Claims (5)
- A kind of 1. cupric oxide comprehensive hot water circulatory system, it is characterised in that includingCistern；Reactor, the reactor include kettle, the hollow clamping sleeve being sheathed on the outside of the kettle and are wound in outside the kettle The coil pipe of side wall, the bottom of the kettle are provided with discharge port, and the side of the hollow clamping sleeve is provided with overfall, the hollow clamping sleeve Bottom be provided with water inlet and discharge outlet, the water inlet passes through the outlet of coil pipe described in pipeline communication, the overfall and row The mouth of a river is respectively communicated with the cistern by pipeline, wherein the entrance of the coil pipe is provided with three-way pipe, the three-way pipe includes cold Water inlet, steam inlet and compressed air inlet；AndFilter press, the top of the filter press are provided with wash water entrance and slurry inlet, and its bottom is provided with washing water outlet, the slurry Entrance connects the discharge port of the kettle, and the wash water entrance connects the cistern.
- 2. the cupric oxide comprehensive hot water circulatory system according to claim 1, it is characterised in that also including the first water pump, institute The first feeding mouth for stating the first water pump connects the discharge port of the kettle, and the first discharging opening of first water pump connects the pressure The slurry inlet of filter.
- 3. the cupric oxide comprehensive hot water circulatory system according to claim 1 or 2, it is characterised in that also including the second water pump, The second feeding mouth connection cistern of second water pump, the second discharging opening of second water pump connect the wash water entrance.
- 4. the cupric oxide comprehensive hot water circulatory system according to claim 1 or 2, it is characterised in that the three-way pipe is provided with First valve, the second valve and the 3rd valve, first valve correspond to the steam inlet, and second valve corresponds to cold water Entrance, the 3rd valve correspond to compressed air inlet.
- 5. the cupric oxide comprehensive hot water circulatory system according to claim 3, it is characterised in that described also including water diversion tank The water inlet of water diversion tank connects the cistern, and the delivery port of the water diversion tank connects the second feeding mouth of second water pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720486728.9U CN207002287U (en) | 2017-05-03 | 2017-05-03 | A kind of cupric oxide comprehensive hot water circulatory system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720486728.9U CN207002287U (en) | 2017-05-03 | 2017-05-03 | A kind of cupric oxide comprehensive hot water circulatory system |
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| Publication Number | Publication Date |
|---|---|
| CN207002287U true CN207002287U (en) | 2018-02-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720486728.9U Expired - Fee Related CN207002287U (en) | 2017-05-03 | 2017-05-03 | A kind of cupric oxide comprehensive hot water circulatory system |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111348688A (en) * | 2018-12-24 | 2020-06-30 | 格林美（江苏）钴业股份有限公司 | Post-treatment device and post-treatment process for cobaltosic oxide synthetic material |
-
2017
- 2017-05-03 CN CN201720486728.9U patent/CN207002287U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111348688A (en) * | 2018-12-24 | 2020-06-30 | 格林美（江苏）钴业股份有限公司 | Post-treatment device and post-treatment process for cobaltosic oxide synthetic material |
| CN111348688B (en) * | 2018-12-24 | 2023-11-21 | 格林美（江苏）钴业股份有限公司 | Device and process for post-treatment of cobaltosic oxide synthetic material |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180213 |