CN206881696U - Phosphorescence pyrimidine complex of iridium reaction unit - Google Patents
Phosphorescence pyrimidine complex of iridium reaction unit Download PDFInfo
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- CN206881696U CN206881696U CN201720347885.1U CN201720347885U CN206881696U CN 206881696 U CN206881696 U CN 206881696U CN 201720347885 U CN201720347885 U CN 201720347885U CN 206881696 U CN206881696 U CN 206881696U
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- safety
- sealing block
- rubber sealing
- retort
- fixed
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Abstract
The utility model embodiment discloses phosphorescence pyrimidine complex of iridium reaction unit, including safety can, and retort is provided with the safety can；Stiff buffer spring is provided between the retort and the safety can；The upper surface of the retort is provided with the first rubber sealing block and the 4th rubber sealing block；The upper surface of the safety can is provided with the second rubber sealing block and the 3rd rubber sealing block；A feeding device is interspersed with first rubber sealing block and second rubber sealing block；A tremie pipe is interspersed with 3rd rubber sealing block and the 4th rubber sealing block；Inertial gas tank is fixed with the lateral wall of the safety can；The first force (forcing) pump is fixed with the top surface of the inertial gas tank；The second force (forcing) pump is fixed with the bottom surface of the inertial gas tank.The beneficial effect of the utility model is security protection performance height, is economized on resources, easy to use, good cooling effect and service life are longer.
Description
Technical field
It the utility model is related to reaction unit field, more particularly to phosphorescence pyrimidine complex of iridium reaction unit.
Background technology
In recent years, electromechanical phosphorescent material is because having good luminescent properties and can reach quantum in 100% in theory
Efficiency and turn into study hotspot.The electromechanical phosphorescent material studied at present is mainly the organic heavy metal complex such as iridium, platinum, ruthenium, gold
Category complex of iridium have the luminous efficiency of relatively short triplet lifetime and Geng Gao, can send at room temperature stronger phosphorescence with
And to adjust emission wavelength the color of electroluminescent device can be made to cover whole visible region by the adjustment of ligand structure, it is
A kind of most studied phosphor material.The complex of iridium of pyrimidine and its derivative has relatively high as electromechanical phosphorescent material
Efficiency and long device lifetime, but the pyrimidine iridium complex phosphorescence material reported at present on document is relatively fewer.Certainly, do not have yet
Dedicated for producing or synthesizing the reactor of such compound or reaction unit.As a kind of new material, urgent need one
Kind can be specifically used to the reaction unit for producing or reacting such compound.
Current phosphorescence pyrimidine complex of iridium reaction unit, directly use a retort, it is easy to cause chemical analysis
And the leakage with the rare gas shared so that security protection performance is low；Can not be to not utilizing with the inert gas shared
Carry out recycling so that waste of resource；Easily the phosphorescence pyrimidine iridium good to complex reaction it can not be stored and be quantified
Take so that victory inconvenient for use；Comprehensive heat caused by complex reaction can not efficiently be cooled so that cooling effect
Fruit difference and vibrations are larger caused by agitating device during the complex reaction, the protection effect without antidetonation buffering so that
The service life of device is shorter.
Utility model content
The utility model provides phosphorescence pyrimidine complex of iridium reaction unit, can solve in the prior art, current phosphorescence
Pyrimidine complex of iridium reaction unit, it is low security protection performance to be present, waste of resource, victory inconvenient for use, cooling-down effect difference and uses
The problem of life-span is shorter.
The utility model provides phosphorescence pyrimidine complex of iridium reaction unit, including safety can, is set in the safety can
There is retort；Four stiff buffer springs of underrun of the retort are connected with the inner bottom surface of the safety can；It is described anti-
Answer and connected respectively by the madial wall of stiff buffer spring and safety can in the relative side wall of tank；The upper end of the retort is set
There are the first rubber sealing block and the 4th rubber sealing block；The upper end of the safety can is provided with the second rubber sealing block and the 3rd rubber
Glue sealing block；First rubber sealing block and the second rubber sealing block consistency from top to bottom；First rubber sealing block and
A feeding device is interspersed with second rubber sealing block；The feeding device includes rubber extruded ball and graded tube；Institute
The upper end for stating graded tube is connected with the rubber extruded ball；The lower end of the graded tube sequentially passes through second rubber sealing block
The inner bottom part of the retort is extended to first rubber sealing block；3rd rubber sealing block and the 4th rubber
Sealing block consistency from top to bottom；A tremie pipe is interspersed with 3rd rubber sealing block and the 4th rubber sealing block；It is described
The upper end of tremie pipe is fixedly connected with blanking funnel；The lower end of the tremie pipe is extended in the retort；The safety can
The center position of upper surface fixes organic frame；Motor is fixed with the frame；The output end of the motor, which is fixed, to be connected
Rotating shaft is connected to, the rotating shaft sequentially passes through the safety can roof and the retort roof；The bottom of the rotating shaft is fixed with
Several fixed blocks；The both sides of the fixed block are respectively fixed with stirring vane；It is symmetrically arranged with the roof of the safety can
First condensation water inlet and the second condensation water inlet；Drainpipe is provided with the side wall of the safety can bottom；The safety can
Lateral wall on be fixed with inertial gas tank；The first force (forcing) pump is fixed with the top surface of the inertial gas tank；It is described lazy
The second force (forcing) pump is fixed with the bottom surface of property gas reservoir；The input of first force (forcing) pump by appendix through connection extremely
Within the upper part of the retort；The output end of first force (forcing) pump is connected by appendix and the inertial gas tank
Connect；Within lower part of the output end of second force (forcing) pump by appendix through connection to the retort；Described second
The input of force (forcing) pump is connected by appendix with the inertial gas tank.
It is preferred that be provided with first switch valve on the tremie pipe, the first switch valve be located at the blanking funnel with
Between the safety can roof.
It is preferred that it is respectively arranged with axle between the rotating shaft and the safety can, between the rotating shaft and the retort
Envelope.
It is preferred that second switch valve is provided with the drainpipe.
It is preferred that between the side wall of the appendix and the safety can, the side wall of the appendix and the retort
Between be respectively arranged with sealing ring.
In the utility model embodiment, there is provided phosphorescence pyrimidine complex of iridium reaction unit, it is anti-by being set in safety can
Tank is answered, the process of phosphorescence pyrimidine complex of iridium reaction is carried out in retort, avoids the chemical analysis in retort and cooperation
Inert gas directly leakage is contacted by staff, wherein fills condensed water in the space between retort and safety can,
These condensed waters can wrap up whole retort, heat caused by complex reaction in retort can be carried out with comprehensive
Cooling so that good cooling effect, and when there is chemical analysis in retort or during the inert gas leakage with sharing, Ke Yiqi
To effective protection and alarming effect so that security protection performance is high；By fixing inert gas on the lateral wall of safety can
Storage tank, and inert gas can be transported in retort and be used by the second force (forcing) pump set, the first pressurization of setting
Unemployed gas in retort can be transported in inertial gas tank by pump so that can circulate profit to inert gas
With economizing on resources；By interting a feeding device, feeding therein in the first rubber sealing block and the second rubber sealing block
Device includes rubber extruded ball and graded tube, and the upper end of graded tube is connected with rubber extruded ball, and the lower end of graded tube sequentially passes through
Second rubber sealing block and the first rubber sealing block extend to the bottom of retort, when the good phosphorescence pyrimidine iridium of use complex reaction
During complex, extruding rubber extruded ball gently is only needed, under the effect of the pressure, realizes and is drawn to phosphorescence pyrimidine complex of iridium
In graded tube, feeding device is then extracted, is titrated to the position used, remaining second rubber sealing block and the first rubber seal
Block still plays the effect of sealing under the condition of palsticity of itself, enabling easily takes phosphorescence pyrimidine complex of iridium；It is logical
Cross and stiff buffer spring is set between safety can and retort as connector so that phosphorescence pyrimidine complex of iridium reaction dress
Put has the protection effect of antidetonation buffering during being stirred so that the service life of device is longer.
Brief description of the drawings
Fig. 1 is phosphorescence pyrimidine complex of iridium reaction unit structural representation provided by the utility model；
Fig. 2 is the feeding device structural representation of phosphorescence pyrimidine complex of iridium reaction unit provided by the utility model.
Description of reference numerals：1- safety cans；2- retort；3- stirring vanes；4- fixed blocks；5- rotating shafts；The rubber of 6- first
Sealing block；7- first condenses water inlet；The rubber sealing blocks of 8- second；9- feeding devices；91- rubber extruded balls；92- graded tubes；
10- frames；11- motor；12- tremie pipes；13- blanking funnels；14- first switch valves；The rubber sealing blocks of 15- the 3rd；16-
Two condensation water inlets；The rubber sealing blocks of 17- the 4th；18- appendixs；The force (forcing) pumps of 19- first；20- inertial gas tanks；21-
Two force (forcing) pumps；22- stiff buffer springs；23- drainpipes；24- second switch valves.
Embodiment
Below in conjunction with the accompanying drawings, an embodiment of the present utility model is described in detail, it is to be understood that this
The protection domain of utility model is not limited by embodiment.
As depicted in figs. 1 and 2, the phosphorescence pyrimidine complex of iridium reaction unit that the utility model embodiment provides, including it is anti-
Tank 1 is protected, retort 2 is provided with the safety can 1；Four stiff buffer springs 22 of underrun of the retort 2 and institute
State the inner bottom surface connection of safety can 1；Pass through stiff buffer spring 22 and safety can 1 respectively in the relative side wall of the retort 2
Madial wall connection；The upper end of the retort 2 is provided with the first rubber sealing block 6 and the 4th rubber sealing block 17；It is described anti-
The upper end of shield tank 1 is provided with the second rubber sealing block 8 and the 3rd rubber sealing block 15；First rubber sealing block 6 and described
The consistency from top to bottom of second rubber sealing block 8；One is interspersed with first rubber sealing block 6 and second rubber sealing block 8
Feeding device 9；The feeding device 9 includes rubber extruded ball 91 and graded tube 92；The upper end of the graded tube 92 and the rubber
Glue extrusion ball 91 connects；The lower end of the graded tube 92 sequentially passes through second rubber sealing block 8 and first rubber is close
Envelope block 6 extends to the inner bottom part of the retort 2；3rd rubber sealing block 15 and the 4th rubber sealing block are about 17
Alignment；A tremie pipe 12 is interspersed with 3rd rubber sealing block 15 and the 4th rubber sealing block 17；The blanking
The upper end of pipe 12 is fixedly connected with blanking funnel 13；The lower end of the tremie pipe 12 is extended in the retort 2；The protection
The center position of the upper surface of tank 1 fixes organic frame 10；Motor 11 is fixed with the frame 10；The motor 11 it is defeated
Go out end and be fixedly connected with rotating shaft 5, the rotating shaft 5 sequentially passes through the roof of safety can 1 and the roof of the retort 2；Described turn
The bottom of axle 5 is fixed with several fixed blocks 4；The both sides of the fixed block 4 are respectively fixed with stirring vane 3；The safety can 1
Roof on be symmetrically arranged with the first condensation water inlet 7 and the second condensation water inlet 16；Set in the side wall of the bottom of safety can 1
It is equipped with drainpipe 23；Inertial gas tank 20 is fixed with the lateral wall of the safety can 1；The top of the inertial gas tank 20
The first force (forcing) pump 19 is fixed with face；The second force (forcing) pump 21 is fixed with the bottom surface of the inertial gas tank 20；Described first
Within upper part of the input of force (forcing) pump 19 by the through connection of appendix 18 to the retort 2；First force (forcing) pump
19 output end is connected by appendix 18 with the inertial gas tank 20；The output end of second force (forcing) pump 21 passes through defeated
Within the through connection of tracheae 18 to the lower part of the retort 2；The input of second force (forcing) pump 21 passes through appendix 18
It is connected with the inertial gas tank 20.First switch valve 14 is provided with the tremie pipe 12, the first switch valve is located at
Between the blanking funnel 13 and the roof of the safety can 1.Between the rotating shaft 5 and the safety can 1, the rotating shaft 5 and institute
State and be respectively arranged with axle envelope between retort 2.Second switch valve 24 is provided with the drainpipe 23.The appendix 18 and institute
State between the side wall of safety can 1, be respectively arranged with sealing ring between the side wall of the appendix 18 and the retort 2.
Operation principle：The phosphorescence pyrimidine complex of iridium reaction unit, by setting retort 2 in safety can 1, phosphorescence is phonetic
The process of pyridine complex of iridium reaction is carried out in retort 2, avoids the chemical analysis in retort 2 and with the indifferent gas shared
Body directly leakage is contacted by staff, wherein fills condensed water in the space between retort 2 and safety can 1, these condensations
Water can wrap up whole retort 2, heat caused by complex reaction in retort 2 can be cooled with comprehensive,
So that good cooling effect, and when having chemical analysis in retort 2 or with the inert gas leakage shared, can play
The protection of effect and alarming effect so that security protection performance is high；By fixing inertial gas tank on the lateral wall of safety can 1
20, and inert gas can be transported in retort 2 and be used by the second force (forcing) pump 21 set, the first pressurization of setting
Unemployed gas in retort 2 can be transported in inertial gas tank 20 by pump 19 so that inert gas can be followed
Ring utilizes, and economizes on resources；By interting a feeding device 9 in the first rubber sealing block 6 and the second rubber sealing block 8, its
In feeding device 9 include rubber extruded ball 91 and graded tube 92, the upper end of graded tube 92 is connected with rubber extruded ball 91, scale
The lower end of pipe 92 sequentially passes through the second rubber sealing block 8 and the first rubber sealing block 6 extends to the bottom of retort 2, works as use
During the good phosphorescence pyrimidine complex of iridium of complex reaction, only need extruding rubber extruded ball 91 gently, under the effect of the pressure, realize
Phosphorescence pyrimidine complex of iridium is drawn in graded tube 92, feeding device 9 is then extracted, is titrated to the position used, it is remaining
Second rubber sealing block 8 and the first rubber sealing block 6 still play the effect of sealing under the condition of palsticity of itself, enabling
Easily take phosphorescence pyrimidine complex of iridium；By setting stiff buffer spring 22 to be used as company between safety can 1 and retort 2
Fitting so that the phosphorescence pyrimidine complex of iridium reaction unit has the protection effect of antidetonation buffering during being stirred,
So that the service life of device is longer.
Disclosed above is only specific embodiment of the utility model, and still, the utility model embodiment is not limited to
This, the changes that any person skilled in the art can think of should all fall into the scope of protection of the utility model.
Claims (5)
1. phosphorescence pyrimidine complex of iridium reaction unit, it is characterised in that：Including safety can (1), it is provided with the safety can (1)
Retort (2)；Four stiff buffer springs (22) of underrun of the retort (2) and the inner bottom surface of the safety can (1)
Connection；Connected respectively by the madial wall of stiff buffer spring (22) and safety can (1) in the relative side wall of the retort (2)
Connect；The upper end of the retort (2) is provided with the first rubber sealing block (6) and the 4th rubber sealing block (17)；The safety can
(1) upper end is provided with the second rubber sealing block (8) and the 3rd rubber sealing block (15)；First rubber sealing block (6) and
Second rubber sealing block (8) consistency from top to bottom；In first rubber sealing block (6) and second rubber sealing block (8)
It is interspersed with a feeding device (9)；The feeding device (9) includes rubber extruded ball (91) and graded tube (92)；The scale
The upper end of pipe (92) is connected with the rubber extruded ball (91)；The lower end of the graded tube (92) sequentially passes through second rubber
Sealing block (8) and first rubber sealing block (6) extend to the inner bottom part of the retort (2)；3rd rubber seal
Block (15) and the 4th rubber sealing block (17) consistency from top to bottom；3rd rubber sealing block (15) and the 4th rubber are close
A tremie pipe (12) is interspersed with envelope block (17)；The upper end of the tremie pipe (12) is fixedly connected with blanking funnel (13)；Institute
The lower end for stating tremie pipe (12) is extended in the retort (2)；The center position of safety can (1) upper surface is fixed with
Frame (10)；Motor (11) is fixed with the frame (10)；The output end of the motor (11) is fixedly connected with rotating shaft
(5), the rotating shaft (5) sequentially passes through the safety can (1) roof and the retort (2) roof；The bottom of the rotating shaft (5)
It is fixed with several fixed blocks (4)；The both sides of the fixed block (4) are respectively fixed with stirring vane (3)；The safety can (1)
Roof on be symmetrically arranged with the first condensation water inlet (7) and second condensation water inlet (16)；The side of safety can (1) bottom
Drainpipe (23) is provided with wall；Inertial gas tank (20) is fixed with the lateral wall of the safety can (1)；The indifferent gas
The first force (forcing) pump (19) is fixed with the top surface of body storage tank (20)；Second is fixed with the bottom surface of the inertial gas tank (20)
Force (forcing) pump (21)；The input of first force (forcing) pump (19) passes through appendix (18) through connection to the retort (2)
Within upper part；The output end of first force (forcing) pump (19) is connected by appendix (18) and the inertial gas tank (20)
Connect；The output end of second force (forcing) pump (21) divides it by appendix (18) through connection to the bottom of the retort (2)
It is interior；The input of second force (forcing) pump (21) is connected by appendix (18) with the inertial gas tank (20).
2. phosphorescence pyrimidine complex of iridium reaction unit as claimed in claim 1, it is characterised in that set on the tremie pipe (12)
First switch valve (14) is equipped with, the first switch valve is located between the blanking funnel (13) and the safety can (1) roof.
3. phosphorescence pyrimidine complex of iridium reaction unit as claimed in claim 1, it is characterised in that the rotating shaft (5) with it is described
Axle envelope is respectively arranged between safety can (1), between the rotating shaft (5) and the retort (2).
4. phosphorescence pyrimidine complex of iridium reaction unit as claimed in claim 1, it is characterised in that set on the drainpipe (23)
It is equipped with second switch valve (24).
5. phosphorescence pyrimidine complex of iridium reaction unit as claimed in claim 1, it is characterised in that the appendix (18) and institute
State between the side wall of safety can (1), be respectively arranged with sealing between the side wall of the appendix (18) and the retort (2)
Circle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720347885.1U CN206881696U (en) | 2017-04-05 | 2017-04-05 | Phosphorescence pyrimidine complex of iridium reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720347885.1U CN206881696U (en) | 2017-04-05 | 2017-04-05 | Phosphorescence pyrimidine complex of iridium reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206881696U true CN206881696U (en) | 2018-01-16 |
Family
ID=61323495
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720347885.1U Expired - Fee Related CN206881696U (en) | 2017-04-05 | 2017-04-05 | Phosphorescence pyrimidine complex of iridium reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206881696U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113019293A (en) * | 2021-04-02 | 2021-06-25 | 董爱民 | Chemical industry reation kettle that stability is good and be convenient for wash |
-
2017
- 2017-04-05 CN CN201720347885.1U patent/CN206881696U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113019293A (en) * | 2021-04-02 | 2021-06-25 | 董爱民 | Chemical industry reation kettle that stability is good and be convenient for wash |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180116 Termination date: 20190405 |
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| CF01 | Termination of patent right due to non-payment of annual fee |