CN206730896U - A kind of high pressure homogenizer - Google Patents
A kind of high pressure homogenizer Download PDFInfo
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- CN206730896U CN206730896U CN201720074431.1U CN201720074431U CN206730896U CN 206730896 U CN206730896 U CN 206730896U CN 201720074431 U CN201720074431 U CN 201720074431U CN 206730896 U CN206730896 U CN 206730896U
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- pressure homogenizer
- inner sleeve
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/20—Jet mixers, i.e. mixers using high-speed fluid streams
- B01F25/27—Mixing by jetting components into a conduit for agitating its contents
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P13/00—Preparation of nitrogen-containing organic compounds
- C12P13/04—Alpha- or beta- amino acids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/06—Jet mills
Abstract
It the utility model is related to a kind of high pressure homogenizer, including motor (10), support and the high pressure cylinders on support, the high pressure cylinders include charging aperture, high-pressure plunger pump (20), with the high pressure resistant nozzle (30) of high-pressure plunger pump (20) outlet connection, and the discharge nozzle (40) being connected with high pressure resistant nozzle (30), the high pressure resistant nozzle (30) includes outer sleeve and inner sleeve (32), inner sleeve (32) is arranged in outer sleeve, inner sleeve (32) internal sequence is stated to be provided with by the first template (35), second template (36), the template sequence that 3rd template (37) and the 4th template (38) combine, every kind of template (35, 36, 37, 38) there is different types of material through hole.The utility model can realize ultra micro emulsification and the ultramicro grinding of less than 20 microns ranks of material Nano grade；The amplification of yield can be realized by using the mode amplified parallel, is highly suitable for from laboratory to industrialized process optimization.
Description
Technical field：
The utility model patent is related to a kind of material mixer structure, especially a kind of high pressure homogenizer.
Background technology：
The equipment that high pressure homogenizer is a kind of homogeneous for being used for liquid material (including liquid-liquid phase or liquid-solid phase), emulsified,
Food or medication chemistry industry are primarily adapted for use in, such as：Homogeneous in the process of producing product such as dairy products, beverage, cosmetics, medicine,
Emulsification process.
Existing high pressure homogenizer be using reciprocating pump as power, by liquid material or using liquid as carrier solid particle (or
Lipochondrion) work valve portion is transported to, by the pressure conduction of the ball valve core inside operating valve, shearing is produced to material, is touched
Hit, hole, the effect such as vortex so that material obtains micronization and mixed uniformly result.
High pressure homogenizer generally existing in the market is complicated, volume is big, efficiency is low and key components and parts (such as
Operating valve) the shortcomings of being easily lost, and be difficult be realized with a low cost Nano grade ultra micro emulsification and less than 20 microns ranks it is super
Miniaturization so that its popularization and application has a definite limitation.
The content of the invention
The utility model purpose is in order to solve the above mentioned problem of conventional high-tension homogenizer, there is provided a kind of small volume, efficiency
High high pressure homogenizer, particularly can with realized compared with low energy consumption the ultra micro of material Nano grade emulsification and 20 microns below ranks
Micronization.
To achieve the above object, the technical scheme of high pressure homogenizer provided by the utility model is as follows：It is a kind of high-pressure homogeneous
Machine, including motor, support and the high pressure cylinders on support, the high pressure cylinders include charging aperture, high-pressure plunger pump,
The high pressure resistant nozzle being connected with high-pressure plunger pump discharge, and the discharge nozzle being connected with high pressure resistant nozzle, the high pressure resistant nozzle
Including outer sleeve and inner sleeve, inner sleeve is arranged in outer sleeve, and the inner sleeve internal sequence is provided with by the first template, the
The template sequence that two templates, the 3rd template and the 4th form assembly form, every kind of template have different types of material through hole.
Further, first template, the second template, the 3rd template and the 4th template are all more for prismatic surface number identical
Prism.The thickness of each multiedge cylinder is 1-50mm.
Further, the material through hole of first template includes equally distributed multiple first entrance holes.
Further, the material through hole of second template includes equally distributed multiple second entrance holes, and described second
Entrance hole inside diameter is more than the first entrance hole inside diameter of the first template.
Further, the material through hole of the 3rd template includes equally distributed multiple 3rd entrance holes and a center
Hole, the centre bore center of circle overlap with template center；Each 3rd entrance hole is connected with centre bore by fine channel；It is each
The inwall of bar fine channel is serrated.
Further, there is a unique centre bore at the 4th template center.
Preferably, the template sequence includes 10 templates, specifically put in order for：First the-the second template-the of template
Three template the-the four template the-the three template the-the second template the-the three template the-the four template the-the second templates of the-the three template；Adjacent
Alignd at Liang Ge template center so that the material through hole of two adjacent forms is alignd and connected.
Further, the material for manufacturing these templates and high voltage bearing inner sleeve is jewel, ceramics, hard alloy, carbonization
Silicon, cermet or high polymer material and their composite, the proof pressure of material is 1-600MPa.
Further, the pipeline wall thickness of high voltage bearing outer sleeve is 2-10cm, and material proof pressure is 1-800MPa.
Using this new high pressure homogenizer, solid particle crushing, homogeneous, the emulsification in fluid can be efficiently realized.
This crushing, homogeneous, emulsifying technology, which can be widely applied to food or medication chemistry and other, needs the crushing, of material
All industries such as matter, emulsification, such as：Crushing, homogeneous in the production process of the products such as dairy products, beverage, cosmetics, medicine, chemical industry,
Emulsification process.
Technical scheme disclosed in the utility model not only includes technical scheme disclosed in this programme, in addition to by this skill
The technical scheme of art scheme any combination.
The utility model patent is mainly reflected in relative to the advantage of traditional high pressure homogenization technique：
1, it is possible to achieve the ultra micro emulsification of material Nano grade and the ultramicro grinding of less than 20 microns ranks, so as to obtain more
The product of high-quality；
2, the amplification of yield can be realized by using the mode amplified parallel, is highly suitable for from laboratory to industry
The process optimization of change.
Brief description of the drawings
Fig. 1 is the structural representation of the utility model high pressure homogenizer.
Fig. 2 is the high pressure resistant nozzle Longitudinal cross section schematic of the utility model high pressure homogenizer.
Fig. 3 is the inner sleeve cross-sectional view of the utility model high pressure homogenizer one embodiment.
Fig. 4 is that the high pressure resistant nozzle template of the utility model high pressure homogenizer one embodiment is arranged under the overlay schematic diagram.
Fig. 5 is the cross-sectional view of first template of the utility model high pressure homogenizer one embodiment.
Fig. 6 is the cross-sectional view of second template of the utility model high pressure homogenizer one embodiment.
Fig. 7 is the cross-sectional view of the 3rd template of the utility model high pressure homogenizer one embodiment.
Fig. 8 is the cross-sectional view of the 4th template of the utility model high pressure homogenizer one embodiment.
Fig. 9 is the millet dry powder former state grain size distribution that the utility model is related to.
Figure 10 is that the 40% dry powder millet 40MPa that the utility model is related to circulates grain size distribution after 1 processing.
Figure 11 is the dry powder rice bran former state grain size distribution that the utility model is related to.
Figure 12 is that the 30% dry powder rice bran 30MPa that the utility model is related to circulates grain size distribution after 1 processing.
Figure 13 is after the rice bran sample 120MPa routine commercial high voltages homogenizer that the utility model is related to circulates 3 processing
Grain size distribution.
Wherein, 10- motor, 20- high-pressure plunger pumps, the high pressure resistant nozzles of 30-, 31- outer sleeve upper envelopes, 32- inner sleeves
Cylinder, 321- endoporus, big envelope under 33- outer sleeves, 34- pads, the templates of 35- first, the entrance holes of 351- first, the templates of 36- second,
The entrance holes of 361- second, the templates of 37- the 3rd, the entrance holes of 371- the 3rd, 372- centre bores, 373- fine channels, the moulds of 38- the 4th
Plate, 381- centre bores, 40- discharge nozzles.
Embodiment
Below in conjunction with accompanying drawing, a kind of high pressure homogenizer of the utility model is described further.
As shown in figure 1, a kind of high pressure homogenizer of the utility model includes motor 10, support and the height on support
Press pump body, the high pressure cylinders include charging aperture, high-pressure plunger pump 20, the high pressure resistant nozzle with the outlet of high-pressure plunger pump 20 connection
30, and the discharge nozzle 40 being connected with high pressure resistant nozzle 30, the high pressure resistant nozzle 30 include outer sleeve and inner sleeve 32, inner sleeve
Cylinder 32 is arranged in outer sleeve, and the internal sequence of inner sleeve 32 is provided with by the first template 35, the second template 36, the 3rd template
37 and the 4th template sequence for combining of template 38, every kind of template (35,36,37,38) there is different material through hole.
First template 35, the second template 36, the 3rd template 37 are identical with the profile of the 4th template 38, are all polygon prism shape, can
To be the column of quadrangular, pentagonal prism, six prisms (as shown in Figure 4) even more polygon prism, in order to well with it is resistance to
The interior shape of the inner sleeve 32 of high pressure nozzle 30 matches, and for it is circumferential to prevent that template from occurring in inner sleeve 32
Rotate.For the different treating capacity requirement of high pressure homogenizer, the thickness range of each template is 1-50mm, and wherein treating capacity is got over
Greatly, the thickness of template is bigger.
As shown in Fig. 2 high voltage bearing outer sleeve includes two parts, a part is outer sleeve upper envelope 31, and another part is
Big envelope 33 under outer sleeve, big envelope 33, which is collectively forming, under outer sleeve upper envelope 31 and outer sleeve accommodates and the sky of sealing inner sleeve 32
Between, inner sleeve 32 is arranged on inside outer sleeve, and the end of the upper and lower ends of inner sleeve 32 is contacted by pad 34 with outer sleeve.It is interior
Coordinate between sleeve 32 and outer sleeve for gap, in order to strengthen the intensity of inner sleeve 32, outer sleeve also uses high voltage bearing material
It is made, when inner sleeve 32 is because by inner-pressure expansion, outer sleeve prevention inner sleeve 32 continues to expand.The pipeline of the outer sleeve
Wall thickness is 2-10cm, proof pressure 1-800MPa, it is preferable that is manufactured from the material that proof pressure is 50-500MPa outer
Sleeve.
As shown in figure 3, be the cross-sectional view of inner sleeve 32 of the utility model high pressure homogenizer one embodiment, inner sleeve
The endoporus 321 for being internally formed a hexagon of cylinder 32, for accommodating the first template 35, the second template 36, the and of the 3rd template 37
The template sequence that 4th template 38 is formed.When template select other shapes prism when, the shape of the endoporus 321 of inner sleeve 32 with
The external boundary shape of these prisms is corresponding.
As shown in figure 4, it is the high pressure resistant nozzle template superposition row of one preferred embodiment of the utility model high pressure homogenizer
Intention is listed, the internal sequence of inner sleeve 32 is provided with by the first template 35, the second template 36, the 3rd template 37 and the 4th template
38 template sequences combined, the sequence include 10 templates, are specially：The templates of first the second templates of template 35- 36- the 3rd
The second templates of template 37- of the 3rd the 3rd the 4th template 38- of template 37- of template 37- the second template 36- of the 4th template 38- of 37- the 3rd
36；Alignd at adjacent Liang Ge template center so that the material through hole of two adjacent forms is alignd and connected.
The material through hole of first template 35 includes equally distributed multiple first entrance holes 351, first entrance hole 351
Inside diameter is 0.5-2mm, the centre distance template center 10-500mm of the first entrance hole 351, first entrance hole
351 centre distance form boundary 0.5-10mm.The number of first entrance hole 351 can be 3,4,5,6 even more
It is more, preferably 6, as shown in Figure 5.
The material through hole of second template 36 includes equally distributed multiple second entrance holes 361, second entrance hole 361
Inside diameter is 3-5mm, the centre distance template center 10-500mm of the second entrance hole 361, second entrance hole 361
Centre distance form boundary 0.5-10mm.The number of second entrance hole 361 can be 3,4,5,6 it is even more more, it is excellent
Elect 6 as, as shown in Figure 6.The inside aperture of second entrance hole 361 of the second template 36 is more than the first importing of the first template 35
The inside aperture in hole 351, so that this high pressure resistant inside of nozzle 30 can reach the effect of cavitation.
The material through hole of 3rd template 37 includes equally distributed multiple 3rd entrance holes 371 and a centre bore 372, institute
It is 3-5mm to state the inside diameter of the 3rd entrance hole 371, the centre distance template center 10-500mm of the 3rd entrance hole 371, institute
State the centre distance form boundary 0.5-10mm of the 3rd entrance hole 371；The center of circle of centre bore 372 overlaps with template center, center
The inside diameter of hole 372 is 3-5mm；Each 3rd entrance hole 371 is connected with centre bore 372 by fine channel 373；It is each
The inwall of bar fine channel 373 is serrated, and the width of fine channel 373 is 0.1-10mm.The number of 3rd entrance hole 371
Can be 3,4,5,6 it is even more more, preferably 6, as shown in Figure 7.
There is a unique centre bore 381 at the center of 4th template 38, the inside diameter of centre bore 381 is 3-5mm.Such as figure
Shown in 8.
The material for manufacturing these templates (35,36,37,38) and high voltage bearing inner sleeve 32 can be jewel, ceramics, hard
Alloy, carborundum, cermet or high polymer material and their composite, the proof pressure of these materials is 1-
600MPa, it is preferable that manufacture these templates and inner sleeve from the material that proof pressure is 50-300MPa.
Using this new high pressure homogenizer, solid particle crushing, homogeneous, the emulsification in fluid can be efficiently realized.
This crushing, homogeneous, emulsifying technology, which can be widely applied to food or medication chemistry and other, needs the crushing, of material
All industries such as matter, emulsification, such as：Crushing, homogeneous in the production process of the products such as dairy products, beverage, cosmetics, medicine, chemical industry,
Emulsification process.
When using the utility model high pressure homogenizer, so that Fig. 4 provides the template sequence of embodiment as an example, its is worked
Journey is described as follows：Enter high pressure resistant nozzle 30 after material is extruded by high-pressure plunger pump 20, material enters first in nozzle 30
, can be quickly through the first template 35 after first entrance hole 351 of the surrounding distribution of template 35, and enter the surrounding of the second template 36
In second entrance hole 361 of distribution, now, first of the internal diameter of the second entrance hole 361 with respect to the first template 35 of the second template 36
The internal diameter of entrance hole 351 becomes big suddenly, and this reducing pressure differential can make fluid produce cavitation effect, so that fluid obtains acutely
Mixing and collision, obtain well mixed fluid mechanics.
The fluid mixed is entered in the 3rd entrance hole 371 of surrounding distribution of the 3rd template 37 by the second template 36,
Under pressure-driven, it can collect via each fine channel 373 towards centre bore 372.In zigzag fine channel 373, fluid
The turbulence dispersion that head-on collision is mixed between fluid is constantly carried out with vias inner walls to move.When fluid converges at heart hole 372 in a template
After conjunction, under pressure-driven, the central entrance hole i.e. centre bore 381 that the 4th piece of template is the 4th template 38 can be entered again.
Fluid via the 4th template 38 centre bore 381, into the 5th piece of template (with the 3rd piece of shape of template identical mould
Plate, i.e. the 3rd template 37) centre bore 372, and along the fine channel 373 of the surrounding of centre bore 372 towards the 3rd of surrounding
Entrance hole 371 continues to flow.Likewise, in zigzag fine channel 373, fluid constantly carries out head-on collision with vias inner walls and mixed
Turbulence dispersion motion between fluid.When fluid reaches the 5th piece of template i.e. the 3rd entrance hole 371 of the surrounding of the 3rd template 37
Afterwards, can enter the surrounding of the 6th piece of template (with second piece of shape of template identical template, i.e. the second template 36) second imports
Hole 361 and through the 6th piece of template hence into the 7th piece of template (with the 3rd piece of shape of template identical template, i.e. the 3rd mould
Plate 37) the 3rd entrance hole 371 of surrounding is distributed in, likewise, fluid under pressure-driven, is understood via each fine channel 373,
Collect towards centre bore 372, in zigzag fine channel 373, fluid constantly carries out head-on collision with vias inner walls and mixed and fluid
Between turbulence dispersion motion, after fluid converges at the 7th piece of template center hole 372, under pressure-driven, can enter again
The central entrance hole of 8th piece of template (with the template the 4th piece of shape of template, i.e. the 4th template 38) is centre bore 381.Stream
Body via the 8th piece of template centre bore 381, into the 9th piece of template (with the 3rd piece of shape of template identical template, i.e., the 3rd
Template 37) centre bore 372, and along the fine channel 373 of the surrounding of centre bore 372 towards the 9th piece of template surrounding
Three entrance holes 371 continue to flow, likewise, in zigzag fine channel 373, it is mixed that fluid constantly carries out head-on collision with vias inner walls
Close the turbulence dispersion motion between fluid.After fluid reaches the 3rd entrance hole 371 of the 9th piece of template surrounding, the can be entered
Second entrance hole 361 of the surrounding of ten pieces of templates (with second piece of shape of template identical template, i.e. the second template 36).Finally,
Fluid enters high pressure nozzle via the second entrance hole 361 of the surrounding of the tenth piece of template and exported, and completes the efficient of convection body material
Homogeneous, emulsification or crushing.
It is relatively outer between template that the exterior design of regular polygon runner orifice plate make it that each functional template stack combinations ensure
The precise positioning put.The high pressure nozzle that heterogeneous fluid containing solid particle is imported to this unique design by high pressure is handled,
In fine channel, cavitation is constantly repeated in solid particle, head-on collision, is crushed, mixing, is finally realized that heterogeneous fluid is efficiently equal
Matter, emulsification, crushing.
Embodiment 1：
According to the utility model, high pressure resistant nozzle design is as follows：
All stencil designs are superimposed into interior bone by installation successively into regular hexagon, then these templates and are shaped as positive six
In side shape, the outside high pressure resistant inner sleeve 32 for circle, big envelope 33 and pad under inner sleeve 32, outer sleeve upper envelope 31, outer sleeve
Piece 34 collectively forms high pressure resistant nozzle 30.This high pressure resistant nozzle 30 is connected with high-pressure plunger pump 20 and motor 10, formed
High pressure homogenizer of the present utility model.
The specific stencil design parameter of the present embodiment is as follows：
1, first piece of template surrounding is symmetrically distributed with 6 entrance holes, and template vertical thickness is 40mm, inside template entrance hole
A diameter of 2mm, entrance hole center origin distance template center origin distance 100mm, entrance hole center origin distance template border
10mm。
2, symmetrical 6 entrance holes of second piece of template surrounding, template vertical thickness is 40mm, and template entrance hole inside is straight
Footpath is 5mm, entrance hole center origin distance template center origin distance 100mm, entrance hole center origin distance template border
10mm。
First piece of template at second piece of template center's origin with aliging so that all entrance hole center origins of two pieces of templates
Align and connect.
3, symmetrical 6 entrance holes of the 3rd piece of template surrounding, template vertical thickness is 40mm, and template entrance hole inside is straight
Footpath is 5mm.Entrance hole center origin distance template center origin distance 40mm, entrance hole center origin distance template border
10mm.In addition, using each entrance hole as starting point, towards template center's origin at through template cut a fine channel, each
Fine channel runs through template, with pitch circle to equal distribution, finally causes template center to form a through hole and run through template.It is each thin
Inside microchannels are in intersection zigzag, channel width 0.2mm.
3rd piece of template at second piece of template center with aliging so that all entrance hole center origins alignment of two pieces of templates
And connect.
4, there is at the 4th piece of template center's origin unique one to import hole path and run through template, template vertical thickness is
40mm, template entrance hole inside diameter are 5mm.Entrance hole center origin distance template center origin distance 40mm, in entrance hole
Heart initial point distance form boundary 10mm.
5, the 5th piece of template is as the 3rd piece of template, symmetrical 6 entrance holes of surrounding, and template vertical thickness is
40mm, template entrance hole inside diameter are 5mm.Entrance hole center origin distance template center origin distance 40mm, in entrance hole
Heart initial point distance form boundary 10mm.In addition, using each entrance hole as starting point, towards template center's origin at through template cutting one
Bar fine channel, each fine channel run through template, with pitch circle to equal distribution, finally cause template center to form a through hole
Through template.In intersection zigzag, channel width 0.2mm inside each fine channel.
6, symmetrical 6 entrance holes of the 6th piece of template surrounding, template vertical thickness is 40mm, and template entrance hole inside is straight
Footpath is 5mm, entrance hole center origin distance template center origin distance 100mm, entrance hole center origin distance template border
10mm。
7, the 7th piece of template is as the 5th piece of template, symmetrical 6 entrance holes of surrounding, and template vertical thickness is
40mm, template entrance hole inside diameter are 5mm.Entrance hole center origin distance template center origin distance 40mm, in entrance hole
Heart initial point distance form boundary 10mm.In addition, using each entrance hole as starting point, towards template center's origin at through template cutting one
Bar fine channel, each fine channel run through template, with pitch circle to equal distribution, finally cause template center to form a through hole
Through the template.In intersection zigzag, channel width 0.2mm inside each fine channel.
8, the 8th piece of template centre has unique importing hole path to run through template, and template vertical thickness is 40mm,
Template entrance hole inside diameter is 5mm.Entrance hole center origin distance template center origin distance 40mm, entrance hole center origin
Distance template border 10mm.
9, the 9th piece of template is as the 5th piece of template, symmetrical 6 entrance holes of surrounding, and template vertical thickness is
40mm, template entrance hole inside diameter are 5mm.Entrance hole center origin distance template center origin distance 40mm, in entrance hole
Heart initial point distance form boundary 10mm.In addition, using each entrance hole as starting point, towards template center's origin at through template cutting one
Bar fine channel, each fine channel run through template, with pitch circle to equal distribution, finally cause template center to form a through hole
Through template.In intersection zigzag, channel width 0.2mm inside each fine channel.
10, the tenth piece of template is as the 6th piece of template, symmetrical 6 entrance holes of surrounding, and template vertical thickness is
40mm, template entrance hole inside diameter are 5mm, entrance hole center origin distance template center origin distance 100mm, in entrance hole
Heart initial point distance form boundary 10mm.
11, most this 10 pieces of model sheetinstallats in the just hexagonal tube passage of high voltage bearing high-strength material, form this reality at last
With the high pressure resistant jet element of new Novel high-pressure homogenizer.
The material for manufacturing these templates and just hexagonal tube passage is hard alloy, and the proof pressure of these materials is
120MPa。
Embodiment 2, utilize Novel high-pressure homogenizer wet pulverizing millet of the present utility model.
The commercially available millets of 5kg are crushed into 30min, the millet of obtained crushing with conventional Universalpulverizer (rotating speed 6000rpm)
Granular size D50 is 97.7um, and the above-mentioned millets (D50 97.7um) crushed of 4kg are added into 6kg water, are being sufficiently stirred feelings
Under condition, under 40MPa homogenization pressure, the Novel high-pressure homogenizer of the design and manufacture of embodiment 1 is pumped into, collects the millet in exit
Slurry, its grain diameter size is detected, as a result D50 is 9.5um.
Embodiment 3, utilize Novel high-pressure homogenizer wet pulverizing rice bran of the present utility model
The commercially available rice brans of 5kg are crushed into 30min with conventional Universalpulverizer (rotating speed 6000rpm), obtained rice bran particle is big
Small D50 is 99.4um, and the above-mentioned rice brans (D50 99.4um) crushed of 3kg are added into 7kg water, in the case of being sufficiently stirred,
Under 30MPa homogenization pressure, the Novel high-pressure homogenizer of the design and manufacture of embodiment 1 is pumped into, collects the rice bran slurry in exit, inspection
Its grain diameter size is surveyed, is as a result 13um for D50.
Embodiment 4, it is reference examples, utilizes conventional commercial high voltage homogenizer wet pulverizing rice bran
The commercially available rice brans of 5kg are crushed into 30min with conventional Universalpulverizer (rotating speed 6000rpm), obtained rice bran particle is big
Small D50 is 99.4um, and the above-mentioned millets (D50 99.4um) crushed of 3kg are added into 7kg water, in the case of being sufficiently stirred,
Under 120MPa homogenization pressure, conventional commercial high voltage homogenizer is pumped into, collects the rice bran slurry in exit, this slurry is repeated into profit
Continue homogeneous 2 times under 120MPa homogenization pressure with this conventional commercial high voltage homogenizer, finally collect and the rice of 3 times is crossed by homogeneous
Chaff slurry, its grain diameter size is detected, be as a result 85.8um for D50.
Embodiment 5, vitamin E nanoemulsions are prepared using Novel high-pressure homogenizer ultra micro emulsification of the present utility model
Under the conditions of 50 DEG C, by 3.5% (W/V) emulsifying agent (lecithin, Span80 and Tween80, mass ratio 1：2：
2) add in 76.5% (W/V) distilled water, it is fully dissolved, be stirred, form aqueous phase, and the purity of addition 20% is
98% vitamin E, under the conditions of 40 DEG C, high-speed shearing machine high speed shear 20min, makes under rotating speed 11000rpm stirring
Two-phase is sufficiently mixed, and forms colostric fluid, and the colostric fluid of emulsification is pressed with Novel high-pressure homogenizer of the present utility model in 30MPa
Under power, high-pressure homogeneous 30min, nanometer micro-emulsion is formed, collect nanometer micro-emulsion, vitamin E microemulsion spherolite footpath is big after testing
Small D50 is 250nm.
Embodiment 6, it is reference examples, vitamin E microemulsion is prepared using routine business high pressure homogenizer ultra micro emulsification.
Under the conditions of 50 DEG C, by 3.5% (W/V) emulsifying agent (lecithin, Span80 and Tween80, mass ratio 1：2：
2) add in 76.5% (W/V) distilled water, it is fully dissolved, be stirred, form aqueous phase, and the purity of addition 20% is
98% vitamin E, under the conditions of 40 DEG C, high-speed shearing machine tells shearing 20min, is under rotating speed 11000rpm stirring
Two-phase is sufficiently mixed, formed colostric fluid, by the colostric fluid of emulsification with conventional commercial high voltage homogenizer under 50MPa pressure, high pressure
Homogeneous 30min, microemulsion is formed, collect microemulsion, after testing, vitamin E microemulsion ball particle size D50 is 4um.
In this description, the utility model is described with reference to its specific embodiment.But it is clear that still can be with
Various modifications and alterations are made without departing from spirit and scope of the present utility model, an ordinary skill people for having this professional knowledge
Member, the technology that can be still taught according to this patent, produces other embodiments in the scope of the utility model, but every
Without departing from the content of technical solutions of the utility model, above example is made according to the technical essence of the utility model any
Simple modification, equivalent change and modification, in the range of still falling within technical solutions of the utility model.
Claims (10)
1. a kind of high pressure homogenizer, including motor (10), support and the high pressure cylinders on support, the high pressure cylinders
Include charging aperture, high-pressure plunger pump (20), with high-pressure plunger pump (20) outlet connection high pressure resistant nozzle (30), and with resistance to height
The discharge nozzle (40) of nozzle (30) connection is pressed, the high pressure resistant nozzle (30) includes outer sleeve and inner sleeve (32), inner sleeve
(32) it is arranged in outer sleeve, it is characterised in that：Inner sleeve (32) internal sequence is provided with by the first template (35), second
The template sequence that template (36), the 3rd template (37) and the 4th template (38) combine, every kind of template (35,36,37,38) tool
There is different types of material through hole.
2. high pressure homogenizer as claimed in claim 1, it is characterised in that：First template (35), the second template (36),
Three templates (37) and the 4th template (38) are all prismatic surface number identical multiedge cylinder.
3. high pressure homogenizer as claimed in claim 2, it is characterised in that：The material through hole of first template (35) includes equal
Multiple first entrance holes (351) of even distribution.
4. high pressure homogenizer as claimed in claim 3, it is characterised in that：The material through hole of second template (36) includes equal
Multiple second entrance holes (361) of even distribution, the second entrance hole (361) inside diameter are more than the first of the first template (35)
Entrance hole (351) inside diameter.
5. high pressure homogenizer as claimed in claim 4, it is characterised in that：The material through hole of 3rd template (37) includes equal
Multiple 3rd entrance holes (371) and a centre bore (372) of even distribution, centre bore (372) center of circle and template center's weight
Close；Each 3rd entrance hole (371) is connected with centre bore (372) by fine channel (374)；Each fine channel
(373) inwall is serrated.
6. high pressure homogenizer as claimed in claim 5, it is characterised in that：Have unique one at 4th template (38) center
Individual centre bore (381).
7. high pressure homogenizer as claimed in claim 6, it is characterised in that：The template sequence includes 10 templates, specific row
Row order be：The template (37)-the of (37)-the four template of first template (36)-the three template of (35)-the second template (38)-the three
The template (36) of (38)-the three template of two templates (37)-the four template of (36)-the three template (37)-the second；Two adjacent templates
Alignd at center so that the material through hole of two adjacent forms is alignd and connected.
8. the high pressure homogenizer as described in claim 1-7 is any, it is characterised in that：Manufacture these templates and high voltage bearing inner sleeve
The material of cylinder (32) is jewel, ceramics, hard alloy, carborundum, cermet or high polymer material and their composite wood
Material, the proof pressure of material is 1-600MPa.
9. the high pressure homogenizer as described in claim 1-7 is any, it is characterised in that：The pipeline wall thickness of outer sleeve is 2-10cm,
Material proof pressure is 1-800MPa.
10. high pressure homogenizer as claimed in claim 8, it is characterised in that：The pipeline wall thickness of outer sleeve is 2-10cm, and material is resistance to
It is stressed as 1-800MPa.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
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| CN2017100249200 | 2017-01-13 | ||
| CN201710024920 | 2017-01-13 |
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| CN206730896U true CN206730896U (en) | 2017-12-12 |
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| CN201720074431.1U Withdrawn - After Issue CN206730896U (en) | 2017-01-13 | 2017-01-19 | A kind of high pressure homogenizer |
| CN201710044089.5A Active CN106582340B (en) | 2017-01-13 | 2017-01-19 | High-pressure homogenizer |
| CN201710083734.4A Pending CN106755154A (en) | 2017-01-13 | 2017-02-16 | A kind of method that use micro passage reaction prepares phosphatidylserine |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710044089.5A Active CN106582340B (en) | 2017-01-13 | 2017-01-19 | High-pressure homogenizer |
| CN201710083734.4A Pending CN106755154A (en) | 2017-01-13 | 2017-02-16 | A kind of method that use micro passage reaction prepares phosphatidylserine |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106582340A (en) * | 2017-01-13 | 2017-04-26 | 上海理星生物技术有限公司 | High-pressure homogenizer |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034248A (en) * | 2017-06-19 | 2017-08-11 | 成都新柯力化工科技有限公司 | A kind of method of continuous high-efficient enzymatic conversion fabricated food phosphatidylserine |
| CN108271885A (en) * | 2018-02-28 | 2018-07-13 | 理星（天津）生物科技有限公司 | A kind of fruits and vegetables compound powder and its preparation method and application |
| CN111073924A (en) * | 2020-01-10 | 2020-04-28 | 福州三合元生物科技有限公司 | Micro-channel continuous synthesis method of vitamin C glucoside |
| CN115720973A (en) * | 2022-11-21 | 2023-03-03 | 宁夏红果生物科技有限公司 | Whole-fruit Chinese wolfberry fresh fruit puree and preparation method and application thereof |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1043562A (en) * | 1996-07-31 | 1998-02-17 | Maruyama Mfg Co Ltd | Emulsifying nozzle device |
| DK1008380T3 (en) * | 1998-12-07 | 2004-07-12 | Dsm Ip Assets Bv | Method and apparatus for mixing or dispersing liquids |
| BR0312153A (en) * | 2002-06-21 | 2005-03-29 | Nestec Sa | Method and device for liquefying a fat-based powder product particularly in the production of chocolate and the like |
| CN101230365A (en) * | 2008-01-08 | 2008-07-30 | 西安皓天生物工程技术有限责任公司 | Method for preparing powdered phosphatidyl serine |
| EP2206551B1 (en) * | 2008-12-23 | 2019-08-07 | Corning Incorporated | Microchannel reactors |
| US8696193B2 (en) * | 2009-03-06 | 2014-04-15 | Ehrfeld Mikrotechnik Bts Gmbh | Coaxial compact static mixer and use thereof |
| CN102439125B (en) * | 2010-12-03 | 2014-04-30 | 上海赢贝生物技术有限公司 | Method for preparing high quality antarctic krill oil of phosphatidylserine containing unsaturated double bond in the fatty acyl |
| CN102814137B (en) * | 2012-08-23 | 2014-07-30 | 诺泽流体科技(上海)有限公司 | Emulsifying cavity device of high-pressure homogeneous emulsifying equipment used for nanocrystallization preparation and method for emulsifying cavity device |
| KR101376971B1 (en) * | 2012-12-07 | 2014-03-25 | 홍해영 | Modular inline type homo mixer using vortex |
| CN103193682B (en) * | 2013-03-28 | 2015-08-26 | 常州大学 | In Continuous Flow micro passage reaction, Guanidinium nitrate acidifying Dehydration is for the method for nitroguanidine |
| CN105463036A (en) * | 2016-01-12 | 2016-04-06 | 南京工业大学 | Method for utilizing micro-reaction device for preparing long-chain fatty acid |
| CN206730896U (en) * | 2017-01-13 | 2017-12-12 | 理星（天津）生物科技有限公司 | A kind of high pressure homogenizer |
-
2017
- 2017-01-19 CN CN201720074431.1U patent/CN206730896U/en not_active Withdrawn - After Issue
- 2017-01-19 CN CN201710044089.5A patent/CN106582340B/en active Active
- 2017-02-16 CN CN201710083734.4A patent/CN106755154A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106582340A (en) * | 2017-01-13 | 2017-04-26 | 上海理星生物技术有限公司 | High-pressure homogenizer |
| CN106582340B (en) * | 2017-01-13 | 2022-07-12 | 理星（天津）生物科技有限公司 | High-pressure homogenizer |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106755154A (en) | 2017-05-31 |
| CN106582340A (en) | 2017-04-26 |
| CN106582340B (en) | 2022-07-12 |
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