CN206676024U - A kind of small-sized extraction equipment of R＆D units - Google Patents
A kind of small-sized extraction equipment of R＆D units Download PDFInfo
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- CN206676024U CN206676024U CN201720374839.0U CN201720374839U CN206676024U CN 206676024 U CN206676024 U CN 206676024U CN 201720374839 U CN201720374839 U CN 201720374839U CN 206676024 U CN206676024 U CN 206676024U
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Abstract
Extraction experiments apparatus field is the utility model is related to, the small-sized extraction equipment of specially a kind of R＆D units；Solve in the prior art that extracter is larger, extraction rate is slow, purity is low, the unsafe problem of extraction process；It includes：Housing, closure, microwave generator, motor, the housing cavity side wall is provided with three corner steadies, and the microwave generator is fixedly mounted on three corner steadies, and motor driving impeller rotates, first extractor and the second extractor are fixedly mounted on housing, and the housing upper surface is provided with master controller；Its advantage is：It is high to extract purity, extraction rate is fast, and whole device is compact-sized, occupies little space, and the environment small suitable for spaces such as R＆D units, microwave is concentrated in whole device, is not produced leakage, is greatly improved security performance.
Description
Technical field
Extraction experiments apparatus field is the utility model is related to, the small-sized extraction equipment of specially a kind of R＆D units.
Background technology
Extraction, also known as solvent extraction or liquid-liquid extraction, also known as extracts, is to have difference in a solvent using component in system
Solubility come separating mixture unit operation.That is, it is molten in the solvent of two kinds of objectionable interminglings (or slightly soluble) using material
The difference of solution degree or distribution coefficient, the method for making solute substance be transferred to out of a kind of solvent in another solvent.Widely
Apply to the industry such as chemistry, metallurgy, food, be common to petroleum refining industry.It is in addition that two kinds after extraction are incompatible mutually
The separated operation of liquid, is called liquid separation.Extraction is to be used for purifying one of means with purifying compound in Organic Chemistry Laboratory.
By extraction, required material can be extracted from solid or liquid mixture.Common extraction equipment has ultrasonic extraction
Agent, microwave abstracting machine, centrifugal extractor.Microwave abstracting machine, in general extraction heat are by extroversion in a manner of heat transfer, heat radiation etc.
In carry out, and microwave abstracting machine be microwave moment penetrate material inside and outside and meanwhile heating extracted, it is micro- compared with traditional extraction heat
The major advantage of ripple extraction is that quality is high, the functional component that can be effectively protected in food, medicine and other chemical combination materials；
Purity is high, extraction yield is high；There is high selectivity to extract；Speed is fast, saves trouble, and can save 50%-90% time；Solvent is used
Amount is few；Safety, energy-conservation, pollution-free, production equipment is simpler, greatlys save investment.Existing laboratory typically uses Centrifugical extraction
Machine, its shortcoming is that the material requirement extracted to needs is higher, especially suitable for the thing that two relative density differences are smaller or easily emulsify
System.
Application No. 201320479880.6 devises a kind of " microwave energy extraction equipment ", microwave energy extraction dress
Put, mainly including frame, microwave heating chamber, conveying pipeline, the defeated pipe of extractant, backflow collection port；It is characterized in that：It is defeated in frame
Expects pipe is passed through from microwave heating chamber, and feeding mouth and discharging collection block are respectively arranged with both ends, and the defeated pipe of extractant is connected on defeated
Expects pipe top, the defeated pipe of extractant is built in conveying pipeline, and the conveying pipeline other end is provided with backflow collection port, is heated in microwave
Bottom of chamber portion is provided with microwave source, has temperature identifier in microwave source, and the defeated pipe of extractant carries out flow control, the equipment by valve
The shortcomings that be two kinds of different solvents when by extraction equipment, it is impossible to sufficiently contact, so as to cause solute sufficient
Transfer, it is second-rate after extraction, it is necessary to which multiple purification by liquid extraction, significantly increases extraction time.Application No.
201520236743.9 devise a kind of " microwave extracting device for Chinese medicine ", and its structure includes feeder motor, helical blade, extraction
Groove, agitating paddle, microwave generator, baffle plate, left and right cylinder etc.；In the helical blade that is internally provided with of feeding warehouse, helical blade leads to
The hole set on feeding warehouse is crossed with feeder motor to be connected；Extraction tank is provided with below feeding warehouse, on the right side of extraction tank
Microwave generator is provided with, the mouth set in the right wall that baffle plate passes through extraction tank stretches into the inside of extraction tank；Electric rotating machine and stir
Mix oar to be arranged between upper and lower air cylinders and extraction tank, the surface for the mouth that the top that agitating paddle is arranged on extraction tank is set, stirring
Oar extend into the inside of extraction tank by the mouth set at the top of extraction tank, is the shortcomings that the device；It is complicated, using more
Individual cylinder, operation difficulty are improved, and microwave generator is directly connected at funnel, microwave is directly exposed, for a long time contact pair
Human body causes certain harm, and the device volume is larger in addition, is not suitable in the less environment in the spaces such as laboratory.
Therefore a kind of small-sized extraction equipment of R＆D units is devised, extraction purity is high, and extraction rate is fast, greatly contracting
Transfer time of the molecule of short required extraction in solvent, whole device is compact-sized, occupies little space, suitable for scientific research
In the small environment in the spaces such as laboratory, and microwave is concentrated in whole device, is not produced leakage, is greatly improved security
Energy.
Utility model content
The utility model provides a kind of small-sized extraction equipment of R＆D units, solves extracter in the prior art and accounts for
Big with space, extraction rate is slow, purity is low, the unsafe problem of extraction process, can effectively improve extraction purity and extraction speed
Rate, transfer time of the molecule of extraction in solvent required for greatly shortening, whole device is compact-sized, space-consuming
Small, the environment small suitable for spaces such as R＆D units, and microwave is concentrated in whole device, does not produce leakage, greatly
Improve security performance.
To achieve the above object, the technical solution adopted in the utility model is specific as follows：
A kind of small-sized extraction equipment of R＆D units, including：Housing 1, closure 2, microwave generator 4, motor 8, its
It is characterised by：The intracavity sidewall of housing 1 is provided with three corner steadies 3, and the microwave generator 4 is fixedly mounted on triangle and fixed
On frame 3, motor 8 is fixedly mounted on the fixed station 7 of the inner chamber bottom surface of housing 1, and the small belt pulley 9 on motor 8 passes through the band of belt 10
Dynamic big belt pulley 11 is rotated, and big belt pulley 11 is connected by impeller shafts 12 with impeller 13, and the impeller 13 is arranged on the second extraction
In tank 6, the second extractor 6 is externally connected to the first extractor 5, and the first extractor 5 and the second extractor 6 are fixedly mounted on shell
On body 1, the upper surface of housing 1 is provided with master controller 16, and closure 2 is provided with handle 19 and funnel 20.
The outside of housing 1 is provided with mounting table 101.
The material of first extractor 5 is stainless steel, and the material of the second extractor 6 is the insulation of glass, ceramics, plastics
Material, the transmitting terminal 401 of microwave generator 4 is between the first extractor 5 and the second extractor 6.
The bottom of second extractor 6 is arc structure, and middle position is provided with discharging tube 17, and inner surface is provided with concentration sense
Device 15 and temperature inductor 14 are answered, the other end of discharging tube 17 stretches out housing 1.
Valve 18 is installed on the discharging tube 17.
The beneficial effects of the utility model are：Microwave abstracting can effectively improve extraction purity and extraction rate, greatly
Transfer time of the molecule of extraction in solvent required for shortening, by microwave generator transmitting terminal be positioned over the first extractor and
Between second extractor so that caused microwave is concentrated in whole device, will not be produced leakage, be greatly improved safety
Performance, whole device is compact-sized, occupies little space, the environment small suitable for spaces such as R＆D units.
Brief description of the drawings
Fig. 1 is internal structure schematic diagram of the present utility model；
Fig. 2 is internal structure front view of the present utility model；
Fig. 3 is the utility model external structure schematic diagram；
Shown in figure：Housing 1, closure 2, three corner steadies 3, microwave generator 4, the first extractor 5, the second extractor
6th, fixed station 7, motor 8, small belt pulley 9, belt 10, big belt pulley 11, impeller shafts 12, impeller 13, temperature inductor 14, concentration
Inductor 15, master controller 16, discharging tube 17, valve 18, handle 19, funnel 20, mounting table 101, transmitting terminal 401.
Embodiment
Below in conjunction with the accompanying drawings and pass through specific embodiment further instruction the technical solution of the utility model：
Embodiment 1
As shown in Figures 1 to 3, the small-sized extraction equipment of a kind of R＆D units, by housing 1, closure 2, three corner steadies
3rd, microwave generator 4, the first extractor 5, the second extractor 6, fixed station 7, motor 8, small belt pulley 9, belt 10, big belt pulley
11st, impeller shafts 12, impeller 13, temperature inductor 14, concentration inductor 15, master controller 16, discharging tube 17, valve 18, handle
19 and funnel 20 form, the outside of the housing 1 is provided with mounting table 101, and its purposes is placement beaker or other containers.
The intracavity sidewall of housing 1 is provided with three corner steadies 3, and microwave generator 4 is arranged on three corner steadies, microwave
Direct current energy is transformed into microwave energy by generator, there is provided continuous-stable is microwave power, is to encounter metal to send out the characteristics of microwave
Raw reflection, metallics can not absorb or conducts microwaves, and microwave can pass through the insulating materials such as glass, ceramics, plastics, but not
Meeting consumed energy, but microwave can not only pass through, and its energy can be by solvent absorption.
The inner chamber bottom surface of housing 1 is provided with fixed station 7, and the fixed station 7 is right-angle prismatic rod structure, and motor 8 is arranged on fixed station 7
Inclined-plane on, small belt pulley 9 is installed on motor 8, by belt 10 drive big belt pulley 11 rotate, impeller 13, with big belt
Wheel 11 is connected by impeller shafts 12, big belt pulley 11, drives impeller 13 to rotate.Impeller 13 is fixed on the bottom of the second extractor 6,
In the rotation process of impeller 13, the liquid in the second extractor 6 is driven to accelerate mixing, extraction required for greatly shortening
Transfer time of the molecule in solvent.
The extractor 6 of first extractor 5 and second is fixed on housing 1, and the material of the first extractor 5 is stainless steel
Deng metal material, the material of the second extractor 6 is the insulating materials such as glass, ceramics, plastics, the transmitting terminal 401 of microwave generator 4
Between the first extractor 5 and the second extractor 6, from microwave property, pass through the structure so that microwave concentrates on second
In extractor 6, do not reveal, increase the security of whole device.
The bottom of second extractor 6 is arc structure, and middle position is installed by discharging tube 17, the output end of discharging tube 17
Positioned at the top of the mounting table 101 of housing 1, the liquid that can be designed so that in the second extractor 6 can completely discharge and
It is readily cleaned.
Temperature inductor 14 and concentration inductor 15 are provided with second extractor 6, valve is installed on discharging tube 17
18, temperature inductor 14, concentration inductor 15 and valve 18 are connected with the master controller 16 installed in the upper surface of housing 1, temperature
Inductor 14 is used for the temperature for detecting liquid in the second extractor 6, by setting specific temperature, improves extraction rate and pure
Degree.Concentration inductor 15 cooperates with valve 18, when concentration inductor 15 senses specific concentration in the second extractor 6
Afterwards, master controller 16 is transferred information to, master controller 16 sends instruction so that valve 18 is opened or closed.Main control
Device is additionally operable to the start-stop of controlled motor 8 and the switch of microwave generator.
Handle 19 and funnel 20 are installed on the lid 2.
When specifically used, solvent is flowed into the second extractor by funnel, specific temperature is set by master controller,
Start microwave generator to be heated, while start motor and be stirred, it is main after concentration inductor senses specific concentration
Controller causes microwave generator and motor to stop, Open valve.
The utility model is not limited to above-mentioned preferred forms, and anyone can draw under enlightenment of the present utility model
Other various forms of products, however, make any change in its shape or structure, it is every that there is same as the present application or phase
Approximate technical scheme, all falls within the scope of protection of the utility model.
Claims (5)
1. a kind of small-sized extraction equipment of R＆D units, including：Housing (1), closure (2), microwave generator (4), motor
(8), it is characterised in that：Housing (1) intracavity sidewall is provided with three corner steadies (3), the fixed peace of the microwave generator (4)
On three corner steadies (3), motor (8) is fixedly mounted on the fixed station (7) of housing (1) inner chamber bottom surface, on motor (8)
Small belt pulley (9) is connected transmission with big belt pulley (11) by belt (10), and big belt pulley (11) passes through impeller shafts (12) and ripple
(13) connection is taken turns, the impeller (13) is arranged in the second extractor (6), and the second extractor (6) is externally connected to the first extraction
Tank (5), the first extractor (5) and the second extractor (6) are fixedly mounted on housing (1), housing (1) the upper surface installation
There is master controller (16), closure (2) is provided with handle (19) and funnel (20).
A kind of 2. small-sized extraction equipment of R＆D units according to claim 1, it is characterised in that：The housing (1)
Outside is provided with mounting table (101).
A kind of 3. small-sized extraction equipment of R＆D units according to claim 1, it is characterised in that：First extraction
Tank (5) material is stainless steel and other metal materials, and the second extractor (6) material is the insulating materials such as glass, ceramics, plastics, described
Microwave generator (4) transmitting terminal (401) is between the first extractor (5) and the second extractor (6).
A kind of 4. small-sized extraction equipment of R＆D units according to claim 1, it is characterised in that：Second extraction
Tank (6) bottom is arc structure, and middle position is provided with discharging tube (17), and inner surface is provided with concentration inductor (15) and temperature sense
Device (14) is answered, discharging tube (17) other end stretches out housing (1).
A kind of 5. small-sized extraction equipment of R＆D units according to claim 4, it is characterised in that：The discharging tube
(17) valve (18) is installed on.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720374839.0U CN206676024U (en) | 2017-04-11 | 2017-04-11 | A kind of small-sized extraction equipment of R＆D units |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720374839.0U CN206676024U (en) | 2017-04-11 | 2017-04-11 | A kind of small-sized extraction equipment of R＆D units |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206676024U true CN206676024U (en) | 2017-11-28 |
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ID=60399001
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720374839.0U Expired - Fee Related CN206676024U (en) | 2017-04-11 | 2017-04-11 | A kind of small-sized extraction equipment of R＆D units |
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| CN (1) | CN206676024U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112843785A (en) * | 2020-12-29 | 2021-05-28 | 镇江市高等专科学校 | Chinese herbal medicine subcritical extraction complete equipment |
-
2017
- 2017-04-11 CN CN201720374839.0U patent/CN206676024U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112843785A (en) * | 2020-12-29 | 2021-05-28 | 镇江市高等专科学校 | Chinese herbal medicine subcritical extraction complete equipment |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171128 Termination date: 20180411 |
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| CF01 | Termination of patent right due to non-payment of annual fee |