CN202762429U - Novel liquid-solid reaction kettle with liquid extracting device - Google Patents
Novel liquid-solid reaction kettle with liquid extracting device Download PDFInfo
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- CN202762429U CN202762429U CN 201220338339 CN201220338339U CN202762429U CN 202762429 U CN202762429 U CN 202762429U CN 201220338339 CN201220338339 CN 201220338339 CN 201220338339 U CN201220338339 U CN 201220338339U CN 202762429 U CN202762429 U CN 202762429U
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- cylindrical shell
- suction pipe
- pumping device
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Abstract
The utility model relates to a novel liquid-solid reaction kettle with a liquid extracting device. The reaction kettle comprises a barrel, an observation hole, a jacket, a stirring apparatus and the liquid extracting device. The observation hole is arranged on a side wall of the barrel, the jacket is arranged on the outer side of the barrel, the stirring apparatus comprises a stirrer and a stirring driving device connected with the stirrer, the stirrer is arranged inside the barrel, the stirring driving device is arranged on the top of the barrel, the liquid extracting device comprises a liquid extracting tube and a liquid extracting driving device, the liquid extracting tube is connected with the liquid extracting driving device, a liquid extracting tube support is arranged on the barrel, and the liquid extracting tube is arranged on the liquid extracting tube support and is inserted into the barrel. Compared with the prior art, the novel liquid-solid reaction kettle has the advantages that energy consumed during extracted liquid vaporization and condensation liquefaction can be saved, ions or other complexes carried in extracted liquid cannot be dissolved, components of an obtained target product are stable relatively, and the novel liquid-solid reaction kettle is particularly suitable for processes for producing target products by means of impregnation.
Description
Technical field
The utility model relates to a kind of reactor, especially relates to a kind of novel liquid-solid reactor with pumping device.
Background technology
Usually the liquid-solid reaction still mainly is comprised of reaction vessel and agitator, and as only needing solid phase, reacted liquid phase is mainly arrived rear recovery of boiling point evaporation of this liquid phase by Steam Heating by the housing of reaction vessel.But situation more for liquid phase or that the liquid phase boiling point is higher then needs to expend a large amount of energy could all evaporate liquid phase walk; And during unnecessary liquid evaporation, component wherein can most of residual target product surface that is attached to.Yet there are no report for the design that this liquid phase directly can be taken away.
The utility model content
The purpose of this utility model is exactly to provide a kind of relatively energy-conservation, the metastable novel liquid-solid reactor with pumping device of product component for the defective that overcomes above-mentioned prior art existence.
The purpose of this utility model can be achieved through the following technical solutions:
A kind of novel liquid-solid reactor with pumping device, this reactor comprises cylindrical shell, peep hole, chuck, agitating device and pumping device, described peep hole is located on the cylinder lateral wall, described chuck is located at the cylindrical shell outside, described agitating device comprises agitator and connected mixer drive, described agitator is located at inner barrel, described mixer drive is located at the cylindrical shell top, described pumping device comprises liquid suction pipe and drawing liquid drive unit, described liquid suction pipe connects the drawing liquid drive unit, described cylindrical shell is provided with the liquid suction pipe support, and described liquid suction pipe is arranged on the liquid suction pipe support and inserts in the cylindrical shell;
After reaction finishes, after the liquid-solid phase layering, liquid suction pipe is inserted in the liquid phase layer in the question response still, the drawing liquid drive unit drives liquid suction pipe liquid is extracted out.
Described cylindrical shell is vertical cylindrical shell, and this cylindrical shell top is ellipse head, and the middle part is cylindrical, and the bottom is conical head or ellipse head.
Described peep hole is the strip peep hole, is provided with withstand voltage lucite, and described peep hole and cylindrical shell are tightly connected, and the seal material determines according to the corrosivity of interior media.
The described chuck outside is welded with 2～4 journal stirrups.
Mechanical connection between described mixer drive and the cylindrical shell, the material of part seal determines according to interior media.
The end that described liquid suction pipe inserts reactor is provided with netted or bar-shaped filter, is efficient sintered metal filter, and the other end of liquid suction pipe is the discharging opening of Extract.
Described drawing liquid drive unit comprises motor, reductor, sprocket wheel and chain, and described motor linkage connects reductor, and described sprocket wheel is located on the liquid suction pipe, and reductor is connected by chain with sprocket wheel, and moving up and down of liquid suction pipe can be accurate to millimeter.
Described drawing liquid drive unit also comprises the limit switch of tape travel control.
Described drawing liquid drive unit is gear device or screw rod driving device.
The utility model has been installed the pumping device that band drives at the top of reactor, after reaction finishes, medium need leave standstill a period of time (deciding on actual conditions) in the reactor, behind solid phase and stratified liquid, (observe from observation panel), liquid suction pipe is inserted liquid phase layer (utilizing the packing seal sealing), utilize the drawing liquid drive unit that liquid phase is extruded from liquid suction pipe, because the liquid suction pipe thread end is equipped with efficient sintered metal filter, so the medium of solid phase can not taken out of, after liquid phase is extracted out substantially, with passing into heat medium in the chuck, residual liquid phase is steamed again.
Compared with prior art, the utility model can be saved the energy with Extract vaporization and condensation liquefaction, ion or other complex compounds carried secretly in the Extract simultaneously can not separated out, the target product component that obtains is relatively stable, and the utility model is particularly useful for the technique with dipping productive target product.
Description of drawings
Fig. 1 is structural representation of the present utility model.
The specific embodiment
Below in conjunction with the drawings and specific embodiments the utility model is elaborated.
Embodiment
A kind of novel liquid-solid reactor with pumping device, structure as shown in Figure 1, this reactor comprises cylindrical shell 1, peep hole 4, chuck 2, agitating device and pumping device.Cylindrical shell 1 is vertical cylindrical shell, and this cylindrical shell top is ellipse head, and the middle part is cylindrical, and the bottom is conical head.Peep hole 4 is located on cylindrical shell 1 sidewall, and peep hole 4 is tightly connected with cylindrical shell 1, and peep hole 4 is the strip peep hole, is provided with withstand voltage lucite, and the seal material determines according to the corrosivity of interior media.Chuck 2 is located at cylindrical shell 1 outside, and chuck 2 outsides are welded with 2～4 journal stirrups 3.Agitating device comprises agitator 5 and connected mixer drive 6, agitator 5 is located at cylindrical shell 1 inside, mixer drive 6 is located at cylindrical shell 1 top, mechanical connection between mixer drive 6 and the cylindrical shell 1, and the material of part seal determines according to interior media.Pumping device comprises liquid suction pipe 7 and drawing liquid drive unit, liquid suction pipe 7 connects the drawing liquid drive unit, cylindrical shell 1 is provided with liquid suction pipe support 12, liquid suction pipe 7 is arranged on the liquid suction pipe support 12 and inserts in the cylindrical shell 1, the end that liquid suction pipe 7 inserts reactor is provided with netted or bar-shaped efficient sintered metal filter, the other end of liquid suction pipe 7 is the discharging opening of Extract, the drawing liquid drive unit comprises motor 11, reductor 10, sprocket wheel 8 and chain 9, motor 11 reductor 10 that is connected, sprocket wheel 8 is located on the liquid suction pipe 7, reductor 10 is connected by chain 9 with sprocket wheel 8, and moving up and down of liquid suction pipe 7 can be accurate to millimeter.The drawing liquid drive unit also comprises the limit switch of tape travel control.
After reaction finishes, after the interior liquid-solid phase layering of question response still, liquid suction pipe 7 is inserted cylindrical shell 1 interior liquid phase layer (utilizing the packing seal sealing), observe the insertion depth of liquid suction pipe 7 by peep hole 4, the drawing liquid drive unit drives liquid suction pipe 7 liquid phase is extracted out, because liquid suction pipe 7 thread ends are equipped with efficient sintered metal filter, so the medium of solid phase can not taken out of, after liquid phase is extracted out substantially, will pass into heat medium in the chuck 2 again, residual liquid phase is steamed.
In the utility model, the drawing liquid drive unit can also be gear device or screw rod driving device.
Claims (8)
1. novel liquid-solid reactor with pumping device, it is characterized in that, this reactor comprises cylindrical shell, peep hole, chuck, agitating device and pumping device, described peep hole is located on the cylinder lateral wall, described chuck is located at the cylindrical shell outside, described agitating device comprises agitator and connected mixer drive, described agitator is located at inner barrel, described mixer drive is located at the cylindrical shell top, described pumping device comprises liquid suction pipe and drawing liquid drive unit, described liquid suction pipe connects the drawing liquid drive unit, and described cylindrical shell is provided with the liquid suction pipe support, and described liquid suction pipe is arranged on the liquid suction pipe support and inserts in the cylindrical shell.
2. a kind of novel liquid-solid reactor with pumping device according to claim 1 is characterized in that, described cylindrical shell is vertical cylindrical shell, and this cylindrical shell top is ellipse head, and the middle part is cylindrical, and the bottom is conical head or ellipse head.
3. a kind of novel liquid-solid reactor with pumping device according to claim 1 is characterized in that, described peep hole is the strip peep hole, and described peep hole and cylindrical shell are tightly connected.
4. a kind of novel liquid-solid reactor with pumping device according to claim 1 is characterized in that mechanical connection between described mixer drive and the cylindrical shell.
5. a kind of novel liquid-solid reactor with pumping device according to claim 1 is characterized in that, the end that described liquid suction pipe inserts reactor is provided with netted or bar-shaped filter.
6. a kind of novel liquid-solid reactor with pumping device according to claim 1, it is characterized in that, described drawing liquid drive unit comprises motor, reductor, sprocket wheel and chain, described motor linkage connects reductor, described sprocket wheel is located on the liquid suction pipe, and reductor is connected by chain with sprocket wheel.
7. a kind of novel liquid-solid reactor with pumping device according to claim 7 is characterized in that, described drawing liquid drive unit also comprises the limit switch of tape travel control.
8. a kind of novel liquid-solid reactor with pumping device according to claim 1 is characterized in that, described drawing liquid drive unit is gear device or screw rod driving device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220338339 CN202762429U (en) | 2012-07-12 | 2012-07-12 | Novel liquid-solid reaction kettle with liquid extracting device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220338339 CN202762429U (en) | 2012-07-12 | 2012-07-12 | Novel liquid-solid reaction kettle with liquid extracting device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202762429U true CN202762429U (en) | 2013-03-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220338339 Expired - Lifetime CN202762429U (en) | 2012-07-12 | 2012-07-12 | Novel liquid-solid reaction kettle with liquid extracting device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202762429U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716713A (en) * | 2012-07-12 | 2012-10-10 | 上海立得催化剂有限公司 | Novel liquid and solid reaction kettle with liquid extraction device |
| CN106943770A (en) * | 2017-05-05 | 2017-07-14 | 章守艳 | Pig duodenum extract extraction element |
-
2012
- 2012-07-12 CN CN 201220338339 patent/CN202762429U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716713A (en) * | 2012-07-12 | 2012-10-10 | 上海立得催化剂有限公司 | Novel liquid and solid reaction kettle with liquid extraction device |
| CN106943770A (en) * | 2017-05-05 | 2017-07-14 | 章守艳 | Pig duodenum extract extraction element |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20130306 |