CN204841003U - Two subcrystalline crystallization equipment - Google Patents
Two subcrystalline crystallization equipment Download PDFInfo
- Publication number
- CN204841003U CN204841003U CN201520409446.XU CN201520409446U CN204841003U CN 204841003 U CN204841003 U CN 204841003U CN 201520409446 U CN201520409446 U CN 201520409446U CN 204841003 U CN204841003 U CN 204841003U
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- Prior art keywords
- crystallisation chamber
- chamber
- crystallisation
- crystallization chamber
- subcrystalline
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Abstract
The utility model relates to a two subcrystalline crystallization equipment, including a crystallization chamber, set up in the feed inlet of crystallization chamber side, establish the discharge gate as for crystallization chamber bottom, a crystallization chamber's inner wall is equipped with the heating jacket, and a crystallization chamber outer wall is equipped with heat preservation and temperature monitoring device, and there is a vacuum pump at a crystallization chamber's top through pipe connections, and a pipe fitting and a crystallization chamber are for seamless cooperation and stretch into a crystallization chamber's inner chamber, is equipped with the filter screen that hides when the foam at the tip of pipe fitting, still is provided with ultrasonic wave defoamer's interface and the interface that concentration analyzer inserted at a crystallization chamber's top, the output of vacuum pump has the 2nd crystallization chamber through pipe connections, and the 2nd crystallization chamber's charge door below is equipped with the filter screen, and the outer wall that the 2nd crystallization chamber's inner wall was equipped with heating jacket and the 2nd crystallization chamber is equipped with the temperature monitoring device. When realizing recycle crystallisation process, takes two subcrystalline crystallization equipment the waste material after the evacuation out.
Description
Technical field
The utility model relates to crystallizer technical field, is specifically related to a kind of two subcrystalline crystallizers.
Background technology
Crystallization is one of most important link in chemical products production process, and crystallization apparatus is also one of most widely used equipment in Chemical Manufacture.Crystallizer of the prior art improves the efficiency of crystallization frequently by vacuumizing, but after exhausting vacuum, the waste liquid of extraction can directly be given up usually, causes great waste.
Utility model content
The purpose of this utility model is to overcome defect of the prior art, designs a kind of two subcrystalline crystallizers that can realize vacuumizing when recycling crystallization process rear extraction waste material.
For achieving the above object, the technical scheme that the utility model adopts is:
A kind of two subcrystalline crystallizers, it is characterized in that, described equipment comprises the first crystallisation chamber, is arranged at the charging aperture of the first crystallisation chamber side, if as the discharging opening bottom the first crystallisation chamber; The inwall of described first crystallisation chamber is provided with heating jacket, first crystallisation chamber outer wall is provided with heat-insulation layer and device for monitoring temperature, the top of described first crystallisation chamber is connected with vavuum pump by pipe fitting, described pipe fitting and the first crystallisation chamber are seamlessly coordinate and stretch into the inner chamber of the first crystallisation chamber, be provided with in the end of described pipe fitting and hide when the filter screen of foam, be also provided with the interface that the interface of ultrasonic wave froth breaker and concentration analyzer are inserted at the top of described first crystallisation chamber; Described vacuum delivery side of pump is connected with the second crystallisation chamber by pipe fitting, is provided with screen pack below the charge door of described second crystallisation chamber, and the inwall of the second crystallisation chamber is provided with heating jacket and the outer wall of the second crystallisation chamber is provided with device for monitoring temperature.
Wherein preferred technical scheme is that described screen pack is be removable installed on the cross section of described second crystallisation chamber.
Preferred technical scheme also has, and the outer wall of described pipe fitting is provided with insulation jacket.
Preferred technical scheme also has, and bottom described first crystallisation chamber, be provided with agitating device, described agitating device comprises the drive motors being located at the first crystallisation chamber outside, and the turning cylinder controlled by drive motors is fixed on the stirring vane on turning cylinder; Described turning cylinder stretches into the first crystallisation chamber inner chamber through knot first brilliant room sidewall, and the length that turning cylinder stretches into the first crystallization chamber is equal with the diameter length of the first crystallisation chamber, and turning cylinder is movably connected on the inwall of the first crystallisation chamber.
Advantage of the present utility model and beneficial effect are: vacuum delivery side of pump by vacuumizing the first crystallisation chamber, then is connected to the second crystallisation chamber by described two subcrystalline crystallizers, takes full advantage of the waste material after vacuumizing, has saved cost; By the agitating device bottom the first crystallisation chamber, accelerate crystallization rate, also accelerate speed final material being cleared out room.
Accompanying drawing explanation
Fig. 1 is the structural representation of the subcrystalline crystallizer of the utility model two.
In figure: 1, the first crystallisation chamber; 2, charging aperture; 3, discharging opening; 4, stirring vane; 5, turning cylinder; 6, drive motors; 7, heating jacket; 8, device for monitoring temperature; 9, insulation jacket; 10, pipe fitting; 11, vavuum pump; 12; Second crystallisation chamber; 13, screen pack; 14, heating jacket; 15, device for monitoring temperature; 16; Discharging opening; 17, heat-insulation layer; 18, the interface of ultrasonic wave froth breaker; 19, the interface that concentration analyzer is slotting; 20, filter screen.
Detailed description of the invention
Below in conjunction with drawings and Examples, detailed description of the invention of the present utility model is further described.Following examples only for clearly the technical solution of the utility model being described, and can not limit protection domain of the present utility model with this.
As shown in Figure 1: the utility model is a kind of two subcrystalline crystallizers, and described equipment comprises the first crystallisation chamber 1, is arranged at the charging aperture 2 of the first crystallisation chamber 1 side, if as the discharging opening 3 bottom the first crystallisation chamber 1; The inwall of described first crystallisation chamber 1 is provided with heating jacket 7, first crystallisation chamber 1 outer wall is provided with heat-insulation layer 17 and device for monitoring temperature 8, the top of described first crystallisation chamber 1 is connected with vavuum pump 11 by pipe fitting 10, described pipe fitting 10 and the first crystallisation chamber 1 are seamlessly coordinate and stretch into the inner chamber of the first crystallisation chamber 1, be provided with in the end of described pipe fitting 10 and hide when the filter screen 20 of foam, be also provided with the interface 19 that the interface 18 of ultrasonic wave froth breaker and concentration analyzer are inserted at the top of described first crystallisation chamber 1; The output of described vavuum pump 11 is connected with the second crystallisation chamber 12 by pipe fitting 10, is provided with screen pack 13 below the charge door of described second crystallisation chamber 12, and the inwall of the second crystallisation chamber 12 is provided with heating jacket 14 and the outer wall of the second crystallisation chamber is provided with device for monitoring temperature 15.The waste liquid that vavuum pump 11 is extracted out enters the second crystallisation chamber 12 by pipe fitting 10, and first filter on screen pack 13, to remove the impurity in waste liquid, filtrate carries out crystallization again in the cavity of the second crystallisation chamber 12, clears out after crystallization completely from discharging opening 16.
The preferred embodiment of the utility model is, described screen pack is 13 to be removable installed on the cross section of described second crystallisation chamber 12.
The preferred embodiment of the utility model also has, and the outer wall of described pipe fitting 1 is provided with insulation jacket 9.
The preferred embodiment of the utility model also has, agitating device is provided with bottom described first crystallisation chamber 1, described agitating device comprises the drive motors 6 being located at the first crystallisation chamber 1 outside, and the turning cylinder 5 controlled by drive motors 6 is fixed on the stirring vane 4 on turning cylinder 5; The sidewall that described turning cylinder 5 passes the brilliant room 1 of knot first stretches into the inner chamber of the first crystallisation chamber 1, and the length that turning cylinder 5 stretches in the first crystallisation chamber 1 is equal with the diameter length of the first crystallisation chamber 1, and turning cylinder 5 is movably connected on the inwall of the first crystallisation chamber 1.
The above is only preferred embodiment of the present utility model; should be understood that; for those skilled in the art; under the prerequisite not departing from the utility model know-why; can also make some improvements and modifications, these improvements and modifications also should be considered as protection domain of the present utility model.
Claims (4)
1. two subcrystalline crystallizers, is characterized in that, described equipment comprises the first crystallisation chamber, are arranged at the charging aperture of the first crystallisation chamber side, if as the discharging opening bottom the first crystallisation chamber; The inwall of described first crystallisation chamber is provided with heating jacket, first crystallisation chamber outer wall is provided with heat-insulation layer and device for monitoring temperature, the top of described first crystallisation chamber is connected with vavuum pump by pipe fitting, described pipe fitting and the first crystallisation chamber are seamlessly coordinate and stretch into the inner chamber of the first crystallisation chamber, be provided with in the end of described pipe fitting and hide when the filter screen of foam, be also provided with the interface that the interface of ultrasonic wave froth breaker and concentration analyzer are inserted at the top of described first crystallisation chamber; Described vacuum delivery side of pump is connected with the second crystallisation chamber by pipe fitting, is provided with screen pack below the charge door of described second crystallisation chamber, and the inwall of the second crystallisation chamber is provided with heating jacket and the outer wall of the second crystallisation chamber is provided with device for monitoring temperature.
2. two subcrystalline crystallizers as claimed in claim 1, is characterized in that, described screen pack is be removable installed on the cross section of described second crystallisation chamber.
3. two subcrystalline crystallizers as claimed in claim 1, is characterized in that, the outer wall of described pipe fitting is provided with insulation jacket.
4. two subcrystalline crystallizers as claimed in claim 1, it is characterized in that, bottom described first crystallisation chamber, be provided with agitating device, described agitating device comprises the drive motors being located at the first crystallisation chamber outside, by the turning cylinder that drive motors controls, be fixed on the stirring vane on turning cylinder; Described turning cylinder stretches into the first crystallisation chamber inner chamber through knot first brilliant room sidewall, and the length that turning cylinder stretches into the first crystallization chamber is equal with the diameter length of the first crystallisation chamber, and turning cylinder is movably connected on the inwall of the first crystallisation chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520409446.XU CN204841003U (en) | 2015-06-15 | 2015-06-15 | Two subcrystalline crystallization equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520409446.XU CN204841003U (en) | 2015-06-15 | 2015-06-15 | Two subcrystalline crystallization equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204841003U true CN204841003U (en) | 2015-12-09 |
Family
ID=54731602
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520409446.XU Expired - Fee Related CN204841003U (en) | 2015-06-15 | 2015-06-15 | Two subcrystalline crystallization equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204841003U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842864A (en) * | 2021-10-19 | 2021-12-28 | 万强强 | Quinone natural product extraction equipment capable of performing crystallization extraction on waste liquid |
-
2015
- 2015-06-15 CN CN201520409446.XU patent/CN204841003U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842864A (en) * | 2021-10-19 | 2021-12-28 | 万强强 | Quinone natural product extraction equipment capable of performing crystallization extraction on waste liquid |
| CN113842864B (en) * | 2021-10-19 | 2023-12-15 | 沛县宗赢工程机械制造有限公司 | Quinone natural product extraction equipment capable of crystallizing and extracting waste liquid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151209 Termination date: 20160615 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |