CN203677988U - Crystallization device - Google Patents
Crystallization device Download PDFInfo
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- CN203677988U CN203677988U CN201420072065.2U CN201420072065U CN203677988U CN 203677988 U CN203677988 U CN 203677988U CN 201420072065 U CN201420072065 U CN 201420072065U CN 203677988 U CN203677988 U CN 203677988U
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- tank body
- crystallization
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- crystallization tank
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Abstract
The utility model relates to chemical equipment, and in particular relates to a crystallization device. The crystallization device comprises a crystallization tank body, a material inlet formed in one side surface of the crystallization tank body, and a material outlet formed in the bottom of the crystallization tank body; the inner wall of the crystallization tank body is provided with a heating sleeve; the outer wall of the crystallization tank body is provided with a temperature monitoring device; the top of the crystallization tank body is connected with a vacuum pump through a pipe fitting; the pipe fitting is in seamless fit with the crystallization tank body and extends into an inner cavity of the crystallization tank body; the output end of the vacuum pump is connected with a second tank body through a pipe fitting; a filter device is arranged below a feeding opening of the second tank body; the inner wall of the second tank body is provided with a heating sleeve and the outer wall of the second tank body is provided with a temperature monitoring device. Due to the adoption of the structure, the crystallization tank body is vacuumized, the output end of the vacuum pump is connected with the second tank body, waste materials generated by that the crystallization tank body is vacuumized are fully utilized, and the cost is saved; through a stirring device arranged on the bottom of the crystallization tank body, the crystallization speed is increased, and the speed of cleaning a final material out of the tank body is also increased.
Description
Technical field
The utility model relates to a kind of chemical industry equipment, particularly a kind of crystallization apparatus.
Background technology
Crystallization is one of most important link in chemical products production process, and crystallization apparatus is also one of most widely used equipment in Chemical Manufacture.Crystallizer of the prior art is often by vacuumizing to improve the efficiency of crystallization, but after exhausting vacuum, the waste liquid of extraction can directly be given up conventionally, has caused great waste.
Utility model content
The utility model technical issues that need to address are to provide a kind of energy and realize the device that vacuumizes rear extraction waste material while recycling crystallization process.
The utility model is achieved through the following technical solutions: comprise crystallization tank body, be located at the charging aperture of crystallizing tank body side surface, be located at the discharging opening of crystallization tank base; Described crystallization inner tank wall is provided with heating jacket, and crystallization tank wall is provided with device for monitoring temperature; Described crystallization tank body top is connected with vavuum pump by pipe fitting, and described pipe fitting and crystallization tank body are seamlessly coordinate and stretch into crystallizing tank intracoelomic cavity; Described vacuum delivery side of pump is connected with the second tank body by pipe fitting, and the charge door below of described the second tank body is provided with filter, and the second inner tank wall is provided with heating jacket and the second tank wall is provided with device for monitoring temperature.
Further, described filter is for being removable installed on described the second tank body cross section.
Further, described pipe fitting outer wall is provided with insulation jacket.
Further, described crystallization tank base is provided with agitating device, and described agitating device comprises the motor of being located at crystallizing tank external body, by the turning cylinder of Electric Machine Control, is fixed on the stirring vane on turning cylinder; Described turning cylinder stretches into crystallizing tank intracoelomic cavity through crystallizing tank body sidewall, and the length that turning cylinder stretches in crystallization tank body equates with the diameter length of crystallization tank body, and turning cylinder is movably connected on crystallization inner tank wall.
The beneficial effect that the utility model brings is: by crystallization tank body is vacuumized, vacuum delivery side of pump is being connected in to the second tank body, is taking full advantage of the waste material after vacuumizing, saving cost; By the agitating device of crystallization tank base, accelerate crystallization rate, also accelerate final material to clear out the speed of tank body.
Brief description of the drawings
Below in conjunction with accompanying drawing, the utility model is described in further detail.
Fig. 1 is the structural representation of a kind of crystallization apparatus of the utility model.
The label that in figure, component names is corresponding is as follows:
1 is crystallization tank body, and 2 is charging aperture, and 3 is discharging opening, 4 is stirring vane, and 5 is turning cylinder, and 6 is motor, 7 is heating jacket, and 8 is device for monitoring temperature, and 9 is insulation jacket, 10 is pipe fitting, and 11 is vavuum pump, and 12 is the second tank body, 13 is filter, 14 is heating jacket, and 15 is device for monitoring temperature, and 16 is discharging opening
Detailed description of the invention
Below in conjunction with drawings and Examples, the utility model is described in further detail:
As the embodiment of a kind of crystallization apparatus of the utility model, as shown in Figure 1, a kind of crystallizer of the present utility model comprises crystallization tank body 1, is located at the charging aperture 2 of crystallization tank body 1 side, is located at the discharging opening 3 of crystallization tank body 1 bottom; Described crystallization tank body 1 inwall is provided with heating jacket 7, and crystallization tank body 1 outer wall is provided with device for monitoring temperature 8; Described crystallization tank body 1 top is connected with vavuum pump 11 by pipe fitting 10, and described pipe fitting 10 and crystallization tank body 1 coordinates and stretch into crystallization tank body 1 inner chamber for seamless; The output of described vavuum pump 11 is connected with the second tank body 12 by pipe fitting, and the charge door of described the second tank body 12 below is provided with that filter 13, the second tank body 12 inwalls are provided with heating jacket 14 and the second tank body 12 outer walls are provided with device for monitoring temperature 15.When crystallization work, start heating jacket 7 and heat, vavuum pump 11 vacuumizes crystallization tank body 1, has greatly improved the speed of crystallization; Temperature during due to some material crystallization is unsuitable too high, otherwise self component can change, and the temperature in 1 in device for monitoring temperature 8 monitoring crystallization in real time tank body, in the time reaching the temperature of predetermined set, enters thermostatic control pattern.The waste liquid that vavuum pump 11 is extracted out enters the second tank body 12 by pipe fitting, first on filter 13, filters, and to remove the impurity in waste liquid, filtrate is carried out crystallization again in the second tank body 12 cavitys, after crystallization completely, clears out from discharging opening 16.
Further, described filter 13 is for being removable installed on described the second tank body 12 cross sections, and such design can change adaptively for the impurity size likely occurring the aperture of filter 12, makes equipment have stronger usability.
Further, described pipe fitting 10 outer walls are provided with insulation jacket 9, and such design makes the waste liquid of extracting out can continue original temperature, provide smoothly guarantee for next step crystallization.
Further, described crystallization tank body 1 bottom is provided with agitating device, and described agitating device comprises the motor 6 of being located at crystallizing tank external body, and the turning cylinder 5 of controlling by motor 6 is fixed on the stirring vane 4 on turning cylinder 5; Described turning cylinder stretches into crystallization tank body 1 inner chamber through crystallization tank body 1 sidewall, and the length that turning cylinder 5 stretches in crystallization tank body 1 equates with the diameter length of crystallization tank body 1, and turning cylinder 5 is movably connected on crystallization tank body 1 inwall.When crystallization work, open motor 6, motor 6 drives turning cylinder 5 to rotate, and turning cylinder 5 and then drive stirring vane 4 rotate, and stirring vane 4 constantly stirs the material in tank body, has greatly improved the crystallization rate of material.When discharging, open agitating device, material, under stirring vane 4 drives, moves toward discharging opening 3 hastily, has improved production efficiency.
Further, the material of described stirring vane 4 is acidproof resistant material, and chemical products generally have certain Acidity of Aikalinity, like this design raising the service life of stirring vane 4.
Claims (4)
1. a crystallization apparatus, comprises crystallization tank body, is located at the charging aperture of crystallizing tank body side surface, is located at the discharging opening of crystallization tank base; Described crystallization inner tank wall is provided with heating jacket, and crystallization tank wall is provided with device for monitoring temperature, it is characterized in that: described crystallization tank body top is connected with vavuum pump by pipe fitting, and described pipe fitting and crystallization tank body are seamlessly coordinate and stretch into crystallizing tank intracoelomic cavity; Described vacuum delivery side of pump is connected with the second tank body by pipe fitting, and the charge door below of described the second tank body is provided with filter, and the second inner tank wall is provided with heating jacket and the second tank wall is provided with device for monitoring temperature.
2. a kind of crystallization apparatus as claimed in claim 1, is characterized in that: described filter is for being removable installed on described the second tank body cross section.
3. a kind of crystallization apparatus as claimed in claim 1, is characterized in that: described pipe fitting outer wall is provided with insulation jacket.
4. a kind of crystallization apparatus as claimed in claim 1, is characterized in that: described crystallization tank base is provided with agitating device, and described agitating device comprises the motor of being located at crystallizing tank external body, by the turning cylinder of Electric Machine Control, is fixed on the stirring vane on turning cylinder; Described turning cylinder stretches into crystallizing tank intracoelomic cavity through crystallizing tank body sidewall, and the length that turning cylinder stretches in crystallization tank body equates with the diameter length of crystallization tank body, and turning cylinder is movably connected on crystallization inner tank wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420072065.2U CN203677988U (en) | 2014-02-19 | 2014-02-19 | Crystallization device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420072065.2U CN203677988U (en) | 2014-02-19 | 2014-02-19 | Crystallization device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203677988U true CN203677988U (en) | 2014-07-02 |
Family
ID=50999953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420072065.2U Expired - Fee Related CN203677988U (en) | 2014-02-19 | 2014-02-19 | Crystallization device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203677988U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105664522A (en) * | 2016-03-25 | 2016-06-15 | 刘云海 | Chemical experiment efficient crystallization device |
| CN106699488A (en) * | 2017-03-16 | 2017-05-24 | 中国工程物理研究院化工材料研究所 | Explosive recrystallization preparation method and device for explosive crystallization |
| CN108671578A (en) * | 2018-05-10 | 2018-10-19 | 江苏鼎烨药业有限公司 | One kind having impurity-eliminating effect and 2,4 dichloro phenol concentration and crystallization device easy to operation |
| CN109280023A (en) * | 2018-12-04 | 2019-01-29 | 河北美邦工程科技股份有限公司 | A kind of caprolactam continuous crystallisation purification process |
-
2014
- 2014-02-19 CN CN201420072065.2U patent/CN203677988U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105664522A (en) * | 2016-03-25 | 2016-06-15 | 刘云海 | Chemical experiment efficient crystallization device |
| CN106699488A (en) * | 2017-03-16 | 2017-05-24 | 中国工程物理研究院化工材料研究所 | Explosive recrystallization preparation method and device for explosive crystallization |
| CN106699488B (en) * | 2017-03-16 | 2018-08-14 | 中国工程物理研究院化工材料研究所 | A kind of explosive recrystallization preparation method and the device for explosive crystallization |
| CN108671578A (en) * | 2018-05-10 | 2018-10-19 | 江苏鼎烨药业有限公司 | One kind having impurity-eliminating effect and 2,4 dichloro phenol concentration and crystallization device easy to operation |
| CN109280023A (en) * | 2018-12-04 | 2019-01-29 | 河北美邦工程科技股份有限公司 | A kind of caprolactam continuous crystallisation purification process |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140702 Termination date: 20150219 |
|
| EXPY | Termination of patent right or utility model |