CN206204260U - A kind of natural perfume material Preparation equipment - Google Patents
A kind of natural perfume material Preparation equipment Download PDFInfo
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- CN206204260U CN206204260U CN201620395325.9U CN201620395325U CN206204260U CN 206204260 U CN206204260 U CN 206204260U CN 201620395325 U CN201620395325 U CN 201620395325U CN 206204260 U CN206204260 U CN 206204260U
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- natural perfume
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Abstract
The utility model discloses a kind of natural perfume material Preparation equipment, it is related to natural perfume material preparation field, is used to realize the multiple batches of or continuous preparation of natural perfume material.The device includes extractor, heat exchange structure and oil water separator；First passage is formed between the outlet of oil water separator and the entrance of extractor, second channel is formed between the outlet of heat exchange structure and the entrance of extractor.Wherein, first passage and second channel can select a conducting.When first passage conducting, during the fluid of extractor output can flow to extractor via heat exchange structure, oil water separator, first passage；When second channel conducting, during the fluid of extractor output can flow to extractor via heat exchange structure, second channel.Above-mentioned technical proposal provides the continuous extraction that can realize plants essential oil and tincture.
Description
Technical field
The utility model is related to natural plants to prepare natural perfume material field, and in particular to a kind of natural perfume material Preparation equipment.
Background technology
Pretreatment procedure, abstraction process, cold is generally comprised with the technological process that natural plants prepare natural perfume material as raw material
Solidifying operation and concentrating and separating operation etc., in natural perfume material production, need to according to the actual requirements select suitable technological process, but its
Condensation procedure is easily ignored due to its function phase to single.
In preparation and production method, steam distillation and solvent extraction method are conventional preparations to vegetal natural perfume
The method of essential oil and medicinal extract.Be passed through water vapour in the extractor of natural plant raw material by prior art, and volatile ingredient steams with water
Steam distillation out, essential oil is prepared by condenser system into separation in oil water separator.Solvent is added to natural plants former
Extraction, concentration are carried out in the extractor of material and prepares medicinal extract.
Inventor has found at least there are following problems in the prior art：Current prepares the natural perfume materials such as essential oil and medicinal extract
In the traditional handicraft of production, steam distillation prepare essential oil technical process be generally the condensed operation of steam containing essential oil condense to
By oil water separator, certain liquid level is kept by the U-shaped design of oil water separator, in lower floor's condensate return to extractor,
Upper strata oil reservoir is released after end to be distilled and is essential oil.According to process requirements, the natural plants in extractor use extraction
Method carries out down one solvent extraction process.But, this traditional handicraft is due to only having simple condensation procedure path, it is impossible to carry out
Steam distillation -- solvent refluxing extraction coupled method realizes that the continuous extraction of natural plants prepares the natural perfume materials such as essential oil and medicinal extract
Complex processing requirements, lack necessary flexibility.Due to preparing the traditional handicraft of the natural perfume materials such as essential oil and medicinal extract production at present
Unitary function, it is impossible to meet the natural perfume materials such as essential oil and medicinal extract and flexibly continuously produce industrialization demand.
Utility model content
One of purpose of the present utility model is to propose a kind of natural perfume material Preparation equipment, is used to realize natural perfume material
It is continuous to prepare.
To achieve the above object, the utility model provides following technical scheme：
The utility model provides a kind of natural perfume material Preparation equipment, including extractor, heat exchange structure and oil water separator；
Be formed with first passage between the entrance of the outlet of the oil water separator and the extractor, the outlet of the heat exchange structure and
Second channel is formed between the entrance of the extractor；
Wherein, the first passage and the second channel can select a conducting；When first passage conducting, the extraction
During the fluid of tank output can flow to the extractor via the heat exchange structure, the oil water separator, the first passage；When
The second channel conducting, the fluid of the extractor output can be described via the heat exchange structure, second channel flow direction
In extractor.
In an alternate embodiment of the invention, the first passage is connected with for preventing the oil water separator from siphonage occur
Emptying pipeline, the emptying pipeline can turn on；There is the natural perfume material of part and the oil water separator in the first passage
The height such as outlet.
In an alternate embodiment of the invention, the heat exchange structure includes First Heat Exchanger, the second heat exchanger and the 3rd heat exchanger；
The outlet of the First Heat Exchanger is connected with the entrance of the 3rd heat exchanger, the outlet of the 3rd heat exchanger with
The oil water separator is connected with the second channel；
Entrance of the outlet of the 3rd heat exchanger also with second heat exchanger is connected, the outlet of second heat exchanger
Can be normally opened.
In an alternate embodiment of the invention, the first passage is provided with the 4th control valve and the 5th control valve, the emptying pipeline
First end be connected to the first passage positioned at the described 4th control valve and it is described 5th control valve between part, the row
Second end of vacant duct is connected by the 8th control valve, the first control valve with the entrance of second heat exchanger.
In an alternate embodiment of the invention, it is provided with the between the outlet of the 3rd heat exchanger and the entrance of the oil water separator
The 6th control valve is provided between the entrance of seven control valves, the outlet of the 3rd heat exchanger and the 5th control valve.
In an alternate embodiment of the invention, natural perfume material is plants essential oil or tincture；When the natural perfume material Preparation equipment is used to plant
Thing extraction of essential oil is operated, the first passage conducting；Operation, described second are extracted when the natural perfume material Preparation equipment is used for tincture
Channel conductive.
In an alternate embodiment of the invention, when the natural perfume material Preparation equipment is used for plants essential oil or tincture extracts operation, emptying
Pipeline is all in conducting state.
In an alternate embodiment of the invention, the outlet of second heat exchanger is provided with the exhaust-valve of emptying.
Based on above-mentioned technical proposal, the utility model embodiment can at least produce following technique effect：
Natural perfume material is plants essential oil or tincture.The outlet of the extractor of natural perfume material Preparation equipment and heat exchange structure
Entrance is connected, and the outlet of heat exchange structure is connected with the entrance of oil water separator and the entrance of extractor simultaneously, is so tied in heat exchange
Second channel is formd between the outlet of structure and the entrance of extractor, between the outlet of oil water separator and the entrance of extractor
Form first passage.Whole natural perfume material Preparation equipment can form two loops：First loop allows fluid under
Stating flow direction is carried out：Extractor → heat exchange structure → oil water separator → extractor, this primary Ioops are used to extract plants essential oil.Second
Bar loop allows that fluid is carried out according to following flow directions：Extractor → heat exchange structure → extractor, this primary Ioops are used to extract
Tincture.
It can be seen that, the natural perfume material Preparation equipment that above-mentioned technical proposal is provided can realize that plants essential oil and the continuous of tincture are carried
Take.
Brief description of the drawings
Accompanying drawing described herein is used for providing being further understood to of the present utility model, constitutes the part of the application,
Schematic description and description of the present utility model is used to explain the utility model, does not constitute to of the present utility model improper
Limit.In the accompanying drawings：
The principle schematic of the natural perfume material Preparation equipment that Fig. 1 is provided for the utility model embodiment；
The natural perfume material preparation method schematic flow sheet that Fig. 2 is provided for another embodiment of the utility model；
The natural perfume material preparation method schematic flow sheet that Fig. 3 is provided for the another embodiment of the utility model；
The natural perfume material preparation method schematic flow sheet that Fig. 4 is provided for the utility model another embodiment.
Reference：
1st, extractor；3rd, oil water separator；21st, First Heat Exchanger；22nd, the second heat exchanger；23rd, the 3rd heat exchanger；4th,
One passage；5th, pipeline is emptied；6th, second channel；V1, the first control valve；V2, the second control valve；V3, the 3rd control valve；V4,
Four control valves；V5, the 5th control valve；V6, the 6th control valve；V7, the 7th control valve；V8, the 8th control valve.
Specific embodiment
The technical scheme that the utility model is provided is illustrated in more detail with reference to Fig. 1 to Fig. 4.
The utility model embodiment provides a kind of natural perfume material Preparation equipment, including extractor 1, heat exchange structure and profit point
From device 3.It is formed with first passage 4 between the outlet of oil water separator 3 and the entrance of extractor 1, the outlet of heat exchange structure and carries
Second channel 6 is formed between the entrance for taking tank 1；Wherein, first passage 4 and second channel 6 can select a conducting.Work as first passage
4 conductings, during the fluid of the output of extractor 1 can flow to extractor 1 via heat exchange structure, oil water separator 3, first passage 4.When
Two passages 6 are turned on, during the fluid of the output of extractor 1 can flow to extractor 1 via heat exchange structure, second channel 6.
Natural perfume material is plants essential oil or tincture.The outlet of the extractor 1 of natural perfume material Preparation equipment and heat exchange structure
Entrance connection, heat exchange structure outlet simultaneously connected with the entrance of oil water separator 3 and the entrance of extractor 1, so changing
Second channel 6 is formd between the outlet of heat structure and the entrance of extractor 1, in outlet and the extractor 1 of oil water separator 3
First passage 4 is formed between entrance.Whole natural perfume material Preparation equipment can form two loops：First loop causes that fluid can
Carried out with according to following flow directions：1 → heat exchange structure of extractor → 3 → extractor of oil water separator 1, this primary Ioops is used to extract plants
Thing essential oil.Article 2 loop allows that fluid is carried out according to following flow directions：1 → heat exchange structure of extractor → extractor 1, this
Loop is used to extract tincture.
It can be seen that, the natural perfume material Preparation equipment that above-mentioned technical proposal is provided can realize that plants essential oil and the continuous of tincture are carried
Take.
Referring to Fig. 1, heat exchange structure includes First Heat Exchanger 21, the second heat exchanger 22 and the 3rd heat exchanger 23.First heat exchange
The outlet of device 21 is connected with the entrance of the 3rd heat exchanger 23, outlet and oil water separator 3 and the second channel 6 of the 3rd heat exchanger 23
Connection.Entrance of the outlet of the 3rd heat exchanger 23 also with the second heat exchanger 22 is connected, and the outlet of the second heat exchanger 22 can be normally opened.The
Two heat exchangers 22 are used to condense not by the steam of the total condensation of the 3rd heat exchanger 23, and cause that condensed liquid enters via steam
Flow out on Kou Yuan roads.
Referring to Fig. 1, the emptying pipeline 5 for preventing oil water separator 3 from siphonage occur is connected with the first pipeline 4,
Emptying pipeline 5 can be turned on.There is the height such as part and natural perfume material outlet of oil water separator 3 in first passage 4.Can so make
Pressure is equal with pressure at the natural perfume material outlet of oil water separator 3 in obtaining first passage 4, can prevent siphonage,
And realize the multiple extraction of natural perfume material.
When individually using above-mentioned first loop, can repeatedly to plant is added in extractor 1, to realize plants essential oil
Multiple batches of extraction；When individually using above-mentioned Article 2 loop, can repeatedly to plant is added in extractor 1, to realize tincture
Multiple batches of extraction.It is understood that the extraction behaviour of one or more batches of plants essential oil can be completed using the first loop
After work, then the extraction that tincture is carried out using second servo loop.Or, carrying out a batch or multiple batches of essential oil using the first loop
After extraction, using second servo loop, the different extractant of single or multiple additions, to realize the multiple extraction of natural perfume material.
It can be seen that, the natural perfume material Preparation equipment that above-mentioned technical proposal is provided can realize that plants essential oil and the continuous of tincture are carried
Take, and the multiple extraction of plants essential oil, tincture can be realized.
Referring to Fig. 1, the on or off of first passage 4 can be controlled using some control valves, it is specific as follows：First leads to
Road 4 is provided with the 4th control valve V4 and the 5th control valve V5, and the first end for emptying pipeline 5 is connected to first passage 4 positioned at the 4th control
Part between the control valves of valve V4 processed and the 5th V5, empties the second end of pipeline 5 by the 8th control valve V8, the first control valve V1
Entrance with the second heat exchanger 22 is connected.4th control valve V4, the 5th control valve V5 are both turned on, then first passage 4 is turned on.
Referring to Fig. 1, similarly, the on or off of second channel 6 can be controlled using some control valves, it is specific as follows：
The 7th control valve V7, the outlet of the 3rd heat exchanger 23 are provided between the outlet of the 3rd heat exchanger 23 and the entrance of oil water separator 3
The 6th control valve V6 is provided with and the entrance of the 5th control valve V5 between.5th control valve V5, the 6th control valve V6 are both turned on, then and the
Two passages 6 are turned on.
Hold above-mentioned, natural perfume material is plants essential oil or tincture.When the natural perfume material Preparation equipment is extracted for plants essential oil
Operation, first passage 4 is turned on, and the fluid of the output of extractor 1 can be flowed to via heat exchange structure, oil water separator 3, first passage 4
In extractor 1.Operation is extracted when the natural perfume material Preparation equipment is used for tincture, second channel 6 is turned on, the stream of the output of extractor 1
Physical efficiency is flowed in extractor 1 via heat exchange structure, second channel 6.
Further, when the natural perfume material Preparation equipment is used for plants essential oil or tincture extracts operation, emptying pipeline 5 is all located
In conducting state.Can so avoid extraction from siphonage occur in operating, be conducive to carrying out repeatedly continuous extraction.
Referring to Fig. 1, the outlet of the second heat exchanger 22 is provided with the exhaust-valve 24 of emptying.When tincture extraction operation is carried out,
The gas of the non-total condensation of the 3rd heat exchanger 23 returns to the second heat exchanger 22 possibly through the pipeline where the first control valve V1
In.Second heat exchanger 22 can again carry out condensation operation, and will condense the liquid backtracking for being formed, by by the 6th control valve
V6 flows into extractor 1.
A specific embodiment is described below.
As shown in figure 1, the natural perfume material Preparation equipment that the utility model embodiment is provided includes that extractor 1, extractor 1 are pressed from both sides
Set steam-heating apparatus, the straight-through steam-heating apparatus in the bottom of extractor 1, First Heat Exchanger 21, the second heat exchanger the 22, the 3rd exchange heat
Device 23, oil water separator 3 and pipe valve V1-V8.
The operation for using the device to be extracted (by taking natural perfume material as an example, needs first to be added in extractor 1 before including operation
Natural plants), each road heating and thermal insulation situation of check device and instrument show and control situation, material situation.Confirmation has no problem
Afterwards, opening controlling valve V1, V4, V7, V5 and V8；Closing control valve V2, V3 and V6；Open jacket steam heater block and bottom is straight
Logical steam heater block carries out steam distillation.Steam is condensed by heat exchange structure and enters oil water separator 3, by water-oil separating
After the U-shaped balanced design of device 3, oil water separator 3 keeps certain liquid, in condensate return to extractor 1.Each parameter stability fortune
Go to after required time, oil reservoir can obtain essential oil product in collecting oil water separator 3.Next, add extracting molten to extractor 1
Matchmaker, opening controlling valve V1, V5, V6 and V8, closing each control valve V2, V3, V4 and V7 carries out plant solvent extraction, and according to parameter
After the time required to setting operation, discharge plant extraction liquid enters next process, releases natural plants residue.In extractor 1
New a collection of natural plants are again loaded into, and continue operation, produce next group product.
Specifically, the method extracted using above-mentioned natural perfume material Preparation equipment is as follows：
Step one：Natural plants are fitted into extractor 1.
In above-mentioned steps one, the mass percent that can add appropriate water, addition to extractor 1 in advance as needed is
The 0-50% of natural plants quality.
Step 2：Opening controlling valve V1, V4, V7, V5 and V8；Closing control valve V2, V3 and V6.Material is thus formed above-mentioned
First loop, and opened on the loop the 8th control valve V8, siphonage can be prevented.
Step 3：Start jacket steam firing equipment, after preheating reaches the temperature of setting, can be opened according to process requirements and carried
The straight-through steam-heating apparatus in the bottom of tank 1 is taken, after water vapour steams liquid condensing to oil water separator 3, keeps certain by U-shaped design
Liquid level, condensate return to extractor 1.
In above-mentioned steps three, start the jacket steam firing equipment of extractor 1, its steam valve aperture is 100-0%, preheating
Temperature is 80-100 DEG C；According to process requirements, the straight-through steam heater in bottom can be opened, its steam valve aperture is 10-
40%；Water vapour distillate condensation flow can be controlled in 10Kg-60Kg/ hours.
Step 4：After running a period of time under conditions of above-mentioned steps two and step 3, oil is formed in oil water separator 3
Layer, steam off heating system is collected in oil water separator 3 essential oil or builds up to subsequent batches one by the second control valve V2
Rise and collect.
In above-mentioned steps three, run time can be at 2-8 hours according to process requirements；If oil reservoir is thicker, can be by opening
Oil reservoir obtains essential oil product during V2 valves collect oil water separator 3；If oil reservoir is relatively thin, oil reservoir can not be collected, treat second batch or
Many batches multiple batches of when building up to compared with thick oil pay to collect together.
Above-mentioned steps one to step 4 is plants essential oil abstraction process.
Step 5：A certain amount of extraction solvent is added into extractor 1.
In above-mentioned steps five, it can be water, ethyl acetate, 5-95% ethanol etc. to extract solvent；Its quality is natural plants
3-15 times.
Step 6：Opening controlling valve V1, V5, V6 and V8, closing control valve V2, V3, V4 and V7 valve, material is thus formed
Above-mentioned Article 2 loop.
Step 7：Start the jacket steam firing equipment of extractor 1, after reaching the temperature of setting, solvent condensate liquid is by the
Six control valve V6 and the 5th control valve V5 condensing refluxes to extractor 1.
In above-mentioned steps seven, according to processing parameter setting, its steam heating valve opening is 0-100%；Its temperature range
Can be room temperature-solvent boiling point (such as solvent water, its temperature range can be -100 DEG C of room temperature)；Solvent condensate liquid condensation flow can be 0-
80Kg/ hours.
Step 8：After running a period of time under conditions of above-mentioned steps six and step 7, steam off heating system is adopted
The operation extracted with solvent terminates, and natural botanical extraction liquid is discharged into next process by pump.
In above-mentioned steps eight, its time range can be 0.5-4 hours.
Above-mentioned steps five to step 8 is tincture abstraction process.Tincture abstraction process is not necessarily intended to extract work in plants essential oil
After sequence, tincture abstraction process can be used alone.
Step 9：Natural plants residue in discharge extractor 1, continuously adds the natural plants of next group.
Step 10：Two-step 8 of repeat step, is capable of achieving multiple batches of essential oil one or many and collects.
It can be seen that the natural perfume material Preparation equipment that above-mentioned technical proposal is provided, valve opening or closing using V1-V8, form
Two kinds of different condensate liquid reflux techniques, are capable of achieving to switch over as needed to realize single batch or multiple batches of continuous production,
Good actual effect can be obtained in production.Simultaneously as devising the 8th control valve V8, it is possible to resolve due to oil water separator 3
U-shaped design technology exist siphonic effect cause oil water separator 3 in oil-water mixture while being back in extractor 1 and receiving
Collect the defective workmanship less than essential oil.
Referring to Fig. 2, another embodiment of the utility model provides a kind of natural perfume material preparation method, comprises the following steps：
Step 10, the first passage of the natural perfume material Preparation equipment for being provided any technical scheme of the utility model are led
It is logical；
Step 20, prepare plants essential oil according to plants essential oil abstraction process.Plants essential oil abstraction process described herein can
With using plants essential oil abstraction process described above.
Herein, the emptying pipeline 5 of the natural perfume material Preparation equipment is turned on, can at least repeat step 20 be twice.By institute
The conducting of emptying pipeline 5 for stating natural perfume material Preparation equipment can be prevented effectively from siphonage, in order to repeatedly extract plants essential oil.
Step 30, the second channel conducting by natural perfume material Preparation equipment；
Step 40, prepare tincture according to tincture abstraction process.Tincture abstraction process described herein can be used and is situated between above
The tincture abstraction process for continuing.
Herein, the emptying pipeline 5 of the natural perfume material Preparation equipment is turned on, can at least repeat step 40 be twice.By institute
The conducting of emptying pipeline 5 for stating natural perfume material Preparation equipment can be prevented effectively from siphonage, in order to repeatedly extract tincture.
Above-mentioned natural perfume material preparation method, using same complete equipment, can simultaneously realize the continuous of plants essential oil and tincture
Extract, repeatedly extract.
Several instantiations are described below.
Embodiment 1：The preparation of Sanming City Youxi essential oil of tobaccos and water extract
Sanming City Youxi tobacco leaf, using beating and double roasting rear panel cigarette, Fujian China Tobacco Industrial Co., Ltd.；Steam, Xiamen state
Can be with collection Thermal Power Co., Ltd.
According to the technological process of Fig. 1, by 20Kg Sanming City Youxi tobacco leaf heating extraction tank 1, opening controlling valve V1, V4, V7,
V5 and V8；Closing control valve V2, V3 and V6.Start the jacket steam firing equipment of extractor 1, valve opening 80%, design temperature
80℃.After reaching the temperature of setting, the straight-through steam heater in bottom, valve opening 30% are opened.Condensate liquid condensation flow can
It is 40Kg/ hours；After parameter stability, run time 4 hours.There is an oil reservoir in oil water separator 3, open second and control valve V2,
Collect essential oil product.
Then by 160Kg water add extractor 1 in, opening controlling valve V1, V5, V6 and V8, closing control valve V2, V3, V4
And V7.Start the jacket steam firing equipment of extractor 1, its valve opening is 60%, and design temperature is 100 DEG C, and condensation flow can
It is 60Kg/ hours；Run time is 2 hours, steam off heating system, and solvent is extracted and terminated, and tobacco leaf water extract passes through pump
It is discharged into entering next process in extraction liquid storage tank.
Finally discharge the tobacco leaf residue in extractor 1.
This embodiment 1 continuously prepares essential oil of tobaccos and water extract for single batch.
Embodiment 2：The preparation of essential oil of the flower of Camellia sinensis and alcohol extracting thing
Fresh Tea Flower, fresh harvesting Fujian Anxi Tieguanyin Tea tea hill；Steam, Xiamen state can be with collection Thermal Power Co., Ltd.
According to the technological process of Fig. 1, during the fresh Tea Flowers of 30Kg are added into extractor 1, opening controlling valve V1, V4, V7, V5
And V8；Closing control valve V2, V3 and V6.Start the jacket steam firing equipment of extractor 1, valve opening 60%, design temperature 60
℃.After reaching the temperature of setting, the straight-through steam heater in bottom, valve opening 20% are opened.Condensate liquid condenses flow
30Kg/ hours.After parameter stability, run time 6 hours.There is an oil reservoir in oil water separator 3.
Then in 95% ethanol of 140Kg being added into extractor 1, opening controlling valve V1, V5, V6 and V8, closing control valve
V2, V3, V4 and V7.Start the jacket steam firing equipment of extractor 1, its valve opening is 40%, and design temperature is 75 DEG C, condensation
Flow can be 20Kg/ hours.Run time is 2 hours, steam off heating system, and solvent is extracted and terminated, tobacco leaf alcohol extracting thing
It is discharged into entering next process in extraction liquid storage tank by pump.
Next the tobacco leaf residue in extractor 1 is discharged.
Above-mentioned each step operation can realize that single batch continuously prepares essential oil of the flower of Camellia sinensis and alcohol extracting thing.
Then by the fresh Tea Flower addition extractors 1 of 30Kg, repeat the above steps, the oil reservoir warp in oil water separator 3
After the accumulation of two batches, collection obtains essential oil product.
Embodiment 2 continuously prepares essential oil of the flower of Camellia sinensis and alcohol extracting thing for two batches.
Embodiment 3：It is prepared by tobacco leaf essential oil, alcohol extracting thing and water extract
Zimbabwe's tobacco leaf, using beating and double roasting rear panel cigarette, Fujian China Tobacco Industrial Co., Ltd.'s import；Steam, tall building
Men Guoneng is same to collect Thermal Power Co., Ltd.
According to the technological process of Fig. 1, by 20Kg Zimbabwe tobacco leaf heating extraction tank 1, opening controlling valve V1, V4, V7,
V5 and V8；Closing control valve V2, V3 and V6.Start the jacket steam firing equipment of extractor 1, valve opening 80%, design temperature
80℃.After reaching the temperature of setting, the straight-through steam heater in bottom, valve opening 30% are opened.Condensate liquid condensation flow can
It is 40Kg/ hours.After parameter stability, run time 4 hours；There are an oil reservoir, essential oil as to be extracted in oil water separator 3.
Then in 95% ethanol of 140Kg being added into extractor 1, opening controlling valve V1, V5, V6 and V8, closing control valve
V2, V3, V4 and V7.Start the jacket steam firing equipment of extractor 1, its valve opening is 60%, and design temperature is 100 DEG C, cold
Solidifying flow can be 60Kg/ hours.Run time be 2 hours, steam off heating system, tobacco leaf alcohol extracting thing by pump discharge into
Enter to extract liquid storage tank.
Next, by 180Kg water add extractor 1 in, opening controlling valve V1, V5, V6 and V8, closing control valve V2, V3,
V4 and V7.Start the jacket steam firing equipment of extractor 1, its valve opening is 55%, and design temperature is 96 DEG C, and condensation flow can
It is 50Kg/ hours.Run time is 2 hours, steam off heating system, and solvent is extracted and terminated, and tobacco leaf water extract passes through pump
It is discharged into extraction liquid storage tank.
Finally discharge the tobacco leaf residue in extractor 1.
This embodiment 3 continuously prepares essential oil, alcohol extracting thing and water extract for single batch.
Referring to Fig. 3, the another embodiment of the utility model provides a kind of natural perfume material preparation method, and it is comprised the following steps：
Step 50, the first passage of the natural perfume material Preparation equipment for being provided any technical scheme of the utility model are led
It is logical.
Step 60, prepare plants essential oil according to plants essential oil abstraction process.
Herein, the emptying pipeline 5 of the natural perfume material Preparation equipment is turned on, can at least repeat step 60 be twice.By institute
The conducting of emptying pipeline 5 for stating natural perfume material Preparation equipment can be prevented effectively from siphonage, in order to repeatedly extract plants essential oil.
Above-mentioned natural perfume material preparation method, using same complete equipment, can realize that plants essential oil is repeatedly extracted.
An instantiation is described below.
Embodiment 4：The preparation of multiple batches of tealeaves essential oil
Tealeaves, Fujian Anxi Tieguanyin Tea；Steam, Xiamen state can be with collection Thermal Power Co., Ltd.
According to the technological process of Fig. 1, during the fresh Tea Flowers of 25Kg are added into extractor 1, opening controlling valve V1, V4, V7, V5
And V8；Close V2, V3 and V6 valve；Start the jacket steam firing equipment of extractor 1, valve opening 55%, 55 DEG C of design temperature；
After reaching the temperature of setting, the straight-through steam heater in bottom, valve opening 25% are opened；Condensate liquid condenses flow
28Kg/ hours；After parameter stability, run time 6 hours；There is an oil reservoir in oil water separator 3；Tealeaves in discharge extractor 1
Residue.
Repeat the above steps, continuous production 6 batches, after the oil reservoir in oil water separator 3 is accumulated through six batches, collection obtains essence
Oil product.
This embodiment 4 continuously prepares tealeaves essential oil for multiple batches of.
Referring to Fig. 4, the utility model another embodiment provides a kind of natural perfume material preparation method, comprises the following steps：
Step 70, the second channel of the natural perfume material Preparation equipment for being provided any technical scheme of the utility model are led
It is logical；
Step 80, prepare tincture according to tincture abstraction process.
Herein, the emptying pipeline 5 of the natural perfume material Preparation equipment is turned on, can at least repeat step 80 be twice.By institute
The conducting of emptying pipeline 5 for stating natural perfume material Preparation equipment can be prevented effectively from siphonage, in order to repeatedly extract tincture.
In description of the present utility model, it is to be understood that term " " center ", " longitudinal direction ", " transverse direction ", "front", "rear",
The orientation or position relationship of the instruction such as "left", "right", " vertical ", " level ", " top ", " bottom ", " interior ", " outward " are based on accompanying drawing institute
The orientation or position relationship for showing, be only for ease of description the utility model and simplify describe, rather than indicate or infer meaning
Device or element must have specific orientation, be specific azimuth configuration and operation, thus it is not intended that to this practicality newly
Type protects the limitation of content.
Finally it should be noted that：Above example is only used to illustrate the technical solution of the utility model, rather than its limitations；
Although being described in detail to the utility model with reference to the foregoing embodiments, it will be understood by those within the art that：
It can still modify to the technical scheme described in foregoing embodiments, or which part technical characteristic is carried out etc.
With replacement, but these modifications or replacement, the essence of appropriate technical solution is departed from each embodiment technology of the utility model
The spirit and scope of scheme.
Claims (8)
1. a kind of natural perfume material Preparation equipment, it is characterised in that including extractor (1), heat exchange structure and oil water separator (3)；
First passage (4), the heat exchange knot are formed between the outlet of the oil water separator (3) and the entrance of the extractor (1)
Second channel (6) is formed between the entrance of the outlet of structure and the extractor (1)；
Wherein, the first passage (4) and the second channel (6) can select a conducting；When the first passage (4) conducting, institute
The fluid for stating extractor (1) output can be flowed to via the heat exchange structure, the oil water separator (3), the first passage (4)
In the extractor (1)；When the second channel (6) conducting, the fluid of extractor (1) output can be tied via the heat exchange
Structure, the second channel (6) are flowed in the extractor (1).
2. natural perfume material Preparation equipment according to claim 1, it is characterised in that the first passage (4) is connected with use
In preventing the oil water separator (3) from the emptying pipeline (5) of siphonage occur, emptying pipeline (5) can turn on；Described
There is part with the height such as the natural perfume material outlet of the oil water separator (3) in one passage (4).
3. natural perfume material Preparation equipment according to claim 2, it is characterised in that the heat exchange structure includes the first heat exchange
Device (21), the second heat exchanger (22) and the 3rd heat exchanger (23)；
The outlet of the First Heat Exchanger (21) is connected with the entrance of the 3rd heat exchanger (23), the 3rd heat exchanger (23)
Outlet connected with the oil water separator (3) and the second channel (6)；
Entrance of the outlet of the 3rd heat exchanger (23) also with second heat exchanger (22) is connected, second heat exchanger
(22) outlet can be normally opened.
4. natural perfume material Preparation equipment according to claim 3, it is characterised in that the first passage (4) is provided with the 4th
Control valve and the 5th control valve, the first end of the emptying pipeline (5) are connected to the first passage (4) positioned at the described 4th control
Part between valve processed and the 5th control valve, the second end of the emptying pipeline (5) is by the 8th control valve, the first control
Valve is connected with the entrance of second heat exchanger (22).
5. according to any described natural perfume material Preparation equipments of claim 3-4, it is characterised in that the 3rd heat exchanger (23)
Outlet and the entrance of the oil water separator (3) between be provided with the 7th control valve, the outlet of the 3rd heat exchanger (23) with
The 6th control valve is provided between the entrance of the 5th control valve.
6. according to any described natural perfume material Preparation equipments of claim 1-4, it is characterised in that natural perfume material is plants essential oil
Or tincture；Operation, first passage (4) conducting are extracted when the natural perfume material Preparation equipment is used for plants essential oil；When this is natural
Spices Preparation equipment is used for tincture and extracts operation, second channel (6) conducting.
7. natural perfume material Preparation equipment according to claim 6, it is characterised in that when the natural perfume material Preparation equipment is used for
Plants essential oil or tincture extract operation, and emptying pipeline (5) is all in conducting state.
8. according to any described natural perfume material Preparation equipments of claim 3-4, it is characterised in that second heat exchanger (22)
Outlet be provided with the exhaust-valve (24) of emptying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620395325.9U CN206204260U (en) | 2016-05-05 | 2016-05-05 | A kind of natural perfume material Preparation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620395325.9U CN206204260U (en) | 2016-05-05 | 2016-05-05 | A kind of natural perfume material Preparation equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206204260U true CN206204260U (en) | 2017-05-31 |
Family
ID=58756285
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620395325.9U Withdrawn - After Issue CN206204260U (en) | 2016-05-05 | 2016-05-05 | A kind of natural perfume material Preparation equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206204260U (en) |
-
2016
- 2016-05-05 CN CN201620395325.9U patent/CN206204260U/en not_active Withdrawn - After Issue
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