CN105907468A - Method and equipment for preparing natural perfume - Google Patents
Method and equipment for preparing natural perfume Download PDFInfo
- Publication number
- CN105907468A CN105907468A CN201610289681.7A CN201610289681A CN105907468A CN 105907468 A CN105907468 A CN 105907468A CN 201610289681 A CN201610289681 A CN 201610289681A CN 105907468 A CN105907468 A CN 105907468A
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- natural perfume
- perfume material
- material preparation
- preparation equipment
- heat exchanger
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a method and equipment for preparing natural perfume, and relates to the field of preparation of natural perfume. The natural perfume can be prepared in multiple batches or can be continuously prepared by the aid of the method and the equipment. The equipment comprises an extraction tank, a heat exchange structure and an oil and water separator. A first channel is formed between an outlet of the oil and water separator and an inlet of the extraction tank, and a second channel is formed between an outlet of the heat exchange structure and the inlet of the extraction tank. One of the first channel and the second channel can be selectively conducted. Fluid outputted from the extraction tank can flow back into the extraction tank via the heat exchange structure, the oil and water separator and the first channel when the first channel is conducted; the fluid outputted from the extraction tank can flow back into the extraction tank via the heat exchange structure and the second channel when the second channel is conducted. According to the technical scheme, the method and the equipment have the advantage that plant essential oil and tincture can be continuously extracted by the aid of the method and the equipment.
Description
Technical field
The present invention relates to natural plants and prepare natural perfume material field, be specifically related to a kind of natural perfume material
Preparation method and equipment.
Background technology
Pre-treatment work is generally comprised with the technological process that natural plants prepares natural perfume material for raw material
Sequence, abstraction process, condensation procedure and concentrating and separating operation etc., in natural perfume material produces, need
Select suitable technological process according to the actual requirements, but its condensation procedure is the most single due to its function
One is easily left in the basket.
Vegetal natural perfume is being prepared and in production method, steam distillation and extraction
Method is the conventional method preparing essential oil and medicinal extract.Water vapour is passed through natural plants by prior art
In the extractor of raw material, volatile ingredient with steam distillation out, is entered by condenser system
Oil water separator separates and prepares essential oil.Solvent is joined the extractor of natural plant raw material
In carry out extraction, medicinal extract is prepared in concentration.
Inventor finds, at least there is following problems in prior art: current prepare essential oil and
In the traditional handicraft that the natural perfume materials such as medicinal extract produce, steam distillation prepares essential oil technical process
Generally the condensed operation of the steam Han essential oil condense to after through oil water separator, pass through water-oil separating
The U-shaped design of device keeps certain liquid level, in lower floor's condensate return to extractor, knot to be distilled
Release upper strata oil reservoir after bundle and be essential oil.According to process requirements, the natural plants in extractor is adopted
Lower one solvent extraction process is carried out with solvent extraction method.But, this traditional handicraft is owing to only having
There is simple condensation procedure path, it is impossible to carry out steam distillation--solvent refluxing extraction coupled method
Realize natural plants extraction continuously and prepare the complex processing requirements of the natural perfume material such as essential oil and medicinal extract,
Lack necessary flexibility.Owing to preparing the tradition that the natural perfume material such as essential oil and medicinal extract produces at present
Process function is single, it is impossible to meets the natural perfume material such as essential oil and medicinal extract and produces industry the most continuously
Change demand.
Summary of the invention
One of them purpose of the present invention is to propose a kind of natural perfume material preparation method and equipment, uses
To realize the continuous preparation of natural perfume material.
For achieving the above object, the invention provides techniques below scheme:
The invention provides a kind of natural perfume material Preparation equipment, including extractor, heat exchange structure and
Oil water separator；It is formed between outlet and the entrance of described extractor of described oil water separator
First passage, is formed with second between outlet and the entrance of described extractor of described heat exchange structure
Passage；
Wherein, described first passage and described second channel can select a conducting；When described first leads to
Road turns on, and the fluid of described extractor output can be via described heat exchange structure, described water-oil separating
Device, described first passage flow in described extractor；When described second channel turns on, described in carry
The fluid taking tank output can flow to described extractor via described heat exchange structure, described second channel
In.
In an alternate embodiment of the invention, described first passage connects has for preventing described water-oil separating
Device occurs that the emptying pipeline of siphonage, described emptying pipeline can turn on；Described first passage is deposited
The height such as the natural perfume material outlet at part and described oil water separator.
In an alternate embodiment of the invention, described heat exchange structure includes First Heat Exchanger, the second heat exchanger
With the 3rd heat exchanger；
The outlet of described First Heat Exchanger connects with the entrance of described 3rd heat exchanger, and the described 3rd
The outlet of heat exchanger connects with described oil water separator and described second channel；
The outlet of described 3rd heat exchanger also entrance with described second heat exchanger connects, and described
The outlet of two heat exchangers can be normally opened.
In an alternate embodiment of the invention, described first passage is provided with the 4th control valve and the 5th control valve,
First end of described emptying pipeline is connected to described first passage and is positioned at described 4th control valve and institute
State the part between the 5th control valve, the second end of described emptying pipeline by the 8th control valve,
First control valve connects with the entrance of described second heat exchanger.
In an alternate embodiment of the invention, the outlet of described 3rd heat exchanger and described oil water separator
The 7th control valve, the outlet of described 3rd heat exchanger and described 5th control valve it is provided with between entrance
Entrance between be provided with the 6th control valve.
In an alternate embodiment of the invention, natural perfume material is plants essential oil or tincture；When this natural perfume material
Preparation equipment extracts operation for plants essential oil, and described first passage turns on；When this natural perfume material
Preparation equipment extracts operation for tincture, and described second channel turns on.
In an alternate embodiment of the invention, when this natural perfume material Preparation equipment is for plants essential oil or tincture
Extracting operation, emptying pipeline is all in conducting state.
In an alternate embodiment of the invention, the outlet of described second heat exchanger is provided with the exhaust-valve of emptying.
The embodiment of the present invention also provides for a kind of natural perfume material preparation method, comprises the following steps:
Step 10, the of the natural perfume material Preparation equipment that arbitrary for present invention technical scheme is provided
One channel conductive；
Step 20, prepare plants essential oil according to plants essential oil abstraction process；
Step 30, the second channel of described natural perfume material Preparation equipment is turned on；
Step 40, prepare tincture according to tincture abstraction process.
In an alternate embodiment of the invention, the emptying pipeline of described natural perfume material Preparation equipment is turned on,
At least repeat step 20 twice.
In an alternate embodiment of the invention, the emptying pipeline of described natural perfume material Preparation equipment is turned on,
At least repeat step 40 twice.
The present invention provides again a kind of natural perfume material preparation method, comprises the following steps:
Step 50, the of the natural perfume material Preparation equipment that arbitrary for present invention technical scheme is provided
One channel conductive；
Step 60, prepare plants essential oil according to plants essential oil abstraction process.
In an alternate embodiment of the invention, the emptying pipeline of described natural perfume material Preparation equipment is turned on,
At least repeat step 60 twice.
The present invention reoffers a kind of natural perfume material preparation method, comprises the following steps:
Step 70, the of the natural perfume material Preparation equipment that arbitrary for present invention technical scheme is provided
Two channel conductive；
Step 80, prepare tincture according to tincture abstraction process.
In an alternate embodiment of the invention, the emptying pipeline of described natural perfume material Preparation equipment is turned on,
At least repeat step 80 twice.
Based on technique scheme, the embodiment of the present invention at least can produce following technique effect:
Natural perfume material is plants essential oil or tincture.Going out of the extractor of natural perfume material Preparation equipment
Mouthful connect with the entrance of heat exchange structure, heat exchange structure the while of outlet with the entrance of oil water separator
Connect with the entrance of extractor, so shape between the outlet and the entrance of extractor of heat exchange structure
Become second channel, between the outlet and the entrance of extractor of oil water separator, formed first lead to
Road.Whole natural perfume material Preparation equipment can form two loops: Article 1 loop makes the fluid can
To carry out according to the following flow direction: extractor → heat exchange structure → oil water separator → extractor, this
Primary Ioops is used for extracting plants essential oil.Article 2 loop make fluid can according to following flow to into
OK: extractor → heat exchange structure → extractor, this primary Ioops is used for extracting tincture.
Visible, the natural perfume material Preparation equipment that technique scheme provides is capable of plants essential oil
Continuous extraction with tincture.
Accompanying drawing explanation
Accompanying drawing described herein is used for providing a further understanding of the present invention, constitutes the application
A part, the schematic description and description of the present invention is used for explaining the present invention, not structure
Become inappropriate limitation of the present invention.In the accompanying drawings:
The principle schematic of the natural perfume material Preparation equipment that Fig. 1 provides for the embodiment of the present invention；
The natural perfume material preparation method schematic flow sheet that Fig. 2 provides for another embodiment of the present invention；
The natural perfume material preparation method schematic flow sheet that Fig. 3 provides for further embodiment of this invention；
The natural perfume material preparation method schematic flow sheet that Fig. 4 provides for yet another embodiment of the invention.
Reference:
1, extractor；3, oil water separator；21, First Heat Exchanger；22, the second heat exchanger；
23, the 3rd heat exchanger；4, first passage；5, emptying pipeline；6, second channel；V1、
First control valve；V2, the second control valve；V3, the 3rd control valve；V4, the 4th control valve；
V5, the 5th control valve；V6, the 6th control valve；V7, the 7th control valve；V8, the 8th control
Valve processed.
Detailed description of the invention
The technical scheme provided the present invention below in conjunction with Fig. 1 to Fig. 4 is explained in more detail
State.
The embodiment of the present invention provides a kind of natural perfume material Preparation equipment, including extractor 1, heat exchange
Structure and oil water separator 3.Shape between outlet and the entrance of extractor 1 of oil water separator 3
Become to have first passage 4, between outlet and the entrance of extractor 1 of heat exchange structure, be formed with second
Passage 6；Wherein, first passage 4 and second channel 6 can select a conducting.When first passage 4
Conducting, the fluid of extractor 1 output can lead to via heat exchange structure, oil water separator 3, first
Road 4 flows in extractor 1.When second channel 6 turns on, the fluid of extractor 1 output can be through
Flowed in extractor 1 by heat exchange structure, second channel 6.
Natural perfume material is plants essential oil or tincture.The extractor 1 of natural perfume material Preparation equipment
Outlet connect with the entrance of heat exchange structure, heat exchange structure export while with oil water separator 3
Entrance connects with the entrance of extractor 1, so in the outlet of heat exchange structure and entering of extractor 1
Second channel 6 is defined, at outlet and the entrance of extractor 1 of oil water separator 3 between Kou
Between formed first passage 4.Whole natural perfume material Preparation equipment can form two loops: first
Bar loop makes fluid can carry out according to the following flow direction: extractor 1 → heat exchange structure → profit
Separator 3 → extractor 1, this primary Ioops is used for extracting plants essential oil.Article 2 loop makes stream
Body can be carried out according to the following flow direction: extractor 1 → heat exchange structure → extractor 1, this primary Ioops
For extracting tincture.
Visible, the natural perfume material Preparation equipment that technique scheme provides is capable of plants essential oil
Continuous extraction with tincture.
Seeing Fig. 1, heat exchange structure includes that First Heat Exchanger the 21, second heat exchanger 22 and the 3rd changes
Hot device 23.The outlet of First Heat Exchanger 21 connects with the entrance of the 3rd heat exchanger 23, and the 3rd changes
The outlet of hot device 23 connects with oil water separator 3 and second channel 6.3rd heat exchanger 23
Outlet also entrance with the second heat exchanger 22 connect, and the outlet energy of the second heat exchanger 22 is normally opened.
Second heat exchanger 22 is for condensing not by the steam of the 3rd heat exchanger 23 total condensation, and makes
Condensed liquid flows out via former road, steam inlet.
Seeing Fig. 1, the first pipeline 4 connects to be had for preventing oil water separator 3 from siphon occur
The emptying pipeline 5 of phenomenon, emptying pipeline 5 can turn on.There is part and profit in first passage 4
The height such as the natural perfume material outlet of separator 3.So can make in first passage 4 pressure with
At the natural perfume material outlet of oil water separator 3, pressure is equal, can prevent siphonage,
And realize the repeatedly extraction of natural perfume material.
When individually using above-mentioned Article 1 loop, repeatedly can add plant in extractor 1,
To realize the multiple batches of extraction of plants essential oil；When individually using above-mentioned Article 2 loop, Ke Yiduo
Secondary interpolation plant in extractor 1, to realize the multiple batches of extraction of tincture.It is understood that
After the extraction operation of the one or more batch of plants essential oil can being completed using the first loop,
Second servo loop is used to carry out the extraction of tincture again.Or, carry out a batch utilizing the first loop
Or after multiple batches of extraction of essential oil, utilizing second servo loop, single or multiple adds different extractions
Agent, to realize the repeatedly extraction of natural perfume material.
Visible, the natural perfume material Preparation equipment that technique scheme provides is capable of plants essential oil
Continuous with tincture extracts, and is capable of the repeatedly extraction of plants essential oil, tincture.
See Fig. 1, can use some control valves to control the on or off of first passage 4,
Specific as follows: first passage 4 is provided with the 4th control valve V4 and the 5th control valve V5, evacuated tube
First end in road 5 is connected to first passage 4 and is positioned at the 4th control valve V4 and the 5th control valve V5
Between part, the second end of emptying pipeline 5 is by the 8th control valve V8, the first control valve
The entrance connection of V1 and the second heat exchanger 22.4th control valve V4, the 5th control valve V5 are equal
Conducting, then first passage 4 turns on.
See Fig. 1, in like manner, some control valves can be used to control the conducting of second channel 6
Or cut-off, specific as follows: between outlet and the entrance of oil water separator 3 of the 3rd heat exchanger 23
It is provided with the 7th control valve V7, the outlet of the 3rd heat exchanger 23 and the entrance of the 5th control valve V5
Between be provided with the 6th control valve V6.5th control valve V5, the 6th control valve V6 are both turned on,
Then second channel 6 turns on.
Holding above-mentioned, natural perfume material is plants essential oil or tincture.When this natural perfume material Preparation equipment is used
Extracting operation in plants essential oil, first passage 4 turns on, and the fluid of extractor 1 output can be via
Heat exchange structure, oil water separator 3, first passage 4 flow in extractor 1.When this natural perfume (or spice)
Material Preparation equipment extracts operation for tincture, and second channel 6 turns on, the stream of extractor 1 output
Physical efficiency flows in extractor 1 via heat exchange structure, second channel 6.
Further, when this natural perfume material Preparation equipment extracts operation for plants essential oil or tincture,
Emptying pipeline 5 is all in conducting state.So can avoid extracting in operation that siphonage occurs,
Be conducive to extracting the most continuously.
Seeing Fig. 1, the outlet of the second heat exchanger 22 is provided with the exhaust-valve 24 of emptying.Carry out
When tincture extracts operation, the gas of the 3rd non-total condensation of heat exchanger 23 is possibly through the first control
The pipeline at valve V1 place processed returns in the second heat exchanger 22.Second heat exchanger 22 can enter again
Row condensation operation, and liquid backtracking condensation formed, by by the 6th control valve V6
Flow to extractor 1.
A specific embodiment is described below.
As it is shown in figure 1, the natural perfume material Preparation equipment that the embodiment of the present invention provides includes extractor
1, straight-through steam-heating apparatus bottom extractor 1 jacket steam firing equipment, extractor 1, the
One heat exchanger the 21, second heat exchanger the 22, the 3rd heat exchanger 23, oil water separator 3 and pipeline
Valve V1-V8.
The operation using this device to carry out extracting (as a example by natural perfume material, needs elder generation before including operation
Natural plants is added in extractor 1), check that device each road heating and thermal insulation situation and instrument show
Show and control situation, material situation.Confirm no problem after, opening controlling valve V1, V4,
V7, V5 and V8；Closing control valve V2, V3 and V6；Open jacket steam heater block and
The straight-through steam heater block in bottom carries out steam distillation.Steam is entered by heat exchange structure condensation
Oil water separator 3, after the U-shaped balanced design of oil water separator 3, oil water separator 3
Keep certain liquid, in condensate return to extractor 1.Each parameter stability runs to be taken
After between, collect in oil water separator 3 oil reservoir essential oil product.It follows that to extractor
1 add extract solvent, opening controlling valve V1, V5, V6 and V8, close each control valve V2,
V3, V4 and V7 carry out plant solvent extraction, and after setting according to parameter and running required time,
Discharge plant extraction liquid and enter next process, release natural plants residue.In extractor 1
It is again loaded into new a collection of natural plants, and continues operation, produce next group product.
Specifically, the method using above-mentioned natural perfume material Preparation equipment to carry out extracting is as follows:
Step one: natural plants is loaded in extractor 1.
In above-mentioned steps one, appropriate water can be added to extractor 1 the most in advance, add
The 0-50% that mass percent is natural plants quality of amount.
Step 2: opening controlling valve V1, V4, V7, V5 and V8；Closing control valve V2,
V3 and V6.Material is thus formed above-mentioned Article 1 loop, and on this loop, open
Eight control valves V8, can prevent siphonage.
Step 3: start jacket steam firing equipment, after preheating reaches the temperature set, according to
Process requirements can open straight-through steam-heating apparatus bottom extractor 1, and water vapour distillate condenses
To oil water separator 3, keeping certain liquid level by U-shaped design, condensate return is to carrying
Take tank 1.
In above-mentioned steps three, starting extractor 1 jacket steam firing equipment, its steam valve is opened
Degree is 100-0%, and preheating temperature is 80-100 DEG C；According to process requirements, bottom can be opened straight
Logical steam heater, its steam valve aperture is 10-40%；Water vapour distillate condensate flow
Amount can be controlled in 10Kg-60Kg/ hour.
Step 4: after running a period of time under conditions of above-mentioned steps two and step 3, profit
Separator 3 is formed oil reservoir, steam off heating system, is collected by the second control valve V2
Essential oil or build up to subsequent batches and collect together in oil water separator 3.
In above-mentioned steps three, the time of operation can be at 2-8 hour according to process requirements；If oil reservoir
Thicker, essential oil product can be obtained by opening oil reservoir in V2 valve collection oil water separator 3；
If oil reservoir is relatively thin, oil reservoir can not be collected, until second batch or many batches when building up to compared with thick oil pay many
Batch is collected together.
Above-mentioned steps one to step 4 is plants essential oil abstraction process.
Step 5: a certain amount of extraction solvent is added to extractor 1.
In above-mentioned steps five, extracting solvent can be water, ethyl acetate, 5-95% ethanol etc.；Its
Quality is 3-15 times of natural plants.
Step 6: opening controlling valve V1, V5, V6 and V8, closing control valve V2, V3,
V4 and V7 valve, material is thus formed above-mentioned Article 2 loop.
Step 7: start extractor 1 jacket steam firing equipment, after reaching the temperature set,
Solvent condensate liquid passes through the 6th control valve V6 and the 5th control valve V5 condensing reflux to extractor 1.
In above-mentioned steps seven, according to processing parameter setting, its steam heating valve opening is
0-100%；Its temperature range can be that (such as solvent water, its temperature range can for room temperature-solvent boiling point
For room temperature-100 DEG C)；Solvent condensate liquid condensation flow can be 0-80Kg/ hour.
Step 8: after running a period of time under conditions of above-mentioned steps six and step 7, closes
Steam-heating system, the operation using solvent to carry out extracting terminates, and natural botanical extraction liquid passes through
Pump is discharged into next process.
In above-mentioned steps eight, its time range can be 0.5-4 hour.
Above-mentioned steps five to step 8 is tincture abstraction process.Tincture abstraction process is not necessarily intended to
After plants essential oil abstraction process, tincture abstraction process can be used alone.
Step 9: discharge the natural plants residue in extractor 1, continuously add the sky of next group
So plant.
Step 10: repeat step 2-step 8, can realize multiple batches of essential oil one or many and collect.
The natural perfume material Preparation equipment that visible technique scheme provides, utilizes the valve of V1-V8
It is turned on and off, forms two kinds of different condensate liquid reflux techniques, can realize carrying out as required
Switching realizes single batch or multiple batches of continuous production, can obtain good actual effect aborning.
Simultaneously as devise the 8th control valve V8, it is possible to resolve U-shaped due to oil water separator 3
The siphonic effect that design technology exists causes oil-water mixture in oil water separator 3 to be back to simultaneously
Extractor 1 is collected the defective workmanship less than essential oil.
Seeing Fig. 2, another embodiment of the present invention provides a kind of natural perfume material preparation method, including
Following steps:
Step 10, the of the natural perfume material Preparation equipment that arbitrary for present invention technical scheme is provided
One channel conductive；
Step 20, prepare plants essential oil according to plants essential oil abstraction process.Plant described herein
Extraction of essential oil operation can use plants essential oil abstraction process described above.
Herein, the emptying pipeline 5 of described natural perfume material Preparation equipment is turned on, can at least repeat
Step 20 twice.The emptying pipeline 5 of described natural perfume material Preparation equipment is turned on and can be prevented effectively from
Siphonage, in order to repeatedly extract plants essential oil.
Step 30, the second channel of natural perfume material Preparation equipment is turned on；
Step 40, prepare tincture according to tincture abstraction process.Tincture abstraction process described herein
Tincture abstraction process described above can be used.
Herein, the emptying pipeline 5 of described natural perfume material Preparation equipment is turned on, can at least repeat
Step 40 twice.The emptying pipeline 5 of described natural perfume material Preparation equipment is turned on and can be prevented effectively from
Siphonage, in order to repeatedly extract tincture.
Above-mentioned natural perfume material preparation method, uses same set of equipment, it is possible to realize plant essence simultaneously
The extracting continuously of oil and tincture, repeatedly extract.
Several instantiation is described below.
Embodiment 1: Sanming City Youxi essential oil of tobaccos and the preparation of water extract
Sanming City Youxi tobacco leaf, uses beating and double roasting rear panel cigarette, and in Fujian, cigarette industry Limited Liability is public
Department；Steam, Xiamen state can be with collecting Thermal Power Co., Ltd.
According to the technological process of Fig. 1,20Kg Sanming City Youxi tobacco leaf is heated in extractor 1,
Opening controlling valve V1, V4, V7, V5 and V8；Closing control valve V2, V3 and V6.Open
Dynamic extractor 1 jacket steam firing equipment, valve opening 80%, design temperature 80 DEG C.Reach
After the temperature set, straight-through steam heater, valve opening 30% bottom unlatching.Condensate liquid
Condensation flow can be 40Kg/ hour；After parameter stability, run 4 hours time.Water-oil separating
Device 3 has an oil reservoir, opens the second control valve V2, collect essential oil product.
Then 160Kg water is added in extractor 1, opening controlling valve V1, V5, V6 and
V8, closing control valve V2, V3, V4 and V7.Start the heating of extractor 1 jacket steam to set
Standby, its valve opening is 60%, and design temperature is 100 DEG C, and condensation flow can be that 60Kg/ is little
Time；The operation time is 2 hours, steam off heating system, and solvent extracts and terminates, tobacco leaf water
Extract is discharged in extract storage tank entering next process by pump.
Finally discharge the tobacco leaf residue in extractor 1.
This embodiment 1 prepares essential oil of tobaccos and water extract continuously for single batch.
Embodiment 2: essential oil of the flower of Camellia sinensis and the preparation of alcohol extracting thing
Fresh Tea Flower, Anxi Tieguanyin Tea tea hill, fresh harvesting Fujian；Steam, Xiamen state can be same
Collection Thermal Power Co., Ltd.
According to the technological process of Fig. 1, fresh for 30Kg Tea Flower is added in extractor 1, opens
Open control valve V1, V4, V7, V5 and V8；Closing control valve V2, V3 and V6.Start
Extractor 1 jacket steam firing equipment, valve opening 60%, design temperature 60 DEG C.Reach to set
After fixed temperature, straight-through steam heater, valve opening 20% bottom unlatching.Condensate liquid is cold
Solidifying flow can be 30Kg/ hour.After parameter stability, run 6 hours time.Oil water separator 3
In have an oil reservoir.
Then 95% ethanol of 140Kg is added in extractor 1, opening controlling valve V1, V5,
V6 and V8, closing control valve V2, V3, V4 and V7.Start extractor 1 jacket steam to add
Hot equipment, its valve opening is 40%, and design temperature is 75 DEG C, and condensation flow can be 20Kg/
Hour.The operation time is 2 hours, steam off heating system, and solvent extracts and terminates, tobacco leaf
Alcohol extracting thing is discharged in extract storage tank entering next process by pump.
Next the tobacco leaf residue in extractor 1 is discharged.
Above-mentioned each step operation can realize single batch and prepare essential oil of the flower of Camellia sinensis and alcohol extracting continuously
Take thing.
Subsequently fresh for 30Kg Tea Flower is added in extractor 1, repeat the above steps, profit
Oil reservoir in separator 3, after two batch accumulation, is collected and is obtained essential oil product.
Embodiment 2 is that two batches prepare essential oil of the flower of Camellia sinensis and alcohol extracting thing continuously.
Embodiment 3: prepared by tobacco leaf essential oil, alcohol extracting thing and water extract
Zimbabwe's tobacco leaf, uses beating and double roasting rear panel cigarette, and in Fujian, cigarette industry Limited Liability is public
Department's import；Steam, Xiamen state can be with collecting Thermal Power Co., Ltd.
According to the technological process of Fig. 1,20Kg Zimbabwe tobacco leaf is heated in extractor 1,
Opening controlling valve V1, V4, V7, V5 and V8；Closing control valve V2, V3 and V6.Open
Dynamic extractor 1 jacket steam firing equipment, valve opening 80%, design temperature 80 DEG C.Reach
After the temperature set, straight-through steam heater, valve opening 30% bottom unlatching.Condensate liquid
Condensation flow can be 40Kg/ hour.After parameter stability, run 4 hours time；Water-oil separating
Device 3 has an oil reservoir, is essential oil to be extracted.
Then 95% ethanol of 140Kg is added in extractor 1, opening controlling valve V1, V5,
V6 and V8, closing control valve V2, V3, V4 and V7.Start extractor 1 jacket steam to add
Hot equipment, its valve opening is 60%, and design temperature is 100 DEG C, and condensation flow can be 60Kg/
Hour.The operation time is 2 hours, steam off heating system, and tobacco leaf alcohol extracting thing passes through pump
It is discharged into extract storage tank.
It follows that 180Kg water is added in extractor 1, opening controlling valve V1, V5, V6
And V8, closing control valve V2, V3, V4 and V7.Start the heating of extractor 1 jacket steam
Equipment, its valve opening is 55%, and design temperature is 96 DEG C, and condensation flow can be 50Kg/
Hour.The operation time is 2 hours, steam off heating system, and solvent extracts and terminates, tobacco leaf
Water extract is discharged in extract storage tank by pump.
Finally discharge the tobacco leaf residue in extractor 1.
This embodiment 3 prepares essential oil, alcohol extracting thing and water extract continuously for single batch.
Seeing Fig. 3, further embodiment of this invention provides a kind of natural perfume material preparation method, its bag
Include following steps:
Step 50, the of the natural perfume material Preparation equipment that arbitrary for present invention technical scheme is provided
One channel conductive.
Step 60, prepare plants essential oil according to plants essential oil abstraction process.
Herein, the emptying pipeline 5 of described natural perfume material Preparation equipment is turned on, can at least repeat
Step 60 twice.The emptying pipeline 5 of described natural perfume material Preparation equipment is turned on and can be prevented effectively from
Siphonage, in order to repeatedly extract plants essential oil.
Above-mentioned natural perfume material preparation method, uses same set of equipment, it is possible to realize plants essential oil many
Secondary extraction.
An instantiation is described below.
Embodiment 4: the preparation of multiple batches of tealeaves essential oil
Tealeaves, Fujian Anxi Tieguanyin Tea；Steam, Xiamen state can be with collecting Thermal Power Co., Ltd.
According to the technological process of Fig. 1, fresh for 25Kg Tea Flower is added in extractor 1, opens
Open control valve V1, V4, V7, V5 and V8；Close V2, V3 and V6 valve；Startup carries
Take tank 1 jacket steam firing equipment, valve opening 55%, design temperature 55 DEG C；Reach to set
Temperature after, straight-through steam heater, valve opening 25% bottom unlatching；Condensate liquid condenses
Flow can be 28Kg/ hour；After parameter stability, run 6 hours time；Oil water separator 3
In have an oil reservoir；Discharge the tea leaf residual in extractor 1.
Repeat the above steps, produces 6 batches continuously, and the oil reservoir in oil water separator 3 is through six batches
After accumulation, collect and obtain essential oil product.
This embodiment 4 prepares tealeaves essential oil continuously for multiple batches of.
Seeing Fig. 4, yet another embodiment of the invention provides a kind of natural perfume material preparation method, including
Following steps:
Step 70, the of the natural perfume material Preparation equipment that arbitrary for present invention technical scheme is provided
Two channel conductive；
Step 80, prepare tincture according to tincture abstraction process.
Herein, the emptying pipeline 5 of described natural perfume material Preparation equipment is turned on, can at least repeat
Step 80 twice.The emptying pipeline 5 of described natural perfume material Preparation equipment is turned on and can be prevented effectively from
Siphonage, in order to repeatedly extract tincture.
In describing the invention, it is to be understood that term " " center ", " longitudinally ",
" laterally ", "front", "rear", "left", "right", " vertically ", " level ",
" push up ", " end ", " interior ", the orientation of the instruction such as " outward " or position relationship are based on attached
Orientation shown in figure or position relationship, be only for ease of describing the present invention and simplifying description, and not
It is instruction or infers the device of indication or element must have specific orientation, for specific orientation
Structure and operation, thus it is not intended that the present invention to be protected the restriction of content.
Last it is noted that above example is only in order to illustrate technical scheme, and
Non-to its restriction；Although the present invention being described in detail with reference to previous embodiment, ability
The those of ordinary skill in territory is it is understood that it still can be to the skill described in foregoing embodiments
Art scheme is modified, or wherein portion of techniques feature is carried out equivalent, but these are repaiied
Change or replace, not making the essence of appropriate technical solution depart from various embodiments of the present invention technical side
The spirit and scope of case.
Claims (15)
1. a natural perfume material Preparation equipment, it is characterised in that include extractor (1), change
Heat structure and oil water separator (3)；The outlet of described oil water separator (3) and described extraction
First passage (4) it is formed with, the outlet of described heat exchange structure and institute between the entrance of tank (1)
State and between the entrance of extractor (1), be formed with second channel (6)；
Wherein, described first passage (4) and described second channel (6) can select a conducting；When
Described first passage (4) turns on, and the fluid that described extractor (1) exports can change via described
Heat structure, described oil water separator (3), described first passage (4) flow to described extractor
(1) in；When described second channel (6) turns on, the fluid energy that described extractor (1) exports
Flow in described extractor (1) via described heat exchange structure, described second channel (6).
Natural perfume material Preparation equipment the most according to claim 1, it is characterised in that described
First passage (4) connects to be had for preventing described oil water separator (3) from siphonage occur
Emptying pipeline (5), described emptying pipeline (5) can turn on；Described first passage (4) exists
The height such as part and the natural perfume material outlet of described oil water separator (3).
Natural perfume material Preparation equipment the most according to claim 2, it is characterised in that described
Heat exchange structure includes First Heat Exchanger (21), the second heat exchanger (22) and the 3rd heat exchanger (23)；
The outlet of described First Heat Exchanger (21) connects with the entrance of described 3rd heat exchanger (23)
Logical, the outlet of described 3rd heat exchanger (23) and described oil water separator (3) and described second
Passage (6) connects；
The outlet of described 3rd heat exchanger (23) also with the entrance of described second heat exchanger (22)
Connection, the outlet of described second heat exchanger (22) can be normally opened.
Natural perfume material Preparation equipment the most according to claim 3, it is characterised in that described
First passage (4) is provided with the 4th control valve and the 5th control valve, described emptying pipeline (5)
First end is connected to described first passage (4) and is positioned at described 4th control valve and described 5th control
Part between valve, the second end of described emptying pipeline (5) is by the 8th control valve, the first control
Valve processed connects with the entrance of described second heat exchanger (22).
5. according to the arbitrary described natural perfume material Preparation equipment of claim 3-4, it is characterised in that
It is provided with between outlet and the entrance of described oil water separator (3) of described 3rd heat exchanger (23)
7th control valve, the outlet of described 3rd heat exchanger (23) and the entrance of described 5th control valve
Between be provided with the 6th control valve.
6. according to the arbitrary described natural perfume material Preparation equipment of claim 1-4, it is characterised in that
Natural perfume material is plants essential oil or tincture；When this natural perfume material Preparation equipment carries for plants essential oil
Extract operation, described first passage (4) turns on；When this natural perfume material Preparation equipment carries for tincture
Extract operation, described second channel (6) turns on.
Natural perfume material Preparation equipment the most according to claim 6, it is characterised in that when this
Natural perfume material Preparation equipment extracts operation for plants essential oil or tincture, and emptying pipeline (5) is all located
In conducting state.
8. according to the arbitrary described natural perfume material Preparation equipment of claim 3-4, it is characterised in that
The outlet of described second heat exchanger (22) is provided with the exhaust-valve (24) of emptying.
9. a natural perfume material preparation method, it is characterised in that comprise the following steps:
Step 10, lead to the first of arbitrary for claim 1-8 described natural perfume material Preparation equipment
Road turns on；
Step 20, prepare plants essential oil according to plants essential oil abstraction process；
Step 30, the second channel of described natural perfume material Preparation equipment is turned on；
Step 40, prepare tincture according to tincture abstraction process.
Natural perfume material preparation method the most according to claim 9, it is characterised in that
The emptying pipeline of described natural perfume material Preparation equipment is turned on, at least repeats step 20 liang
Secondary.
11. natural perfume material preparation methods according to claim 9, it is characterised in that
The emptying pipeline of described natural perfume material Preparation equipment is turned on, at least repeats step 40 liang
Secondary.
12. 1 kinds of natural perfume material preparation methods, it is characterised in that comprise the following steps:
Step 50, lead to the first of arbitrary for claim 1-8 described natural perfume material Preparation equipment
Road turns on；
Step 60, prepare plants essential oil according to plants essential oil abstraction process.
13. natural perfume material preparation methods according to claim 12, it is characterised in that
The emptying pipeline of described natural perfume material Preparation equipment is turned on, at least repeats step 60 liang
Secondary.
14. 1 kinds of natural perfume material preparation methods, it is characterised in that comprise the following steps:
Step 70, lead to the second of arbitrary for claim 1-8 described natural perfume material Preparation equipment
Road turns on；
Step 80, prepare tincture according to tincture abstraction process.
15. natural perfume material preparation methods according to claim 14, it is characterised in that
The emptying pipeline of described natural perfume material Preparation equipment is turned on, at least repeats step 80 liang
Secondary.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610289681.7A CN105907468B (en) | 2016-05-05 | 2016-05-05 | Natural spice preparation method and equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610289681.7A CN105907468B (en) | 2016-05-05 | 2016-05-05 | Natural spice preparation method and equipment |
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| Publication Number | Publication Date |
|---|---|
| CN105907468A true CN105907468A (en) | 2016-08-31 |
| CN105907468B CN105907468B (en) | 2023-09-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610289681.7A Active CN105907468B (en) | 2016-05-05 | 2016-05-05 | Natural spice preparation method and equipment |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107047819A (en) * | 2017-02-27 | 2017-08-18 | 四川星麻哥食品有限公司 | It is a kind of that the equipment that flavour and fragrance substance produces flavored oils is extracted from spice |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202446854U (en) * | 2011-12-31 | 2012-09-26 | 浙江康恩贝制药股份有限公司 | Device for separating and collecting Chinese medicinal volatile oil |
| CN203833913U (en) * | 2014-04-07 | 2014-09-17 | 鲁南制药集团股份有限公司 | High-efficiency traditional Chinese medicine material volatile oil extraction device |
| CN105540547A (en) * | 2016-02-02 | 2016-05-04 | 成都科佑达技术开发有限公司 | Chlorine dioxide generator |
-
2016
- 2016-05-05 CN CN201610289681.7A patent/CN105907468B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202446854U (en) * | 2011-12-31 | 2012-09-26 | 浙江康恩贝制药股份有限公司 | Device for separating and collecting Chinese medicinal volatile oil |
| CN203833913U (en) * | 2014-04-07 | 2014-09-17 | 鲁南制药集团股份有限公司 | High-efficiency traditional Chinese medicine material volatile oil extraction device |
| CN105540547A (en) * | 2016-02-02 | 2016-05-04 | 成都科佑达技术开发有限公司 | Chlorine dioxide generator |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107047819A (en) * | 2017-02-27 | 2017-08-18 | 四川星麻哥食品有限公司 | It is a kind of that the equipment that flavour and fragrance substance produces flavored oils is extracted from spice |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105907468B (en) | 2023-09-01 |
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