CN206152395U - Traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function - Google Patents

Traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function Download PDF

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Publication number
CN206152395U
CN206152395U CN201621182390.XU CN201621182390U CN206152395U CN 206152395 U CN206152395 U CN 206152395U CN 201621182390 U CN201621182390 U CN 201621182390U CN 206152395 U CN206152395 U CN 206152395U
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CN
China
Prior art keywords
probe
optical fiber
fiber sensor
sensor probe
lid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn - After Issue
Application number
CN201621182390.XU
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Chinese (zh)
Inventor
王海霞
所同川
于洋
李正
宋新波
刘长青
李忠林
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Tianjin University of Traditional Chinese Medicine
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Tianjin University of Traditional Chinese Medicine
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Application filed by Tianjin University of Traditional Chinese Medicine filed Critical Tianjin University of Traditional Chinese Medicine
Priority to CN201621182390.XU priority Critical patent/CN206152395U/en
Application granted granted Critical
Publication of CN206152395U publication Critical patent/CN206152395U/en
Withdrawn - After Issue legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function, including a jar body, cover, be provided with the optical fiber sensor base in the well lower part of the jar body, the optical fiber sensor base includes the tubulose body and has mesoporous lid, the optical fiber sensor probe is through the inner wall movably connected of sealing rubber circle with the tubulose body, the upper end of tubulose body with have mesoporous lid swing joint, the mesopore of lid is run through on the upper portion that makes the optical fiber sensor probe, the lower tip of optical fiber sensor probe is provided with the external screw thread, the lateral wall inner surface provided with an inner thread of probe cap, and the lower part of probe cap sets up porosely, and probe cap bottom wall upper surface is provided with the speculum, probe cap and optical fiber sensor probe connection, the optical fiber sensor probe is connected with near -infrared spectroscopy through optic fibre. The utility model discloses the realization is drawed, in the concentration process online near -infrared real -time detection at different positions, effectively improves accuracy, the accuracy nature of analysis, can be used to guide the big production process of chinese materia medica preparation.

Description

A kind of Chinese medicine extraction near infrared online detection function, concentration tank
Technical field
This utility model is related to a kind of extraction near infrared online detection function, concentrator, belongs to Chinese medicine preparation Prepare and production process field of quality control.
Background technology
What is may occurred due to the unstability in Chinese medicine source, the complexity of itself and in each processing and manufacturing link answers Miscellaneous change, control conforming to end product quality proposes very high requirement.Therefore, it is past to the quality control of Chinese medicine preparation Toward can not adhere rigidly to raw material determine and product terminal test in terms of, and to the technological parameter during production, physical and chemical index, pass Key composition is even more important in interior quality control.Extract, concentration process as Chinese medicine preparation key link, to a great extent Decide the active constituent content and performance change of final preparation, therefore to the control of product quality of the two production links particularly It is important, especially on-line checking.But, at present the concentrator that extracts on the market all lacks strong on-line checking assembling, right The quality control of the two production processes is also very roughly.Such as in extraction process, due to the mass discrepancy between medical material batch and Impact of the fluctuation of extraction process operating mode to final extraction effect is but negligent of considering that this directly affects extraction efficiency between batch Concordance.And in concentration process, often simply using technological parameters and density, pol, water content etc. such as quantity of steam, pressure As mass parameter come the quality that controls and evaluate product, it is difficult to accomplish the unified production monitoring of standard between batch, this all direct shadow Ring the quality conformance of final extractum.
Near-infrared spectrum technique is a kind of typical pharmacy procedure analytical technology, and it has easy to operate, spectral information amount The advantages of abundant, analysis is quick and precisely, sample need not be processed, environmental pollution is low and with low cost, is widely used in recent years In the qualitative and quantitative analysis detection of Chinese medicine preparation production process, for the monitor in real time and quality of Chinese medicine preparation production link Detection all brings conveniently.But, at present in the near infrared detection of Chinese medicine extraction and concentration production process, it is difficult to real meaning Upper theory can accomplish on-line checking.Detection in extraction process, typically all manually takes out or is introduced into side by extracting solution It is analyzed on road, may be affected by external environments such as air, temperature in the process, so as to affects near-infrared to test As a result;And in concentration process, due to the restriction of negative pressure, it is difficult to realize that near-infrared is tested in Conventional concentration equipment.Therefore, open Send out the extraction near infrared online detection device a kind of, thickener is needed badly, this is extracted for Chinese medicine production, concentration process Automated condtrol, online quality-monitoring all has great importance.
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, there is provided a kind of near infrared online detection function Chinese medicine extraction, concentrator.
The technical solution of the utility model is summarized as follows:
A kind of Chinese medicine extraction near infrared online detection function, concentration tank, including tank body 3, cover 2, on cover 2 Vacuum-pumping tube 1, visor 8 and agitator 9 are provided with, the outside winding of tank body is provided with heating tape 4, set in the middle and lower part of tank body Fibre Optical Sensor base 5 is equipped with, the Fibre Optical Sensor base 5 includes tubular body 17 and the lid 16 with mesopore, optical fiber Sensor probe 14 is flexibly connected by sealing rubber ring 15 with the inwall of tubular body 17, the upper end of tubular body 17 with carry The lid 16 of mesopore is flexibly connected, and makes the top of fiber-optic sensor probe 14 through the mesopore of lid;Fiber-optic sensor probe 14 Bottom be provided with external screw thread, the bottom that the inner surface setting of side wall 13 on the top of probe cap 10 has female thread, probe cap 10 sets Hole 18 is equipped with, the upper surface of probe cap diapire 11 is provided with the lower end spiral shell of reflecting mirror 12, probe cap 10 and fiber-optic sensor probe 14 Stricture of vagina connects, and fiber-optic sensor probe 14 is connected by optical fiber 6 near infrared spectrometer 7.
Advantage of the present utility model:
(1) this utility model realizes the near infrared online real-time detection of extraction of traditional Chinese medicine, to different extraction times, difference The truth of extracting solution provides real-time judge under extraction conditions, is easy to production process monitoring, is conducive to instructing actual production.
(2) this utility model realizes the near infrared online real-time detection of traditional Chinese drug inspissation process, to different concentration times, difference The truth of concentrated solution provides real-time judge under the conditions of concentration, is easy to production process monitoring, is conducive to instructing actual production.
(3) heating tape heating is provided with by outside winding in this utility model.
(4) in this utility model, fiber-optic sensor probe and probe cap stretch into the position of tank body can be with flexible, favorably In the information for determining pot liquid at different loci, the integrated information of liquid can be provided, for the comprehensive regulation of production process It is necessary.
(6) extraction near infrared online detection device described in the utility model, thickener simple structure, energy consumption It is low, pollution-free, and cleaning, maintenance are readily disassembled, it is applied widely, can be used to decoct extraction, decompression extraction, Soakage extraction, subtract In pressure concentration process.
Description of the drawings
Fig. 1 is the structural representation of the Chinese medicine extraction near infrared online detection function, concentration tank.
Fig. 2 is the partial enlarged drawing of Fibre Optical Sensor base 5 in Fig. 1.
Specific embodiment
This utility model is further described below by accompanying drawing.
A kind of Chinese medicine extraction near infrared online detection function, concentration tank, including tank body 3, cover 2, on cover 2 Vacuum-pumping tube 1, visor 8 and agitator 9 are provided with, the outside winding of tank body is provided with heating tape 4, set in the middle and lower part of tank body Fibre Optical Sensor base 5 is equipped with, the Fibre Optical Sensor base 5 includes tubular body 17 and the lid 16 with mesopore, optical fiber Sensor probe 14 is flexibly connected by sealing rubber ring 15 with the inwall of tubular body 17, the upper end of tubular body 17 with carry The lid 16 of mesopore is closely flexibly connected, and makes the top of fiber-optic sensor probe 14 through the mesopore of lid;Fibre Optical Sensor is visited 14 bottom is provided with external screw thread, and it (is herein office in Fig. 2 that the inner surface setting of side wall 13 on the top of probe cap 10 has female thread Cut open), the bottom of probe cap 10 is provided with hole 18, and the upper surface of probe cap diapire 11 is provided with reflecting mirror 12, probe cap 10 and optical fiber Lower end (in Fig. 2 herein for the office cut open) threaded connection of sensor probe 14, fiber-optic sensor probe 14 is by optical fiber 6 and near-infrared Spectrogrph 7 connects.
The one end of vacuum orifice 1 is fixed on top cover, and the other end is equipped with flange-interface, can be closed when needing closed and be connect Mouthful, can be attached by pipe when needing to be connected with the vaporizer for being furnished with vacuum and condensing units.
Top cover 2 can be opened flexibly, and close when with the good seal of tank body 3.
Chinese medicine extraction near infrared online detection function, concentration tank can realize heating and agitating function.
Fiber-optic sensor probe 14 is transflector fiber-optic sensor probe, and light path is transmitted to first by optical fiber sensing probe Liquid material (prepare liquid) in hole 18, prepare liquid is reflected spectral information by reflecting mirror 12 final in near-infrared Spectrogrph 7 is presented.
The bottom of fiber-optic sensor probe 14 is provided with external screw thread, and the inner surface setting of side wall 13 of probe cap 10 has interior spiral shell Stricture of vagina, turn probe cap 10 can make to move or move down on probe cap 10, thus can adjust the light path of test.
The setting of sealing rubber ring 15 can make to move or move down in fiber-optic sensor probe 14, it is also possible to make on probe cap 10 Move or move down.

Claims (1)

1. a kind of Chinese medicine extraction near infrared online detection function, concentration tank, is characterized in that including tank body (3), cover (2) vacuum-pumping tube (1), visor (8) and agitator (9), are provided with cover (2), it is characterized in that the outside winding in tank body Heating tape (4) is provided with, the middle and lower part of tank body is provided with Fibre Optical Sensor base (5), Fibre Optical Sensor base (5) bag Tubular body (17) and the lid (16) with mesopore are included, fiber-optic sensor probe (14) is by sealing rubber ring (15) and tubulose The inwall of body (17) is flexibly connected, and the upper end of tubular body (17) is flexibly connected with the lid (16) with mesopore, makes optical fiber Mesopore of the top of sensor probe (14) through lid;The bottom of fiber-optic sensor probe (14) is provided with external screw thread, visits The bottom that side wall (13) inner surface setting on head cap (10) top has female thread, probe cap (10) is provided with hole (18), probe cap Diapire (11) upper surface is provided with reflecting mirror (12), and probe cap (10) is threadedly coupled with the lower end of fiber-optic sensor probe (14), Fiber-optic sensor probe (14) is connected by optical fiber (6) near infrared spectrometer (7).
CN201621182390.XU 2016-11-03 2016-11-03 Traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function Withdrawn - After Issue CN206152395U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621182390.XU CN206152395U (en) 2016-11-03 2016-11-03 Traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621182390.XU CN206152395U (en) 2016-11-03 2016-11-03 Traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function

Publications (1)

Publication Number Publication Date
CN206152395U true CN206152395U (en) 2017-05-10

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CN201621182390.XU Withdrawn - After Issue CN206152395U (en) 2016-11-03 2016-11-03 Traditional chinese medicine draws, concentrated jar with near -infrared on -line measuring function

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106334337A (en) * 2016-11-03 2017-01-18 天津中医药大学 Traditional Chinese medicine extraction and concentration tank having near-infrared online detection function

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106334337A (en) * 2016-11-03 2017-01-18 天津中医药大学 Traditional Chinese medicine extraction and concentration tank having near-infrared online detection function
CN106334337B (en) * 2016-11-03 2018-12-18 天津中医药大学 A kind of traditional Chinese medicine extraction near infrared online detection function, concentration tank

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Granted publication date: 20170510

Effective date of abandoning: 20181218