CN205620387U - Spontaneous imbibition displacement of reservoir oil measuring device of rock core - Google Patents

Spontaneous imbibition displacement of reservoir oil measuring device of rock core Download PDF

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Publication number
CN205620387U
CN205620387U CN201620417109.XU CN201620417109U CN205620387U CN 205620387 U CN205620387 U CN 205620387U CN 201620417109 U CN201620417109 U CN 201620417109U CN 205620387 U CN205620387 U CN 205620387U
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China
Prior art keywords
rock core
bottle
oil
experiment
frizing
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Expired - Fee Related
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CN201620417109.XU
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Chinese (zh)
Inventor
宿帅
申颍浩
杨志辉
任凯
付冰
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China University of Petroleum Beijing
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China University of Petroleum Beijing
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/24Earth materials

Abstract

The utility model relates to a spontaneous imbibition displacement of reservoir oil measuring device of rock core, its structure includes: meter buret, experiment bottle, the rock core holder, the experiment bottle base, the experiment rock core, the frizing device seals at a distance from the device, the frizing rocker, its characterized in that: meter buret be located experiment bottle top, can measure discharge crude oil volume, the experiment bottle base be located experiment bottle below, the placing object body in can be to the bottle with the experiment bottle after -separating, the rock core holder place on experiment bottle inside bottom surface, the experiment rock core fixed on the rock core holder, the frizing device pass that sealing on the experiment bottle lateral wall separates the device and the frizing rocker links to each other, seal to separate the device and can make the water in the bottle not flow from the experiment bottle lateral wall, frizing device motion state can be controlled to the frizing rocker, the oil that will test the rock core wall drips to be scraped down, and then can make meter buret measure the oil volume attached to the rock core wall.

Description

A kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus
Technical field
This utility model belongs to oil-gas field development field, is specifically related to a kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus.
Background technology
Along with deepening continuously unconventional reservoir research, increasing production mechanism is revealed.At Study In Reservoir fracturing process Time, find that the petroleum resources being present in its content is also had necessarily while reservoir is carried out pressure break by the fracturing fluid used Displacement effect.Compared with conventional sandstone reservoir, the spontaneous imbibition of low permeability gas reservoir reservoir, particularly clay shale with low permeability gas reservoir Ability is higher, and this allows for fracturing fluid time shale reservoir is carried out pressure break, the super dryness having due to rock itself, powerful hair The effect of tubule power and clay chemistry power etc. so that fracturing fluid to matrix flow, enters substrate and the seam of inside thereof from crack In gap.The fracturing fluid being entered substrate and internal interstices thereof by imbibition displacement can go out its internal petroleum resources, thus improves oil gas The recovery ratio of resource, creates more preferable economic benefit.
In order to study fracturing fluid to the phenomenon of reservoir displacement effect and effect, a kind of driving device is needed to test.Mesh Before, conventional spontaneous imbibition measurement apparatus is roughly divided into two classes, and a class weighs the change of core quality after suction liquid by balance Changing, a class is the change being weighed by graduated cylinder and discharging core fluids volume.
At present, in carrying out Equations of The Second Kind experiment.Saturated oils rock core needed for experiment is handled and is put into well the reality installing displacement liquid After testing instrument, displacing fluid will penetrate in rock core substrate and gap thereof by the way of spontaneous imbibition, by its internal fat oil displacement Out.Density due to oil is less than the density of displacing fluid, so can be floated to liquid upper strata by displacement oil out.By observing Float to the oil column in graduated glass tubing, can intuitively learn that imbibition is entered the displacing fluid displacement of rock core and gone out how much oil.But It is, in experimentation, in the oil droplet part that driven liquid displacement goes out can float to carry graduated reflex glass pipe, one Dividing and then can adsorb at core surface, this just causes impact to precision of experiment metering so that experimental data is more inclined than actual value Low, it is impossible to be accurately obtained experimental result.
Therefore to study this process more preferably, more accurately, need on original instrument and equipment, carry out Optimal improvements.
Summary of the invention
The technical problem to be solved is to provide a kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus so that the device after improvement The oil droplet at core surface can be adsorbed after being gone out by displacement scrape so that it is floating entrance is in the glass tubing of metering, it is achieved real The accurate measurement tested.
For solving above-mentioned technical problem, the technical scheme that this utility model is used is:
A kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus, its structure includes: gauge line, test bottle, core holding unit, test bottle Base, tests rock core, oil-scraping device, packing device, frizing rocking bar, it is characterised in that: described gauge line is positioned at test bottle Top, it is possible to measuring and discharge crude oil volume, described test bottle base is positioned at below test bottle, can after separating with test bottle Placing object in bottle, described core holding unit is placed on the bottom surface within test bottle, and described experiment rock core is fixed on On core holding unit, described oil-scraping device is connected through the packing device on test bottle sidewall with frizing rocking bar, described packing Device can make the water in bottle not flow out from test bottle sidewall, and frizing rocking bar can control oil-scraping device kinestate, will test rock The oil droplet in heart wall face scrapes.
By such scheme, the graduated hollow circular-tube of band that described gauge line is isometrical, measurable scope is from 0.5ml-2.0ml ?.
Design principle of the present utility model:
Due to hollow billet wetting effect, after the hydrophilic saturated crude oil of rock core when putting in water, rely on the spontaneous of capillary force initiation Water can be sucked in rock core by imbibition effect, simultaneously also has a certain amount of crude oil to be discharged, the crude oil volume being discharged by measurement with The change of time can draw spontaneous imbibition curve.But, owing to the factor impact such as viscous force of crude oil can make a part be discharged Crude oil be bonded on rock core wall, the crude oil volume making measurement is inaccurate.In this device, will mainly by special oil-scraping structure The oil droplet being attached to rock sample surface scrapes.Operating procedure is as follows:
(1) first the rock core used by experiment is processed into the specification specified, then puts it into drying baker and dry, drying chamber Temperature is set to 105 degrees Celsius, general dry six hours after quality no longer change, think rock drying.Rock after drying Heart saturated oils, fully saturated at it and fix with core holding unit after drying the oil of Adsorption on Surface.
(2) injecting displacing fluid used by appropriate experiment in test bottle, the page is higher than major part scale in gauge line.Will experiment Bottle base (being connected to core holding unit and experiment rock core) is connected and by contact surface good seal with test bottle, can start experiment and survey Amount.
(3) in recording gauge buret, first to rotate frizing rocking bar when the size of oil column, the oil droplet of experiment core surface absorption is scraped Fall so that it is in floating entrance gauge line, so can record the oil mass that displacing fluid displacement goes out more accurately.Gone out by record displacement Oil mass contrast again saturated enter rock core total oil mass, the recovery ratio size that displacing fluid works can be learnt.
The beneficial effects of the utility model:
Be can be seen that by above-mentioned principle design, a kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus that this utility model provides has as follows Advantage: instrument is easy, portable and carrying, all can test under major part environment, also can meet under some heating conditions Experiment measure;Simple to operate, use the principle of spontaneous imbibition to test, only the rock core handled well need to be put into experimental provision In, record experimental data;Compared with conventional experimental provision, the mode wiped off at the oil droplet of core surface will be adsorbed with crossing, Make experimental data more accurate.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of a kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus of this utility model embodiment 1.In figure: 1 metering Pipe, 2 test bottles, 3 core holding units, 4 test bottle bases, 5 experiment rock cores, 6 oil-scraping devices, 7 packing devices, 8 Frizing rocking bar.
Detailed description of the invention
Embodiment 1
A kind of rock core spontaneous imbibition displacement of reservoir oil measurement apparatus, its structure includes: gauge line, test bottle, core holding unit, test bottle Base, tests rock core, oil-scraping device, packing device, frizing rocking bar, it is characterised in that: described gauge line is positioned at test bottle Top, it is possible to measuring and discharge crude oil volume, described test bottle base is positioned at below test bottle, can after separating with test bottle Placing object in bottle, described core holding unit is placed on the bottom surface within test bottle, and described experiment rock core is fixed on On core holding unit, described oil-scraping device is connected through the packing device on test bottle sidewall with frizing rocking bar, described packing Device can make the water in bottle not flow out from test bottle sidewall, and frizing rocking bar can control oil-scraping device kinestate, will test rock The oil droplet in heart wall face scrapes.
The undeclared part related in this utility model is same as the prior art or uses prior art to be realized.

Claims (1)

1. a rock core spontaneous imbibition displacement of reservoir oil measurement apparatus, its structure includes: gauge line (1), test bottle (2), and rock core presss from both sides Holder (3), test bottle base (4), experiment rock core (5), oil-scraping device (6), packing device (7), frizing rocking bar (8), it is characterised in that: described gauge line (1) is positioned at test bottle (2) top, it is possible to measure the volume discharging crude oil, Described test bottle base (4) is positioned at test bottle (2) lower section, can place thing with test bottle (2) after separating in bottle Body, described core holding unit (3) is placed on the bottom surface that test bottle (2) is internal, and described experiment rock core (5) is consolidated Be scheduled on core holding unit (3), described oil-scraping device (6) through the packing device (7) on test bottle (2) sidewall with Frizing rocking bar (8) is connected, and described packing device (7) can make the water in bottle not flow out from test bottle (2) sidewall, scrapes Oil rocking bar (8) can control oil-scraping device (6) kinestate, is scraped by the oil droplet of experiment rock core (5) wall.
CN201620417109.XU 2016-05-11 2016-05-11 Spontaneous imbibition displacement of reservoir oil measuring device of rock core Expired - Fee Related CN205620387U (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106769752A (en) * 2016-11-29 2017-05-31 中国石油大学(北京) Rotatable imbibition experimental provision
CN107144515A (en) * 2017-07-05 2017-09-08 西安石油大学 Imbibition experimental provision and its method
CN109459556A (en) * 2018-12-05 2019-03-12 中国石油大学(北京) Dynamic imbibition device and the experimental method tested for dynamic imbibition
WO2019145745A1 (en) * 2018-01-23 2019-08-01 Total Sa Method and apparatus for analyzing a rock sample
CN110346260A (en) * 2019-08-02 2019-10-18 东北石油大学 Fine and close oil reservoir matrix rock core static state imbibition recovery ratio laser measuring device for measuring and method

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106769752A (en) * 2016-11-29 2017-05-31 中国石油大学(北京) Rotatable imbibition experimental provision
CN107144515A (en) * 2017-07-05 2017-09-08 西安石油大学 Imbibition experimental provision and its method
WO2019145745A1 (en) * 2018-01-23 2019-08-01 Total Sa Method and apparatus for analyzing a rock sample
US11340208B2 (en) 2018-01-23 2022-05-24 Total Se Method and apparatus for analyzing a rock sample
CN109459556A (en) * 2018-12-05 2019-03-12 中国石油大学(北京) Dynamic imbibition device and the experimental method tested for dynamic imbibition
CN109459556B (en) * 2018-12-05 2022-07-08 中国石油大学(北京) Dynamic imbibition device and experimental method for dynamic imbibition experiment
CN110346260A (en) * 2019-08-02 2019-10-18 东北石油大学 Fine and close oil reservoir matrix rock core static state imbibition recovery ratio laser measuring device for measuring and method
CN110346260B (en) * 2019-08-02 2022-03-08 东北石油大学 Laser measurement device and method for static imbibition recovery ratio of matrix core of tight oil reservoir

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Granted publication date: 20161005

Termination date: 20170511