CN103278430A - Low-permeability rock core start-up pressure gradient testing device - Google Patents

Low-permeability rock core start-up pressure gradient testing device Download PDF

Info

Publication number
CN103278430A
CN103278430A CN2013101952712A CN201310195271A CN103278430A CN 103278430 A CN103278430 A CN 103278430A CN 2013101952712 A CN2013101952712 A CN 2013101952712A CN 201310195271 A CN201310195271 A CN 201310195271A CN 103278430 A CN103278430 A CN 103278430A
Authority
CN
China
Prior art keywords
pressure gradient
rock core
low
steel pole
low permeability
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101952712A
Other languages
Chinese (zh)
Inventor
陈志明
汪伟英
刘冰
蔡雨桐
欧阳云丽
科文丽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yangtze University
Original Assignee
Yangtze University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yangtze University filed Critical Yangtze University
Priority to CN2013101952712A priority Critical patent/CN103278430A/en
Publication of CN103278430A publication Critical patent/CN103278430A/en
Pending legal-status Critical Current

Links

Images

Abstract

The invention relates to a low-permeability rock core start-up pressure gradient testing device, belonging to the technical field of a hydrocarbon reservoir evaluation method in oil-gas exploration and development processes. The low-permeability rock core start-up pressure gradient testing device is characterized in that a movable steel rod (4) is sheathed at the upper end of a bracket (7); a horizontal steel rod (1) is arranged on the top of the movable steel rod (4); a rotary table (13) is arranged on the bracket (7); one end of a steel wire pull rope (8) is arranged on the rotary table (13), and the other end of the steel wire pull rope (8) is arranged on the horizontal steel rod (1) by three fixed pulleys (2) and a movable pulley (9); a liquid storage tank (10) is arranged in a liquid carrier table (11); the bottom end of the liquid storage tank (10) is connected with a rubber tube (12) which is communicated with the bottom end of an intermediate container (14); the top of the intermediate container (14) is provided with an opening and is connected with a pipeline (19); the other end of the pipeline (19) is connected with one end of a rock core clamp holder (16). The low-permeability rock core start-up pressure gradient testing device can provide continuous injection pressure by continuously increasing the height of the liquid level of the liquid storage tank, so that the low-permeability rock core start-up pressure gradient can be measured. The low-permeability rock core start-up pressure gradient testing device has the characteristics of being simple and reasonable in structure, convenient to use, high in measurement accuracy, economical and practical.

Description

A kind of low permeability cores starting pressure gradient proving installation
Technical field:
The present invention relates to a kind of low permeability cores starting pressure gradient proving installation, belong to oil and gas zone evaluation method and technology field in the oil-gas exploration and development process.
Background technology:
In the development of low-permeability oil reservoir process, the starting pressure gradient can produce very big influence to the reservoir development effect.Therefore, the research to hypotonic rock starting pressure gradient has very important meaning.
The research of starting pressure gradient is a very fine and hard work, does not also have perfect research method at present.Improve in shortage under the situation of research method, identical hypotonic rock sample tends to obtain different starting pressure gradients, the reliability of experimental data can not get guaranteeing, and the knotty problem of a large amount of LOW PERMEABILITY RESERVOIR is still unresolved,, pressure decline low as per-well production is fast etc., and this is just unfavorable greatly to the exploitation generation of China's LOW PERMEABILITY RESERVOIR.At present, many scholars study the starting pressure gradient of hypotonic rock on the basis of experiment.Now use comparatively generally " pressure reduction-flow " method and capillary equilibrium method, its pumping source that uses is N 2Bottle, constant-flux pump or high precision pump.
But the test of starting pressure gradient needs minimum flow conditions, and the flow velocity of above-mentioned pumping source is all excessive, is not desirable pumping source, uses its measurement of carrying out the starting pressure gradient will inevitably reduce the accuracy of experiment.In addition, experiment pressure reduction is mainly measured by tensimeter, and present manometric minimum scale is 500Pa, and pressure reduction is big at interval, can't realize that pressure reduction is continuous, can not obtain abundant representative data, and pressure reduction requires stabilization time very long, expends time in very much and energy, and data precision can't be guaranteed, cause than mistake, can not satisfy actual requirement.
Summary of the invention:
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of low permeability cores starting pressure gradient proving installation, by improving constantly the liquid level of fluid reservoir, continuous injection pressure is provided, accurately measure the Starting pressure of low permeability cores gradient, have the characteristics simple and reasonable, easy to use, that measuring accuracy is high, economical and practical.
The present invention realizes above-mentioned purpose by following technical solution.
In a kind of structure of low permeability cores starting pressure gradient proving installation, be provided with horizontal steel pole, fixed pulley, rule, movable steel pole, tighten up screw, tighten screw, support, steel wire tow line, travelling block, fluid reservoir, carrier fluid platform, rubber tube, rotating disk, intermediate receptacle, base, core holding unit, confined pressure pump, low permeability cores, pipeline, graduated cylinder; Support is installed on the base, is set with movable steel pole in the upper end of support; Movable steel pole can slide up and down in support, and is fixed by tightening up screw; On the top of movable steel pole horizontal steel pole is installed, at the other parallel rule that is equipped with of support; At support rotating disk is installed, rotating disk can rotate, and by the chucking screw it is tightened; One end of steel wire tow line is installed on the rotating disk, and the other end is installed on the horizontal steel pole through three fixed pulleys and a travelling block; The carrier fluid platform hangs the below that is installed in travelling block, and fluid reservoir places the carrier fluid platform, is connected with rubber tube in the bottom of fluid reservoir; The lower end of rubber tube is connected with the bottom of intermediate receptacle; The top of intermediate receptacle is provided with opening, is connected with pipeline, and the other end of pipeline is connected with an end of core holding unit; The outlet of the pipeline of the core holding unit other end is positioned at the top of graduated cylinder; Low permeability cores is equipped with in inside at core holding unit, and side joint has the confined pressure pump outside.
The present invention compared with prior art, by improving constantly the liquid level of fluid reservoir, continuous injection pressure is provided, just can measure the Starting pressure of low permeability cores gradient, liquid level can be accurate to 1mm, the measurement of starting pressure can be accurate to 10Pa, has improved 50 times than conventional method precision, has the characteristics simple and reasonable, easy to use, that measuring accuracy is high, economical and practical.
Description of drawings:
Fig. 1 is general structure synoptic diagram of the present invention.
In the drawings: 1. horizontal steel pole, 2. fixed pulley, 3. rule, 4. movable steel pole, 5. tighten up screw, 6. chucking screw, 7. support, 8. steel wire tow line, 9. travelling block, 10. fluid reservoir, 11. carrier fluid platforms, 12. rubber tubes, 13. rotating disks, 14. intermediate receptacles, 15. bases, 16. core holding units, 17. confined pressure pumps, 18. low permeability cores, 19. pipelines, 20. graduated cylinders.
Embodiment:
The invention will be further described below in conjunction with drawings and Examples.
A kind of low permeability cores starting pressure of the present invention gradient proving installation by horizontal steel pole 1, fixed pulley 2, rule 3, movable steel pole 4, tighten up screw 5, chucking screw 6, support 7, steel wire tow line 8, travelling block 9, fluid reservoir 10, carrier fluid platform 11, rubber tube 12, rotating disk 13, intermediate receptacle 14, base 15, core holding unit 16, confined pressure pump 17, low permeability cores 18, pipeline 19, graduated cylinder 20 and form; Support 7 is installed on the base 15, is set with movable steel pole 4 in the upper end of support 7; Movable steel pole 4 can slide up and down in support 7, and is fixed by tightening up screw 5; Horizontal steel pole 1 is installed, at the support 7 other parallel rules 3 that are equipped with on the top of movable steel pole 4; At support 7 rotating disk 13 is installed, rotating disk 13 can rotate, and by tightening screw 6 with its chucking; One end of steel wire tow line 8 is installed on the rotating disk 13, and the other end is installed on the horizontal steel pole 1 through three fixed pulleys 2 and a travelling block 9; Carrier fluid platform 11 hangs the below that is installed in travelling block 9, and fluid reservoir 10 places carrier fluid platform 11, is connected with rubber tube 12 in the bottom of fluid reservoir 10; The lower end of rubber tube 12 is connected with the bottom of intermediate receptacle 14; The top of intermediate receptacle 14 is provided with opening, is connected with pipeline 19, and the other end of pipeline 19 is connected with an end of core holding unit 16; The outlet of the pipeline 19 of core holding unit 16 other ends is positioned at the top of graduated cylinder 20; In the inside of core holding unit 16 low permeability cores 18 is housed, side joint has confined pressure pump 17 outside.
Adopt the present invention to measure the Starting pressure of low permeability cores gradient, can carry out as follows:
(1), low permeability cores 18 cleaned after, be put in oven dry (12h) in the constant temperature oven (60 ° of C), weigh then, and measure its length L and perm-plug method.
(2), low permeability cores 18 samples after will handling place in the high pressure vessel, start vacuum pump and vacuumize (12h), make its saturation experiments salt solution.
(3), low permeability cores 18 samples of saturation experiments salt solution are packed in the core holding unit 16, apply confined pressure with confined pressure pump 17 simulating oil deposit conditions; Injection experiments salt solution in fluid reservoir 10, rubber tube 12 and intermediate receptacle 14.
(4), before measurement, regulate the height of fluid reservoir 10, make the liquid level of fluid reservoir 10 consistent with the height of core holding unit 16 ends, the pressure reduction that makes low permeability cores 18 two ends is 0, and writes down the liquid level value h of fluid reservoir 10 at this moment 1
(5), when measuring, promote the height of fluid reservoir 10 by rotating disk 13 gradually with the interval of 1mm, a period of time is stablized at the interval of every rising 1mm, and the liquid level of fluid reservoir 10 is risen gradually.When promoting fluid reservoir 10, observe the liquid level situation in the core holding unit 16 endpiece pipelines 19; Before fluid column pressure reached starting pressure, the liquid level in the core holding unit 16 endpiece pipelines 19 can not flow; After reaching starting pressure, the liquid level in the core holding unit 16 endpiece pipelines 19 begins to flow; Liquid level in core holding unit 16 endpiece pipelines 19 has just begun moment of flowing, and writes down the liquid level value h of fluid reservoir 10 this moment 2
(6), after measurement is finished, experimental record data calculate the starting pressure gradient of low permeability cores 18, computing formula (1) is:
GradP = ρg ( h 2 - h 1 ) L × 10 - 4 - - - ( 1 )
Wherein: GradP: be starting pressure gradient, MPa/m;
ρ: be experiment brine density, g/cm 3
G: be acceleration of gravity, m/s 2
h 1:: be the liquid level value of initial fluid reservoir, mm;
h 2: be the flow liquid level value of fluid reservoir of moment of liquid level, mm;
L: be rock core length, cm.

Claims (3)

1. low permeability cores starting pressure gradient proving installation is by horizontal steel pole (1), fixed pulley (2), rule (3), movable steel pole (4), tighten up screw (5), chucking screw (6), support (7), steel wire tow line (8), travelling block (9), base (15), pipeline (19), graduated cylinder (20) and form; It is characterized in that in its structure, being provided with fluid reservoir (10), carrier fluid platform (11), rubber tube (12), rotating disk (13), intermediate receptacle (14), core holding unit (16), confined pressure pump (17), low permeability cores (18); Support (7) is installed on the base (15), is set with movable steel pole (4) in the upper end of support (7); On the top of movable steel pole (4) horizontal steel pole (1) is installed, at the other parallel rule (3) that is equipped with of support (7); At support (7) rotating disk (13) is installed, rotating disk (13) can rotate, and by tightening screw (6) with its chucking; One end of steel wire tow line (8) is installed on the rotating disk (13), and the other end is installed on the horizontal steel pole (1) through three fixed pulleys (2) and a travelling block (9); Carrier fluid platform (11) hangs the below that is installed in travelling block (9), and fluid reservoir (10) places carrier fluid platform (11), is connected with rubber tube (12) in the bottom of fluid reservoir (10); The lower end of rubber tube (12) is connected with the bottom of intermediate receptacle (14); The top of intermediate receptacle (14) is provided with opening, is connected with pipeline (19), and the other end of pipeline (19) is connected with an end of core holding unit (16); The outlet of the pipeline (19) of core holding unit (16) other end is positioned at the top of graduated cylinder (20); In the inside of core holding unit (16) low permeability cores (18) is housed.
2. a kind of low permeability cores starting pressure gradient proving installation according to claim 1 is characterized in that movable steel pole (4) can slide up and down, and is fixed by tightening up screw (5) in support (7).
3. a kind of low permeability cores starting pressure gradient proving installation according to claim 2 is characterized in that being connected to confined pressure pump (17) in the outside of core holding unit (16).
CN2013101952712A 2013-05-23 2013-05-23 Low-permeability rock core start-up pressure gradient testing device Pending CN103278430A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013101952712A CN103278430A (en) 2013-05-23 2013-05-23 Low-permeability rock core start-up pressure gradient testing device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013101952712A CN103278430A (en) 2013-05-23 2013-05-23 Low-permeability rock core start-up pressure gradient testing device

Publications (1)

Publication Number Publication Date
CN103278430A true CN103278430A (en) 2013-09-04

Family

ID=49061014

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2013101952712A Pending CN103278430A (en) 2013-05-23 2013-05-23 Low-permeability rock core start-up pressure gradient testing device

Country Status (1)

Country Link
CN (1) CN103278430A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104297126A (en) * 2014-10-17 2015-01-21 中国石油天然气股份有限公司 Device and method applied to measurement of low-permeability reservoir gas seepage start-up pressure gradient
CN106124381A (en) * 2016-06-21 2016-11-16 河南理工大学 Hypotonic coal seam reservoirs gas free-boundary problem and the on-the-spot test method of permeability
CN106324212A (en) * 2015-06-19 2017-01-11 中国石油化工股份有限公司 Quick testing device and method of rock core gas start pressure
CN106918541A (en) * 2017-03-20 2017-07-04 中海石油(中国)有限公司 Fluid starts in a kind of observation seepage environment measurement apparatus and method
US10801943B2 (en) 2017-06-26 2020-10-13 China University Of Petroleum-Beijing Apparatus and method for measuring apparent permeability of tight rock core

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH041555A (en) * 1990-04-17 1992-01-07 Hosokawa Micron Corp Measuring instrument for liquid penetration speed to power and granular material
CN101852714A (en) * 2010-04-30 2010-10-06 中国石油大学(北京) Measuring system and method of low-speed non-linear seepage parameters
CN101968423A (en) * 2009-07-27 2011-02-09 中国石油天然气股份有限公司 Low-permeability reservoir bed starting pressure testing method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH041555A (en) * 1990-04-17 1992-01-07 Hosokawa Micron Corp Measuring instrument for liquid penetration speed to power and granular material
CN101968423A (en) * 2009-07-27 2011-02-09 中国石油天然气股份有限公司 Low-permeability reservoir bed starting pressure testing method
CN101852714A (en) * 2010-04-30 2010-10-06 中国石油大学(北京) Measuring system and method of low-speed non-linear seepage parameters

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
陈志明 等: "低渗透岩石渗流规律的实验研究方法综述", 《新疆石油科技》, vol. 22, no. 2, 31 December 2012 (2012-12-31), pages 29 - 31 *
陈志明 等: "低渗透油藏启动压力梯度的研究方法", 《石油化工应用》, vol. 31, no. 7, 31 July 2012 (2012-07-31), pages 7 - 10 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104297126A (en) * 2014-10-17 2015-01-21 中国石油天然气股份有限公司 Device and method applied to measurement of low-permeability reservoir gas seepage start-up pressure gradient
CN104297126B (en) * 2014-10-17 2016-08-31 中国石油天然气股份有限公司 low permeability reservoir gas seepage starting pressure gradient measuring device and measuring method
CN106324212A (en) * 2015-06-19 2017-01-11 中国石油化工股份有限公司 Quick testing device and method of rock core gas start pressure
CN106124381A (en) * 2016-06-21 2016-11-16 河南理工大学 Hypotonic coal seam reservoirs gas free-boundary problem and the on-the-spot test method of permeability
CN106918541A (en) * 2017-03-20 2017-07-04 中海石油(中国)有限公司 Fluid starts in a kind of observation seepage environment measurement apparatus and method
US10801943B2 (en) 2017-06-26 2020-10-13 China University Of Petroleum-Beijing Apparatus and method for measuring apparent permeability of tight rock core

Similar Documents

Publication Publication Date Title
CN204286989U (en) A kind of shale gas device for testing diffusion coefficient
CN103278430A (en) Low-permeability rock core start-up pressure gradient testing device
CN105203705B (en) A kind of heavy component deposition causes the method for testing of reservoir damage
CN203658217U (en) Seepage starting pressure gradient test device
CN109443867B (en) The method that the physical parameter of a kind of pair of tight rock is continuously detected
CN104359819A (en) Device and method for determining gas-water relative permeability of low-infiltration dense rock core
CN202033067U (en) Solid volume measurement instrument
CN104677771A (en) Magnetic levitation weight method-based method for determining porosity of shale
CN104237098A (en) Method for measuring gradient of rock starting pressure
CN106501151B (en) A kind of shale aperture measurement device and method based on imbibition and ion diffusion property
CN104897514A (en) Device for measuring danks surface gas adsorption and danks desorption curves
CN104237099A (en) Device and method for determining radial permeability of compact rock core
CN102621034A (en) Reservoir capillary pressure curve determinator under high temperature and pressure
CN109580454B (en) Method for testing fluid sensitivity of tight reservoir by using pressure oscillation method
CN205620277U (en) Novel spontaneous displacement of reservoir oil of rock core is measured device
CN204718916U (en) A kind of device measuring coal/shale surface gas absorption and desorption curve
CN204649586U (en) A kind of Oil in Super-low Permeability rock core leads to nitrogen water two-phase relative permeability determinator
CN105319153A (en) Measuring method of liquid full pressure gradient-flow relation in low-permeability reservoir
CN204267017U (en) A kind of oil-water separation metering device
CN105424545A (en) Determination method and device for air content of sediment of natural gas hydrate
CN202710435U (en) Device for measuring density of soil by using electronic balance
CN103149137A (en) Constant-pressure steady-state gas permeability measuring instrument
CN205138969U (en) Test device of semi -automatization soil capillary rising degree on water and speed
CN106949942A (en) The calibration method of its measurement oil tank outage of oil truck capacity calibrating installation and application
CN203164080U (en) Capillary micro-channel densimeter based on molecular surface tension of liquid

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
AD01 Patent right deemed abandoned

Effective date of abandoning: 20160106

C20 Patent right or utility model deemed to be abandoned or is abandoned