CN204319833U - A kind of macroporous resin adsorption separator - Google Patents
A kind of macroporous resin adsorption separator Download PDFInfo
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- CN204319833U CN204319833U CN201420679581.1U CN201420679581U CN204319833U CN 204319833 U CN204319833 U CN 204319833U CN 201420679581 U CN201420679581 U CN 201420679581U CN 204319833 U CN204319833 U CN 204319833U
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- tank body
- macroreticular resin
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- liquid
- feed tube
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Abstract
The utility model discloses a kind of macroporous resin adsorption separator, it is primarily of tank body, feed tube, drain pipe, circulation pipe composition, two-layer macroreticular resin is provided with in tank body, the left side of tank body is provided with two feed tubes, and one is liquid feed tube, the zeolite regeneration liquid feed tube of another root, one end of zeolite regeneration liquid feed tube is provided with three imports, the other end directly connects tank body top, and the right side of described tank body is provided with circulation pipe, and the lower end of tank body is provided with drain pipe.The utility model has the following advantages: in tank body, arrange two-layer macroreticular resin layer, upper strata macroreticular resin layer and lower floor's macroreticular resin layer, and adsorption effect is better; Be provided with water circulating pump, liquid constantly circulated in tank body, fully contacts with macroreticular resin, improve adsorption rate; One end of pipe liquid feed tube is provided with liquid import, and the other end is connected to tank interior from tank body top, and arranges a vertical with it water distributor at port, liquid can be made evenly by macroreticular resin, fully contact.
Description
Technical field
The utility model relates to a kind of adsorption separation device, particularly a kind of macroporous resin adsorption separator, belongs to medicine purification & isolation field.
Background technology
Effective Component of Chinese Medicine and effective population are the material bases of China's traditional Chinese medicine disease therapy for thousands of years.In plant, composition is comparatively complicated, and think that cellulose, chlorophyll, natural gum and inorganic salts etc. are for invalid components at present, active ingredient has alkaloid, flavonoids, organic acid, amino acid, cumarin etc.Effective component extracting and effective population are then conducive to reducing former drug toxicity, improve curative effect of medication; Improve dosage, production control quality; Expand Chinese herbal medicine resource; Carry out chemistry can become or structure of modification; Explore the principle that Chinese herbal medicine is cured the disease; All significant to the promotion aspect such as study of tcm new drug and the modernization of Chinese medicine.
Traditional Chinese medicine extraction separation is the design such as existence, polarity, dissolubility science, reasonable, a feasible technique according to Effective Component of Chinese Medicine and effective population, adopts a series of isolation technics.In recent years along with the fast development of modernization IE, the high-new engineering of some modernizations is just constantly used for reference to traditional Chinese medicine extraction separating technology.
Utility model content
The technical problems to be solved in the utility model, is to provide a kind of macroporous resin adsorption separator.
The utility model is realized by following proposal: a kind of macroporous resin adsorption separator, it is primarily of tank body, feed tube, drain pipe, circulation pipe forms, two-layer macroreticular resin is provided with: upper strata macroreticular resin and lower floor's macroreticular resin in described tank body, macroreticular resin upper end, described upper strata is provided with upper strata macroreticular resin import, lower end is provided with upper strata macroreticular resin outlet, described lower floor's macroreticular resin upper end is provided with lower floor's macroreticular resin import, lower end is provided with lower floor's macroreticular resin outlet, the left side of described tank body is provided with two feed tubes, one is liquid feed tube, the zeolite regeneration liquid feed tube of another root, one end of described liquid feed tube is provided with liquid import, the other end is connected to tank interior from tank body top, and a vertical with it water distributor is set at port, liquid can be made evenly to pass through macroreticular resin, abundant contact, one end of described zeolite regeneration liquid feed tube is provided with three imports, distilled water import respectively, eluent import, regenerated liquid import, the other end directly connects tank body top, the right side of described tank body is provided with circulation pipe, described circulation pipe is provided with circulating pump, the lower end of described tank body is provided with drain pipe, one end of described drain pipe is provided with liquid outlet.
Described tank body upper left-hand is provided with vacuum orifice, the pressure of tank interior can be extracted out.
Described tank body upper right is provided with Pressure gauge, can show the pressure of tank interior.
Be provided with liquid level gauge between described tank body and circulation pipe, liquid level counts transparent glass tube, can detect the height of the liquid of tank interior, and described liquid level gauge is provided with visor, directly can observe the internal environment of tank body.
The left lower of described tank body is provided with temperature and visits device, the temperature of detectable tank interior.
Be equipped with protection network under described upper strata macroreticular resin and lower floor's macroreticular resin, prevent macroreticular resin from revealing.
The import department of described circulation pipe is provided with screen pack, can prevent foreign material from entering circulation pipe.
Described tank base is provided with two supports.
Described liquid import, distilled water import, eluent import, regenerated liquid import, liquid outlet side are equipped with control valve.
The beneficial effects of the utility model are:
1. a kind of macroporous resin adsorption separator of the utility model arranges two-layer macroreticular resin layer in tank body, and upper strata macroreticular resin layer and lower floor's macroreticular resin layer, adsorption effect is better.
2. a kind of macroporous resin adsorption separator of the utility model is provided with water circulating pump, liquid is constantly circulated in tank body, fully contacts with macroreticular resin, improve adsorption rate.
3. the other end of the liquid feed tube of a kind of macroporous resin adsorption separator of the utility model is connected to tank interior from tank body top, and arranges a vertical with it water distributor at port, liquid can be made evenly by macroreticular resin, fully contact.
4. a kind of macroporous resin adsorption separator of the utility model is provided with liquid level gauge, and can detect the height of the liquid of tank interior, described liquid level gauge is provided with visor, directly can observe the internal environment of tank body.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of macroporous resin adsorption separator of the utility model;
In figure: 1 is tank body, 2 is liquid feed tube, 3 is drain pipe, 4 is circulation pipe, 5 is zeolite regeneration liquid feed tube, 6 is upper strata macroreticular resin, 7 is lower floor's macroreticular resin, 8 is upper strata macroreticular resin import, 9 is the outlet of upper strata macroreticular resin, the macroreticular resin import of 10 lower floors, 11 is lower floor's macroreticular resin outlet, 12 is liquid import, 13 is water distributor, 14 is distilled water import, 15 is eluent import, 16 is regenerated liquid import, 17 is circulating pump, 18 is liquid outlet, 19 vacuum orifices, 20 is Pressure gauge, 21 is visor, 22 is liquid level gauge, 23 is that temperature visits device, 24 is protection network, 25 is control valve, 26 is screen pack, 27 is support.
Detailed description of the invention
Below in conjunction with Fig. 1, the utility model is further illustrated:
A kind of macroporous resin adsorption separator, it is primarily of tank body 1, feed tube, drain pipe 3, circulation pipe 4 forms, two-layer macroreticular resin is provided with: upper strata macroreticular resin 6 and lower floor's macroreticular resin 7 in tank body 1, upper strata macroreticular resin 6 upper end is provided with upper strata macroreticular resin import 8, lower end is provided with upper strata macroreticular resin outlet 9, lower floor's macroreticular resin 7 upper end is provided with lower floor's macroreticular resin import 10, lower end is provided with lower floor's macroreticular resin outlet 11, upper strata macroreticular resin 6 and lower floor's macroreticular resin are equipped with protection network 24 7 times, prevent macroreticular resin from revealing, the left side of tank body 1 is provided with two feed tubes, one is liquid feed tube 2, the zeolite regeneration liquid feed tube 5 of another root, one end of liquid feed tube 2 is provided with liquid import 12, the other end is connected to tank body 1 from tank body 1 top inner, and a vertical with it water distributor 13 is set at port, liquid can be made evenly to pass through macroreticular resin, abundant contact, one end of zeolite regeneration liquid feed tube 5 is provided with three imports, distilled water import 14 respectively, eluent import 15, regenerated liquid import 16, the other end directly connects tank body 1 top, the right side of tank body 1 is provided with circulation pipe 4, circulation pipe 4 is provided with circulating pump 17, the import department of circulation pipe 4 is provided with screen pack 26, can prevent foreign material from entering circulation pipe 4, the lower end of tank body 1 is provided with drain pipe 3, one end of drain pipe 3 is provided with liquid outlet 18, tank body 1 upper left-hand is provided with vacuum orifice 19, the pressure of tank body 1 inside can be extracted out, tank body 1 upper right is provided with Pressure gauge 20, the pressure of tank body 1 inside can be shown, liquid level gauge 22 is provided with between tank body 1 and circulation pipe 4, liquid level gauge 22 is transparent glass tube, the height of the liquid of tank body 1 inside can be detected, liquid level gauge 22 is provided with visor 21, directly can observe the internal environment of tank body 1, the left lower of tank body 1 is provided with temperature and visits device 23, the temperature of detectable tank body 1 inside, two supports 27 are provided with bottom tank body 1, liquid import 12, distilled water import 14, eluent import 15, regenerated liquid import 16, liquid outlet 18 is other is equipped with control valve 25.
It is below the course of work of a kind of macroporous resin adsorption separator of the utility model.
Adsorption process: liquid to be processed is entered liquid feed tube 2 by liquid import 12, two-layer macroreticular resin layer is evenly entered by water distributor 13, now close the control valve 25 of liquid outlet 18, ON cycle pump 17, until the amount of leakage of liquid outlet 18 reaches respective standard, then open the control valve 25 of liquid outlet 18, complete adsorption process.
Elution process: inject eluent by eluent import 15, general employing 0-90 ethanol gradient elution, eluent is flowed out by liquid outlet 18, collects eluent, concentrates, and namely obtains the required material be separated.
Regenerative process: first inject ethanol by regenerated liquid import 16, until liquid outlet 18 trickle is colourless, then injects distilled water by distilled water import 14, is washed till neutrality, completes regenerative process with distilled water, and after regeneration, macroreticular resin can reuse.
Although done comparatively detailed elaboration to the technical solution of the utility model and enumerated; be to be understood that; to those skilled in the art; amendment is made to above-described embodiment or adopts equivalent replacement scheme; this is apparent to those skilled in the art; these modifications or improvements on the basis of not departing from the utility model spirit, all belong to the scope that the utility model is claimed.
Claims (9)
1. a macroporous resin adsorption separator, it is primarily of tank body (1), feed tube, drain pipe (3), circulation pipe (4) forms, it is characterized in that: described tank body is provided with two-layer macroreticular resin in (1): upper strata macroreticular resin (6) and lower floor's macroreticular resin (7), macroreticular resin (6) upper end, described upper strata is provided with upper strata macroreticular resin import (8), lower end is provided with upper strata macroreticular resin outlet (9), described lower floor macroreticular resin (7) upper end is provided with lower floor's macroreticular resin import (10), lower end is provided with lower floor's macroreticular resin outlet (11), the left side of described tank body (1) is provided with two feed tubes, one is liquid feed tube (2), the zeolite regeneration liquid feed tube (5) of another root, one end of described liquid feed tube (2) is provided with liquid import (12), the other end is connected to tank body (1) from tank body (1) top inner, and a vertical with it water distributor (13) is set at port, one end of described zeolite regeneration liquid feed tube (5) is provided with three imports, distilled water import (14) respectively, eluent import (15), regenerated liquid import (16), the other end directly connects tank body (1) top, the right side of described tank body (1) is provided with circulation pipe (4), described circulation pipe (4) is provided with circulating pump (17), the lower end of described tank body (1) is provided with drain pipe (3), one end of described drain pipe (3) is provided with liquid outlet (18).
2. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: described tank body (1) upper left-hand is provided with vacuum orifice (19).
3. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: described tank body (1) upper right is provided with Pressure gauge (20).
4. a kind of macroporous resin adsorption separator according to claim 1, it is characterized in that: be provided with liquid level gauge (22) between described tank body (1) and circulation pipe (4), described liquid level gauge (22) is provided with visor (21).
5. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: the left lower of described tank body (1) is provided with temperature and visits device (23).
6. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: be equipped with protection network (24) under described upper strata macroreticular resin (6) and lower floor's macroreticular resin (7).
7. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: the import department of described circulation pipe (4) is provided with screen pack (26).
8. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: described tank body (1) bottom is provided with two supports (27).
9. a kind of macroporous resin adsorption separator according to claim 1, is characterized in that: described liquid import (12), distilled water import (14), eluent import (15), regenerated liquid import (16), liquid outlet (18) side are equipped with control valve (25).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420679581.1U CN204319833U (en) | 2014-11-12 | 2014-11-12 | A kind of macroporous resin adsorption separator |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420679581.1U CN204319833U (en) | 2014-11-12 | 2014-11-12 | A kind of macroporous resin adsorption separator |
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| CN204319833U true CN204319833U (en) | 2015-05-13 |
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| CN201420679581.1U Expired - Fee Related CN204319833U (en) | 2014-11-12 | 2014-11-12 | A kind of macroporous resin adsorption separator |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104307205A (en) * | 2014-11-12 | 2015-01-28 | 成都彼斯特生物科技有限公司 | Macroporous resin adsorption-separation device |
| CN105617715A (en) * | 2016-01-18 | 2016-06-01 | 江西中天医药生物有限公司 | Method for removing arsenic from termite extracts by virtue of adsorption of novel resin |
| CN114053756A (en) * | 2021-11-06 | 2022-02-18 | 江苏龙泰环保设备制造有限公司 | Macroporous resin adsorption device |
-
2014
- 2014-11-12 CN CN201420679581.1U patent/CN204319833U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104307205A (en) * | 2014-11-12 | 2015-01-28 | 成都彼斯特生物科技有限公司 | Macroporous resin adsorption-separation device |
| CN105617715A (en) * | 2016-01-18 | 2016-06-01 | 江西中天医药生物有限公司 | Method for removing arsenic from termite extracts by virtue of adsorption of novel resin |
| CN114053756A (en) * | 2021-11-06 | 2022-02-18 | 江苏龙泰环保设备制造有限公司 | Macroporous resin adsorption device |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150513 Termination date: 20181112 |
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| CF01 | Termination of patent right due to non-payment of annual fee |