CN203090525U - Effective plant extract absorbing device - Google Patents
Effective plant extract absorbing device Download PDFInfo
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- CN203090525U CN203090525U CN 201320118679 CN201320118679U CN203090525U CN 203090525 U CN203090525 U CN 203090525U CN 201320118679 CN201320118679 CN 201320118679 CN 201320118679 U CN201320118679 U CN 201320118679U CN 203090525 U CN203090525 U CN 203090525U
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- cylindrical container
- cylindrical
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Abstract
The utility model relates to an effective plant extract absorbing device. The device comprises cylindrical containers, wherein an upper sealing end cover and a lower sealing end cover are arranged on each cylindrical container; a liquid inlet is formed in the upper sealing end cover of each cylindrical container and connected with a liquid inlet pipeline; a liquid outlet is formed in the lower sealing end cover of each cylindrical container and connected with a liquid outlet pipeline; macroporous adsorption resin is filled in each cylindrical container; the cylindrical containers containing the macroporous adsorption resin are vertically installed on a rack; the rack comprises a fixed base and a movable support frame; the movable support frame can be rotatably put down and hinged with the fixed base; a hydraulic cylinder is hinged between the movable support frame and the fixed base; a plurality of cylindrical containers are fixed on the movable support frame and connected between the liquid inlet pipeline and the liquid outlet pipeline in series and parallel through valves. Adsorbents can be simply loaded and unloaded in the device, and disposable fillers can be loaded in the device, so that the device has high column efficiency; and the device is simple in structure and low in production cost.
Description
Technical field
The utility model relates to separation technology field, is specifically related to a kind of plant extract active ingredient adsorbent equipment.
Background technology
During China's Chinese medicine is produced at present, extracting separating and purifying technology has water extraction and alcohol precipitation method, ethanol extract from water precipitation, acid-base precipitation method etc. comparatively simply to extract purification technique, but simple extract separation and purification thing that purification technique obtains to contain impurity such as protein, polysaccharide, polypeptide, tannin, thermal source many through this, become the modernization of Chinese medicine and moved towards the technical bottleneck of international market.
Along with the development of technology, with adsorbents adsorb active ingredient, the technology of removing impurity is widely used in the production process of biogenetic products, and whether proper the adsorption process of this workshop section solves will directly influence the yield of product.Adsorbent equipment select then particular importance for use.Existing adsorbent equipment: the adsorbent charging and discharging mouth of chromatographic column is separately positioned on the upper and lower side of chromatographic column; the charging and discharging mouth bore that is used for adsorbent is little; filling, unloading to adsorbent are loaded down with trivial details; the bigger chromatographic column of diameter of using on the industrial production and volume particularly; because diameter and volume that this chromatographic column is used are bigger; for production safety, chromatographic column can be fixed on fixing support rack tightly usually, avoid causing casualties and the waste of soup etc. because of chromatographic column collapses.And the charging aperture of chromatographic column is arranged on the chromatographic column upper end, filling to adsorbent is loaded down with trivial details, can not carry out the filling of disposable filler, exist post to imitate problems such as not high, application number is a kind of chromatographic column of 201210284654.2, though this chromatographic column to the unloading of adsorbent and clean more convenient, its complex structure, manufacturing cost height.
Summary of the invention
The purpose of this utility model is at the deficiencies in the prior art, and a kind of plant extract active ingredient adsorbent equipment is provided, and its filling to adsorbent, unloading simply can be carried out the filling of disposable filler, and post is imitated high, and it is simple in structure, low cost of manufacture.
The purpose of this utility model is achieved in that a kind of plant extract active ingredient adsorbent equipment, comprise cylindrical container, described cylindrical container is provided with end cover and lower seal end cap, inlet is set on the last end cover of cylindrical container to be connected with the feed liquor pipeline, liquid outlet is set on the lower seal end cap of cylindrical container to be connected with the fluid pipeline, be filled with macroporous absorbent resin in the cylindrical container, the cylindrical container that macroporous absorbent resin is housed all vertically is installed on the frame, described frame comprises firm banking and movable support frame, described movable support frame is rotatable to be hinged on the firm banking with falling, be hinged with hydraulic cylinder between movable support frame and the firm banking, fix a plurality of cylindrical containers on the described movable support frame, a plurality of cylindrical containers pass through the valve series-parallel connection between feed liquor pipeline and fluid pipeline.
The last end cover and the lower seal end cap of described cylindrical container are hemispherical shell, be connected by flange respectively between the cylindrical shell of cylindrical container and the two halves spherical shell, the cylindrical shell top of described cylindrical container is provided with visor, described hemispherical shell is provided with filter mesh layer, is provided with sealing gasket between the cylindrical shell of described cylindrical container and the two halves spherical shell.
The top of the last end cover of described cylindrical container is provided with check-valves.
The cylinder body of described hydraulic cylinder is hinged on the firm banking, the hinged movable support frame of the axis of the piston of hydraulic cylinder, and the axis of the piston by hydraulic cylinder fell movable support frame or was supported on the firm banking.
The inlet of a plurality of cylindrical containers all connects the feed liquor pipeline by valve, the liquid outlet of a plurality of cylindrical containers all connects the fluid pipeline by valve, form a plurality of cylindrical containers and be connected in parallel on structure between feed liquor pipeline and the fluid pipeline, the liquid outlet of one cylindrical container connects the inlet of another cylindrical container by valve, forms a plurality of cylindrical containers and is connected on structure between feed liquor pipeline and the fluid pipeline.
Described liquid inlet and outlet pipeline laying is on movable support frame.
The beneficial effects of the utility model are: owing to adopt technique scheme, be hinged with hydraulic cylinder between movable support frame and the firm banking.When needs filling, unloading adsorbent, the control hydraulic cylinder fell movable support frame on firm banking, and last end cover and the lower seal end cap of opening cylindrical container load, unload adsorbent.This structure makes the utility model to adsorbent easy accessibility, quick.
Fix a plurality of cylindrical containers on the described movable support frame, a plurality of cylindrical containers pass through the valve series-parallel connection between feed liquor pipeline and fluid pipeline, control the flow velocity of feed liquid by by-pass valve control, guarantee the optimum flow rate that macroporous absorbent resin absorption requires, reach best adsorption effect.When a plurality of cylindrical containers are connected in parallel between feed liquor pipeline and the fluid pipeline by valve, can be under low linear flow rate, carry out big flow operation, compare with prior art, flow velocity can improve 5-10 doubly, also is convenient to amplify at the enterprising line linearity in existing technology basis, enhance productivity, shorten disengaging time, make product keep high activity, high yield, remarkable in economical benefits.When a plurality of cylindrical containers are connected between feed liquor pipeline and the fluid pipeline by valve, be convenient to feed liquid is carried out multiple adsorb, adsorbent is fully adsorbed the active ingredient in the feed liquid, improve the filler utilization rate, make the unit volume filler reach high bound.
Be filled with macroporous absorbent resin in the cylindrical container, the physicochemical property of macroporous absorbent resin is stable, and its main feature is porous and higher specific surface area, advantages of good adsorption effect.
The top of the last end cover of described cylindrical container is provided with check-valves.Opens check valve, the bubble that adsorption process is produced in time discharges, and prevents that bubble is to the liquid distribution of eluant, eluent and the influence of separating effect, and also can avoid liquid in container when effluxing, internal tank forms negative pressure, produces vacuum phenomenon, thereby prevents that container from deforming or ftractureing.
Description of drawings
Fig. 1 is a structural representation of the present utility model;
Fig. 2 is that the A of Fig. 1 is to view;
Fig. 3 is the P portion enlarged drawing of Fig. 2.
In the accompanying drawing, 1 is cylindrical container, and 2 is last end cover, and 3 is the lower seal end cap, and 4 is firm banking, 5 is movable support frame, and 6 is hydraulic cylinder, and 7 is valve, and 8 is visor, and 9 is filter mesh layer, 10 is sealing gasket, and 11 is check-valves, and 12 is the feed liquor pipeline, and 13 is the fluid pipeline.
The specific embodiment
Referring to Fig. 1 to Fig. 3, a kind of plant extract active ingredient adsorbent equipment, comprise cylindrical container 1, described cylindrical container 1 is provided with end cover 2 and lower seal end cap 3, the last end cover and the lower seal end cap of the described cylindrical container of present embodiment are hemispherical shell, said hemispherical shell is not proper hemispherical shell, can be smaller part elliposoidal housing or other.Be connected by flange respectively between the cylindrical shell of cylindrical container and the two halves spherical shell, the cylindrical shell top of described cylindrical container 1 is provided with visor 8, by the top visor observe feed liquid reach need liquid level after, close the feed liquor pipeline.Described hemispherical shell is provided with filter mesh layer 9, is provided with sealing gasket 10 between the cylindrical shell of described cylindrical container and the two halves spherical shell.The top of the last end cover 2 of described cylindrical container 1 is provided with check-valves 11.Opens check valve, the bubble that adsorption process is produced in time discharges, and prevents that bubble is to the liquid distribution of eluant, eluent and the influence of separating effect, and also can avoid liquid in container when effluxing, internal tank forms negative pressure, produces vacuum phenomenon, thereby prevents that container from deforming or ftractureing.Inlet is set on the last end cover 2 of cylindrical container 1 is connected, liquid outlet is set on the lower seal end cap 3 of cylindrical container 1 is connected with fluid pipeline 13 with feed liquor pipeline 12.Be filled with macroporous absorbent resin in the cylindrical container 1, the physicochemical property of macroporous absorbent resin is stable, and its main feature is porous and higher specific surface area, advantages of good adsorption effect.The cylindrical container 1 that macroporous absorbent resin is housed all vertically is installed on the frame, described frame comprises firm banking 4 and movable support frame 5, described firm banking 4 by bolting on the ground, described movable support frame 5 is made of some crossbeams and longeron, described movable support frame 5 is hinged on the firm banking 4 by bearing pin, and movable support frame can rotate and fell on firm banking.Be hinged with hydraulic cylinder 6 between movable support frame 5 and the firm banking 4.Wherein, the cylinder body of described hydraulic cylinder 6 is hinged on the firm banking 4 by bearing pin, and the axis of the piston of hydraulic cylinder 6 is by the hinged movable support frame 5 of bearing pin, and the axis of the piston by hydraulic cylinder fell movable support frame 5 or was supported on the firm banking 4.Preferably, described hydraulic cylinder is two, and two corresponding respectively both sides that are arranged on movable support frame one side of hydraulic cylinder.Certainly the utility model also can be provided with one or three hydraulic cylinders.Fix a plurality of cylindrical containers 1 on the described movable support frame 5, a plurality of cylindrical containers 1 pass through valve 7 series-parallel connections between feed liquor pipeline 12 and fluid pipeline 13.Control the flow velocity of feed liquid by by-pass valve control, guarantee the optimum flow rate that macroporous absorbent resin absorption requires, reach best adsorption effect.Wherein, the inlet of a plurality of cylindrical containers 1 all connects feed liquor pipeline 12 by valve, the liquid outlet of a plurality of cylindrical containers 1 all connects fluid pipeline 13 by valve, forms a plurality of cylindrical containers 1 and is connected in parallel on structure between feed liquor pipeline 12 and the fluid pipeline 13.When a plurality of cylindrical containers are connected in parallel between feed liquor pipeline and the fluid pipeline by valve, can be under low linear flow rate, carry out big flow operation, compare with prior art, flow velocity can improve 5-10 doubly, also is convenient to amplify at the enterprising line linearity in existing technology basis, enhance productivity, shorten disengaging time, make product keep high activity, high yield, remarkable in economical benefits.The liquid outlet of one cylindrical container connects the inlet of another cylindrical container by valve, forms a plurality of cylindrical containers 1 and is connected on structure between feed liquor pipeline 12 and the fluid pipeline 13.When a plurality of cylindrical containers are connected between feed liquor pipeline and the fluid pipeline by valve, be convenient to feed liquid is carried out multiple adsorb, adsorbent is fully adsorbed the active ingredient in the feed liquid, improve the filler utilization rate, make the unit volume filler reach high bound.The cylindrical container of present embodiment is four, the inlet of four cylindrical containers connects the feed liquor pipeline by first, second, third and fourth valve respectively, the liquid outlet of four cylindrical containers all connects the fluid pipeline by the 5th, six, seven, eight valves, the liquid outlet of first cylindrical container connects the inlet of first cylindrical container by the 9th valve, the liquid outlet of second cylindrical container connects the inlet of three cylindrical shape container by the tenth valve, and the liquid outlet of the 11 cylindrical container connects the inlet of the 4th cylindrical container by the 3rd valve.Certainly the utility model can also be provided with two or more cylindrical containers according to actual needs.Described liquid inlet and outlet pipeline 12,13 is laid on the movable support frame 5.
The underframe of movable support frame is provided with fixing hole.When needs filling, unloading adsorbent, unclamp the bolt in the fixing hole of underframe of movable support frame, the control hydraulic cylinder fell movable support frame on firm banking, and last end cover and the lower seal end cap of opening cylindrical container load, unload adsorbent.After filling, unloading were finished, the control hydraulic cylinder was supported on movable support frame on the firm banking, by bolt movable support frame tightly is fixed on the firm banking then.This structure makes the utility model to adsorbent easy accessibility, quick.
The utility model is exclusively used in the extraction of moulting hormone, the moulting hormone soup that extracts enters the cylindrical container that macroporous absorbent resin is housed by the feed liquor pipeline, macroporous absorbent resin directly adsorbs the effective ingredient in the moulting hormone soup, and useless composition is drained by the fluid pipeline with soup.And then feed eluent by the feed liquor pipeline, and the moulting hormone of macroporous resin adsorption is desorbed, will be rich in the technological process that the eluent output of moulting hormone enters next step by the fluid pipeline.
Claims (6)
1. plant extract active ingredient adsorbent equipment, comprise cylindrical container, it is characterized in that: described cylindrical container is provided with end cover and lower seal end cap, inlet is set on the last end cover of cylindrical container to be connected with the feed liquor pipeline, liquid outlet is set on the lower seal end cap of cylindrical container to be connected with the fluid pipeline, be filled with macroporous absorbent resin in the cylindrical container, the cylindrical container that macroporous absorbent resin is housed all vertically is installed on the frame, described frame comprises firm banking and movable support frame, described movable support frame is rotatable to be hinged on the firm banking with falling, be hinged with hydraulic cylinder between movable support frame and the firm banking, fix a plurality of cylindrical containers on the described movable support frame, a plurality of cylindrical containers pass through the valve series-parallel connection between feed liquor pipeline and fluid pipeline.
2. plant extract active ingredient adsorbent equipment according to claim 1, it is characterized in that: the last end cover and the lower seal end cap of described cylindrical container are hemispherical shell, be connected by flange respectively between the cylindrical shell of cylindrical container and the two halves spherical shell, the cylindrical shell top of described cylindrical container is provided with visor, described hemispherical shell is provided with filter mesh layer, is provided with sealing gasket between the cylindrical shell of described cylindrical container and the two halves spherical shell.
3. plant extract active ingredient adsorbent equipment according to claim 1 and 2, it is characterized in that: the top of the last end cover of described cylindrical container is provided with check-valves.
4. plant extract active ingredient adsorbent equipment according to claim 1, it is characterized in that: the cylinder body of described hydraulic cylinder is hinged on the firm banking, the hinged movable support frame of the axis of the piston of hydraulic cylinder, the axis of the piston by hydraulic cylinder fell movable support frame or was supported on the firm banking.
5. plant extract active ingredient adsorbent equipment according to claim 1, it is characterized in that: the inlet of a plurality of cylindrical containers all connects the feed liquor pipeline by valve, the liquid outlet of a plurality of cylindrical containers all connects the fluid pipeline by valve, form a plurality of cylindrical containers and be connected in parallel on structure between feed liquor pipeline and the fluid pipeline, the liquid outlet of one cylindrical container connects the inlet of another cylindrical container by valve, forms a plurality of cylindrical containers and is connected on structure between feed liquor pipeline and the fluid pipeline.
6. plant extract active ingredient adsorbent equipment according to claim 1 is characterized in that: described liquid inlet and outlet pipeline laying is on movable support frame.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320118679 CN203090525U (en) | 2013-03-15 | 2013-03-15 | Effective plant extract absorbing device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320118679 CN203090525U (en) | 2013-03-15 | 2013-03-15 | Effective plant extract absorbing device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203090525U true CN203090525U (en) | 2013-07-31 |
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ID=48841971
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201320118679 Expired - Lifetime CN203090525U (en) | 2013-03-15 | 2013-03-15 | Effective plant extract absorbing device |
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| Country | Link |
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| CN (1) | CN203090525U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109847404A (en) * | 2019-01-16 | 2019-06-07 | 云南通海杨氏天然产物有限公司 | Novel and multifunctional enrichment huge pillar and its application |
| CN116173918A (en) * | 2022-11-28 | 2023-05-30 | 中触媒新材料股份有限公司 | Capture agent and system for purifying mixed cresol separation desorbent |
-
2013
- 2013-03-15 CN CN 201320118679 patent/CN203090525U/en not_active Expired - Lifetime
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109847404A (en) * | 2019-01-16 | 2019-06-07 | 云南通海杨氏天然产物有限公司 | Novel and multifunctional enrichment huge pillar and its application |
| CN109847404B (en) * | 2019-01-16 | 2020-09-18 | 云南通海杨氏天然产物有限公司 | Multifunctional enrichment large column and application thereof |
| CN116173918A (en) * | 2022-11-28 | 2023-05-30 | 中触媒新材料股份有限公司 | Capture agent and system for purifying mixed cresol separation desorbent |
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| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20130731 |