CN204261381U - Ultrasonic wave form selenium separator - Google Patents
Ultrasonic wave form selenium separator Download PDFInfo
- Publication number
- CN204261381U CN204261381U CN201420627883.4U CN201420627883U CN204261381U CN 204261381 U CN204261381 U CN 204261381U CN 201420627883 U CN201420627883 U CN 201420627883U CN 204261381 U CN204261381 U CN 204261381U
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- ultrasonic wave
- resin column
- hopper
- control system
- computer controller
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Abstract
Ultrasonic wave form selenium separator, it is characterized in that structure: polyflon post is settled at ultrasonic wave hopper center, ultrasonic wave hopper periphery arranges protective cover, high frequency ultrasound wave producer is arranged between ultrasonic wave hopper outer wall and protective cover, water inlet pipe and the magnetic valve of recirculated cooling water are installed bottom ultrasonic wave hopper, ultrasonic wave hopper are joined overflow pipe and fluid temperature sensor; Liquid level sensor in material liquid entrance, eluent entrance and resin column is settled on resin column top, and bottom resin column, configuration controls resin column internal drainage flow sensor and draining adjustable electromagnetic valve; Material liquid basin, eluent basin by pipeline connection fat post, and have topping-up pump; Pump on each equipment, valve, sensor and actor part are connected with the circuit module of each control system by wire by computer controller.Have that the purity being separated different shape selenium is high, separative efficiency is high, cost-saving, the feature that reduces environmental pollution.
Description
Technical field
The utility model belongs to the equipment that chemical substance is separated, particularly teaching testing device, be applied to the ultrasonic wave form selenium separator that variform selenium [Organic Selenium: albumen selenium and polysaccharide selenium etc., inorganic selenium: Se (IV) and Se (VI)] is separated.
Background technology
Traditional form selenium is separated, and animal or plant sample treatment is become solution and adsorbent mix and blend to adsorb, and then, is placed on by adsorbent in closed container and is placed in constant temperature oscillation machine and vibrates the adsorbent selenium of wash-out, then obtain product to after eluent process.The method separation purity is not high, separative efficiency is low, eluent consumption large, and harmful substance is volatile causes environmental pollution.Operated in accordance with conventional methods process need apparatus amount is large, numerous and diverse, (adsorbent to be taken out in container the dry raw material waste liquid of pouring, reload closed container constant temperature oscillation wash-out form selenium, drench again and dryly collect the operations such as eluent), equally also make this teaching testing device utensil consumption large, medicine waste is serious, because skilled operation degree is different, the yield difference of product is larger.
Summary of the invention
The utility model object is to provide a kind of ultrasonic wave form selenium separator, and overcome the deficiency that conventional method separation purity and separative efficiency are in the past low, can meet teaching test requirement, contaminated solution problem also can be applicable to industrial-scale production.
Ultrasonic wave form selenium separator of the present utility model, comprise computerized control system, automatic infusion system, high-frequency ultrasonic vibration heating, temperature control system and operation procedure control system, it is characterized in that cyclone separator arrangement: polyflon post is settled at ultrasonic wave hopper center, ultrasonic wave hopper periphery arranges protective cover, high frequency ultrasound wave producer is arranged between ultrasonic wave hopper outer wall and protective cover, water inlet pipe and the ultrasonic wave hopper recirculated water magnetic valve thereof of ultrasonic wave hopper recirculated cooling water are installed bottom ultrasonic wave hopper, fluid temperature sensor in the overflow pipe of ultrasonic wave hopper top configuration cycles cooling water and hopper, liquid level sensor in material liquid entrance, eluent entrance and resin column is settled on polyflon post top, and the configuration of polyflon column bottom controls resin column internal drainage flow sensor and resin column draining adjustable electromagnetic valve, material liquid basin, eluent basin by pipeline connection polyflon post, and arrange topping-up pump, pump on each equipment, valve, sensor and actor part are connected with the circuit module of each control system by wire by computer controller.The utility model ultrasonic wave form selenium separator, has that the purity being separated different shape selenium is high, separative efficiency is high, cost-saving, the feature that reduces environmental pollution.This separator is compared with conventional method: add controllability, decrease adsorbent in container, to take out the dry raw material waste liquid of pouring, reload closed container constant temperature oscillation wash-out form selenium, drench again and dryly collect the operations such as eluent, decrease the working time, reduce eluent consumption and post processing sewage cost.To extract different shape selenium in certain Blueberry, raw material state is identical, the different shape selenium that legacy equipment extracts, and 1.0kg blueberry can extract Organic Selenium 53.68mg, and because of the difference in operation, general purity is about 65% ~ 85%; And using this equipment 1.0kg blueberry can extract Organic Selenium 67.22mg, purity can reach more than 80% ~ 95%.
Accompanying drawing explanation
Fig. 1 is the device structure schematic diagram of the utility model ultrasonic wave form selenium separator;
Fig. 2 is that the circuit module that described ultrasonic wave form selenium splitter circuit controls connects schematic block diagram.
Detailed description of the invention
Ultrasonic wave form selenium separator, comprise computerized control system, automatic infusion system, high-frequency ultrasonic vibration heating and temperaturel control system, see Fig. 1, it is characterized in that structure: polyflon post 1 is settled at ultrasonic wave hopper 2 center, periphery arranges protective cover 3, high frequency ultrasound wave producer 8 is arranged between ultrasonic wave hopper 2 outer wall and protective cover 3, overflow pipe 6 is installed on ultrasonic wave hopper 2 top, ultrasonic wave hopper temperature sensor 7, hopper circulating water inlet 10 is installed bottom ultrasonic wave hopper 2, hopper recirculated water magnetic valve 9, resin column 1 top arranges liquid level sensor 5 in material liquid inlet pipe 4 and eluent inlet pipe 19 and resin column, the material liquid inlet pipe 4 of material liquid basin 15, the eluent inlet pipe 19 of eluent basin 16 arranges raw material liquid pump 18 respectively, wash-out liquid pump 17, configure configuration on the resin column draining flow sensor 12 of mensuration resin column draining flow velocity, pipeline in polyflon post 1 bottom discharge pipeline and control the resin column draining adjustable electromagnetic valve 11 of resin column internal drainage speed, the material liquid of the successively injection from resin column 1 upper end and eluent will share discharge outlet and discharge through resin column draining adjustable electromagnetic valve 11 in lower end, all electricity pieces are connected with computer operation table 14 by wire and sensor conductor 13.Magnetic valve is divided into complete folding type and adjustable type, all will use in this equipment different parts two kinds, if ultrasonic wave hopper recirculated water magnetic valve 9 and resin column draining adjustable electromagnetic valve 11 are exactly two kinds of different magnetic valves.
The electrical configurations of ultrasonic wave form selenium separator control system, as shown in Figure 2: the computerized control system in computer controller 14 comprises automatic infusion control system, high frequency ultrasound wave power, fluid temperature induction and automatic cycle water cooling control system in hopper, the measurement of rate of flow of resin column internal drainage and draining regulation and control system and operation procedure control system, it is characterized in that circuit connecting relation: the computerized control system circuit module in computer controller 14, computer controller 14 is called for short in block diagram 2, connect ultrasonic wave hopper temperature setting circuit and high-frequency ultrasonic power setting circuit respectively, computer controller 14 1 output is fixed on the high frequency ultrasound wave producer 8 of ultrasonic wave hopper 2 outer wall, computer controller 14 1 output is connected to the resin column draining adjustable electromagnetic valve 11 on the discharge pipe line of resin column 1 lower end, computer controller 14 1 output is connected to cooling water and enters ultrasonic wave hopper recirculated water magnetic valve 9 in ultrasonic wave hopper 2 pipeline, computer controller 14 1 output is connected to the wash-out liquid pump 17 between eluent basin 16 outlet and resin column 1, computer controller 14 1 output is connected to the raw material liquid pump 18 between raw material receiver 15 outlet and resin column 1, computer controller 14 1 input connects the liquid level sensor 5 on resin column 1, computer controller 14 1 input connects the ultrasonic wave hopper temperature sensor 7 of ultrasonic wave hopper 2, computer controller 14 1 input connects the resin column draining flow sensor 12 in resin column 1 pipeline, all forms loop be connected electrical part.
In resin column, flow rate of liquid controls: load in polyflon post by the adsorbent chosen, according to the adsorption effect of the adsorbent selected to different shape selenium and the elute effect of eluent, flow rate of liquid in setting resin column, under absorption and washing steps state, in resin column, flow rate of liquid is burst to controller by the draining flow sensor 12 in the drainage pipeline of resin column lower end is counter.All should carry out lab scale early stage to different raw materials in production operation, after obtaining absorption, elute effect scope, reset adsorbent amount, then according to adsorbent amount determination material liquid injection rate and eluent consumption.Flow rates value adjusts according to material characteristic, the flow velocity in post because of select adsorbent granule size, the consumption of adsorbent, adsorbent treatment effect in early stage relevant with factors such as the resin column diameters selected.
Claims (3)
1. ultrasonic wave form selenium separator, comprise computerized control system, automatic infusion system, high-frequency ultrasonic vibration heating, temperature control system and operation procedure control system, it is characterized in that cyclone separator arrangement: polyflon post is settled at ultrasonic wave hopper center, ultrasonic wave hopper periphery arranges protective cover, high frequency ultrasound wave producer is arranged between ultrasonic wave hopper outer wall and protective cover, water inlet pipe and the ultrasonic wave hopper recirculated water magnetic valve thereof of ultrasonic wave hopper recirculated cooling water are installed bottom ultrasonic wave hopper, fluid temperature sensor in the overflow pipe of ultrasonic wave hopper top configuration cycles cooling water and hopper, liquid level sensor in material liquid entrance, eluent entrance and resin column is settled on polyflon post top, and the configuration of polyflon column bottom controls resin column internal drainage flow sensor and resin column draining adjustable electromagnetic valve, material liquid basin, eluent basin by pipeline connection polyflon post, and arrange topping-up pump, pump on each equipment, valve, sensor and actor part are connected with the circuit module of each control system by wire by computer controller.
2. ultrasonic wave form selenium separator according to claim 1, it is characterized in that structure: polyflon post (1) is settled at ultrasonic wave hopper (2) center, periphery arranges protective cover (3), high frequency ultrasound wave producer (8) is arranged between ultrasonic wave hopper (2) outer wall and protective cover (3), overflow pipe (6) is installed on ultrasonic wave hopper (2) top, ultrasonic wave hopper temperature sensor (7), hopper circulating water inlet (10) is installed in ultrasonic wave hopper (2) bottom, hopper recirculated water magnetic valve (9), resin column (1) top arranges liquid level sensor (5) in material liquid inlet pipe (4) and eluent inlet pipe (19) and resin column, the material liquid inlet pipe (4) of material liquid basin (15), the eluent inlet pipe (19) of eluent basin (16) arranges raw material liquid pump (18) respectively, wash-out liquid pump (17), configure configuration on the resin column draining flow sensor (12) of mensuration resin column draining flow velocity, pipeline in polyflon post (1) bottom discharge pipeline and control the resin column draining adjustable electromagnetic valve (11) of resin column internal drainage speed, the material liquid of the successively injection from resin column (1) upper end and eluent will share discharge outlet and discharge through resin column draining adjustable electromagnetic valve (11) in lower end, all electricity pieces are connected with computer operation table (14) by wire and sensor conductor (13).
3. ultrasonic wave form selenium separator according to claim 1, it is characterized in that the electrical configurations of control system, circuit connecting relation: the computerized control system in computer controller (14) comprises automatic infusion control system, high frequency ultrasound wave power, fluid temperature induction and automatic cycle water cooling control system in hopper, the measurement of rate of flow of resin column internal drainage and draining regulation and control system and operation procedure control system, it is characterized in that circuit connecting relation: the computerized control system circuit module in computer controller (14), be called for short computer controller (14), connect ultrasonic wave hopper temperature setting circuit and high-frequency ultrasonic power setting circuit respectively, computer controller (14) one output is connected to the high frequency ultrasound wave producer (8) being fixed on ultrasonic wave hopper (2) outer wall, computer controller (14) one output is connected to the resin column draining adjustable electromagnetic valve (11) on the discharge pipe line of resin column (1) lower end, computer controller (14) one output is connected to cooling water and enters ultrasonic wave hopper recirculated water magnetic valve (9) in ultrasonic wave hopper (2) pipeline, computer controller (14) one output is connected to the wash-out liquid pump (17) between eluent basin (16) outlet and resin column (1), computer controller (14) one output is connected to the raw material liquid pump (18) between raw material receiver (15) outlet and resin column (1), computer controller (14) one input connects the liquid level sensor (5) on resin column (1), computer controller (14) one input connects the ultrasonic wave hopper temperature sensor (7) of ultrasonic wave hopper (2), computer controller (14) one input connects the resin column draining flow sensor (12) in resin column (1) pipeline, all forms loop be connected electrical part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420627883.4U CN204261381U (en) | 2014-10-27 | 2014-10-27 | Ultrasonic wave form selenium separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420627883.4U CN204261381U (en) | 2014-10-27 | 2014-10-27 | Ultrasonic wave form selenium separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204261381U true CN204261381U (en) | 2015-04-15 |
Family
ID=52796281
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420627883.4U Expired - Fee Related CN204261381U (en) | 2014-10-27 | 2014-10-27 | Ultrasonic wave form selenium separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204261381U (en) |
-
2014
- 2014-10-27 CN CN201420627883.4U patent/CN204261381U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150415 Termination date: 20191027 |