CN204247166U - A kind of internal heating type autoclave - Google Patents
A kind of internal heating type autoclave Download PDFInfo
- Publication number
- CN204247166U CN204247166U CN201420703764.2U CN201420703764U CN204247166U CN 204247166 U CN204247166 U CN 204247166U CN 201420703764 U CN201420703764 U CN 201420703764U CN 204247166 U CN204247166 U CN 204247166U
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- tank body
- seal cover
- temperature
- reacting tank
- heating type
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Abstract
The utility model relates to a kind of internal heating type autoclave, it is characterized in that: the retort comprising reacting tank body and seal cover formation, in retort, put in single head heat-generating pipe by reacting tank body, single head heat-generating pipe is formed by the temperature gradient zone of center to outer arm in retort; Dividing plate is had between temperature gradient zone; The quartz pushrod having extension downward to each temperature gradient zone by seal cover, the quartz pushrod end outside seal cover has and for the optics end face observed, by the reactor reactions change of optics end face temp. indicator gradient zones, and can carry out record by the reactor reaction time; Described reacting tank body is connected by flange seal with seal cover.The utility model, when not increasing equipment, carries out identical conditions reaction under obtaining multiple temperature simultaneously.
Description
Technical field
The utility model relates to a kind of reactor, particularly a kind of internal heating type autoclave.
Background technology
Reactor is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, has been used for the pressure vessel of the technical process such as sulfuration, hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reactor, decomposition pot, polymeric kettle etc.Reactor mode of heating has electrical heating, hot water heating, conduction oil circulating-heating, outer (interior) coil pipe heating etc., and the type of cooling is chuck cooling and the cooling of still inner coil pipe.
Reactor adopts any mode of heating to be all allow the chemical reaction process in reactor complete at the temperature controlled, and generally different temperature, its process of carrying out chemical reaction is distinguishing, and in some situations, difference is sizable.
Obtain reaction information at different temperature at one time, can only be completed by multiple reactor, this can increase cost, and the change of simultaneous reactions condition can affect chemical reaction process.
When carrying out chemical reaction in reactor, due to the impact by structure, internal chemical course of reaction cannot obtain sensorial perception, when particularly utilizing reactor to carry out education experiment or other scientific experiment, sensorial perception can not only improve teaching interest, can also cultivate and improve the quality of teaching.
Utility model content
The purpose of this utility model is to provide a kind of when not increasing equipment, carries out a kind of internal heating type autoclave of identical conditions reaction under obtaining multiple temperature simultaneously.
The purpose of this utility model realizes like this, a kind of internal heating type autoclave, it is characterized in that: the retort comprising reacting tank body and seal cover formation, in retort, put in single head heat-generating pipe by reacting tank body, single head heat-generating pipe is formed by the temperature gradient zone of center to outer arm in retort; Dividing plate is had between temperature gradient zone; The quartz pushrod having extension downward to each temperature gradient zone by seal cover, the quartz pushrod end outside seal cover has and for the optics end face observed, by the reactor reactions change of optics end face temp. indicator gradient zones, and can carry out record by the reactor reaction time; Described reacting tank body is connected by flange seal with seal cover.
To be had to each temperature gradient zone by seal cover and extend downward stirring and pitch, the stirring fork outside seal cover has drive motors, can the reaction mass of whipping temp gradient zones by drive motors.
To be had to the cavity of reacting tank body by seal cover and extend downward thermocouple, thermocouple connects temperature and pressure device for digit-displaying, by the temperature in temperature and pressure device for digit-displaying display reacting tank body.
To be had to the cavity of reacting tank body by seal cover and extend downward pressure sensor, pressure sensor connects temperature and pressure device for digit-displaying, by the pressure in temperature and pressure device for digit-displaying display reacting tank body.
Described optics end face has an image unit, is observed the reactor reactions change of temperature gradient zone by image unit.
Described reacting tank body is made up of interior outer tank body, and outer tank adopts stainless steel, and interior tank body is quartzy tank body.
Described single head heat-generating pipe diameter is between 12mm-15mm.
The utility model has the advantages that:
(1) the interior heating of realization response still, formation temperature gradient in reactor; Reactant is made only in the region limited, to synthesize required material;
Require:
(1) pressure of 10MPa can be born;
(2) heating-up temperature of heat-generating pipe can reach 800 DEG C, and the most high energy of the temperature in reactor reaches 300 DEG C;
(3) pressure in reactor can be demonstrated;
(4) temperature of three zoness of different (in heating tube wall, reactor inwall, reactor liquid) in reactor can be measured;
(5) volume of reaction chamber can reach 200ml(80mm140mm);
(6) the efficient heat generation length of heat-generating pipe is no more than 80mm, avoids dry combustion method;
(7) temperature control can be realized.
Accompanying drawing explanation
Below in conjunction with embodiment accompanying drawing the utility model answered and further illustrates:
Fig. 1 is the utility model example structure schematic diagram.
In figure, 1, reacting tank body; 2, seal cover; 3, single head heat-generating pipe; 4, temperature gradient zone; 5, dividing plate; 6, fork is stirred; 7, quartz pushrod; 8, image unit; 9, thermocouple; 10, pressure sensor; 11, temperature and pressure device for digit-displaying; 12; Optics end face; 13, drive motors; 14, outer tank; 15, interior tank body.
Detailed description of the invention
Embodiment 1
As shown in Figure 1, a kind of internal heating type autoclave, comprise the retort of reacting tank body 1 and seal cover 2 formation, in retort, put in single head heat-generating pipe 3 by seal cover 2, single head heat-generating pipe 3 diameter is between 12mm-15mm; Single head heat-generating pipe 3 is formed by the temperature gradient zone 4 of center to outer arm in retort; Dividing plate 5 is had between temperature gradient zone 4; The quartz pushrod 7 having extension downward to each temperature gradient zone 4 by seal cover 2, quartz pushrod 7 end outside seal cover 2 has can for the optics end face 12 observed, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor reaction time.Described reacting tank body 1 is connected by flange seal with seal cover 2.
Embodiment 2
As shown in Figure 1, a kind of internal heating type autoclave, comprise the retort of reacting tank body 1 and seal cover 2 formation, in retort, put in single head heat-generating pipe 3 by seal cover 2, single head heat-generating pipe 3 diameter is between 12mm-15mm; Single head heat-generating pipe 3 is formed by the temperature gradient zone 4 of center to outer arm in retort; Dividing plate 5 is had between temperature gradient zone 4; The quartz pushrod 7 having extension downward to each temperature gradient zone 4 by seal cover 2, quartz pushrod 7 end outside seal cover 2 has can for the optics end face 12 observed, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor reaction time; To be had to each temperature gradient zone 4 by seal cover 2 and extend downward stirring and pitch 6, the stirring fork 6 outside seal cover 2 has drive motors 13, can the reaction mass of whipping temp gradient zones by drive motors 13.
Embodiment 3
As shown in Figure 1, a kind of internal heating type autoclave, comprise the retort of reacting tank body 1 and seal cover 2 formation, in retort, put in single head heat-generating pipe 3 by seal cover 2, single head heat-generating pipe 3 diameter is between 12mm-15mm; Single head heat-generating pipe 3 is formed by the temperature gradient zone 4 of center to outer arm in retort; Dividing plate 5 is had between temperature gradient zone 4; The quartz pushrod 7 having extension downward to each temperature gradient zone 4 by seal cover 2, quartz pushrod 7 end outside seal cover 2 has can for the optics end face 12 observed, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor reaction time; To be had to each temperature gradient zone 4 by seal cover 2 and extend downward stirring and pitch 6, the stirring fork 6 outside seal cover 2 has drive motors 13, can the reaction mass of whipping temp gradient zones by drive motors 13; To be had to the cavity of reacting tank body 1 by seal cover 2 and extend downward thermocouple 9, thermocouple 9 connects temperature and pressure device for digit-displaying 11, shows the temperature in reacting tank body 1 by temperature and pressure device for digit-displaying 11; To be had to the cavity of reacting tank body 1 by seal cover 2 and extend downward pressure sensor 10, pressure sensor 10 connects temperature and pressure device for digit-displaying 11, shows the pressure in reacting tank body 1 by temperature and pressure device for digit-displaying 11.
Embodiment 4
As shown in Figure 1, a kind of internal heating type autoclave, comprise the retort of reacting tank body 1 and seal cover 2 formation, in retort, put in single head heat-generating pipe 3 by seal cover 2, single head heat-generating pipe 3 diameter is between 12mm-15mm; Single head heat-generating pipe 3 is formed by the temperature gradient zone 4 of center to outer arm in retort; Dividing plate 5 is had between temperature gradient zone 4; The quartz pushrod 7 having extension downward to each temperature gradient zone 4 by seal cover 2, quartz pushrod 7 end outside seal cover 2 has can for the optics end face 12 observed, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor reaction time.Described optics end face 12 has an image unit 8, is observed the reactor reactions change of temperature gradient zone by image unit 8.Image unit adopts known technology.
Described reacting tank body 1 is made up of interior outer tank body, and outer tank 14 adopts stainless steel, and interior tank body 15 is quartzy tank body.
Claims (7)
1. an internal heating type autoclave, it is characterized in that: comprise the retort that reacting tank body (1) and seal cover (2) are formed, in retort, put in single head heat-generating pipe (3) by reacting tank body (1), single head heat-generating pipe (3) is formed by the temperature gradient zone (4) of center to outer arm in retort; Dividing plate (5) is had between temperature gradient zone (4); The quartz pushrod (7) having extension downward to each temperature gradient zone (4) by seal cover (2), seal cover (2) quartz pushrod outward (7) end has can for the optics end face (12) observed, by the reactor reactions change of optics end face (12) temp. indicator gradient zones, and carry out record by the reactor reaction time; Described reacting tank body (1) is connected by flange seal with seal cover (2).
2. a kind of internal heating type autoclave according to claim 1, it is characterized in that: (6) are pitched in the stirring having extension downward to each temperature gradient zone (4) by seal cover (2), seal cover (2) stirring fork (6) outward has drive motors (13), can the reaction mass of whipping temp gradient zones by drive motors (13).
3. a kind of internal heating type autoclave according to claim 1, it is characterized in that: to be had to the cavity of reacting tank body (1) by seal cover (2) and extend downward thermocouple (9), thermocouple (9) connects temperature and pressure device for digit-displaying (11), by the temperature in temperature and pressure device for digit-displaying (11) display reacting tank body (1).
4. a kind of internal heating type autoclave according to claim 1, it is characterized in that: to be had to the cavity of reacting tank body (1) by seal cover (2) and extend downward pressure sensor (10), pressure sensor (10) connects temperature and pressure device for digit-displaying (11), by the pressure in temperature and pressure device for digit-displaying (11) display reacting tank body (1).
5. a kind of internal heating type autoclave according to claim 1, is characterized in that: described optics end face (12) has an image unit (8), is observed the reactor reactions change of temperature gradient zone by image unit (8).
6. a kind of internal heating type autoclave according to claim 1, is characterized in that: described reacting tank body (1) is made up of interior outer tank body, and outer tank (14) adopts stainless steel, and interior tank body (15) is quartzy tank body.
7. a kind of internal heating type autoclave according to claim 1, is characterized in that: described single head heat-generating pipe (3) diameter is between 12mm-15mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420703764.2U CN204247166U (en) | 2014-11-21 | 2014-11-21 | A kind of internal heating type autoclave |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420703764.2U CN204247166U (en) | 2014-11-21 | 2014-11-21 | A kind of internal heating type autoclave |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204247166U true CN204247166U (en) | 2015-04-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420703764.2U Expired - Fee Related CN204247166U (en) | 2014-11-21 | 2014-11-21 | A kind of internal heating type autoclave |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204247166U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104525047A (en) * | 2014-11-21 | 2015-04-22 | 程维强 | Internal-heating high-pressure reaction kettle |
-
2014
- 2014-11-21 CN CN201420703764.2U patent/CN204247166U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104525047A (en) * | 2014-11-21 | 2015-04-22 | 程维强 | Internal-heating high-pressure reaction kettle |
| CN104525047B (en) * | 2014-11-21 | 2016-10-19 | 程维强 | A kind of internal heating type autoclave |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150408 Termination date: 20161121 |
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| CF01 | Termination of patent right due to non-payment of annual fee |