CN104525047B - A kind of internal heating type autoclave - Google Patents
A kind of internal heating type autoclave Download PDFInfo
- Publication number
- CN104525047B CN104525047B CN201410671282.8A CN201410671282A CN104525047B CN 104525047 B CN104525047 B CN 104525047B CN 201410671282 A CN201410671282 A CN 201410671282A CN 104525047 B CN104525047 B CN 104525047B
- Authority
- CN
- China
- Prior art keywords
- tank body
- temperature
- temperature gradient
- retort
- sealing lid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
Abstract
The present invention relates to a kind of internal heating type autoclave, it is characterized in that: include reacting tank body and seal the retort that lid is constituted, having been put in single head heat-generating pipe in retort by reacting tank body, single head heat-generating pipe is formed by center to the temperature gradient zone of outer arm in retort；Dividing plate is had between temperature gradient zone；Being had the quartz pushrod under extending to each temperature gradient zone by sealing lid, sealing the quartz pushrod end outside lid has the optics end face being available for observing, and by the reactor reactions change of optics end face temp. indicator gradient zones, and carries out record by the reactor response time；Described reacting tank body is connected by flange seal with sealing lid.The present invention, in the case of not increase equipment, can obtain simultaneously carry out identical conditions reaction at multiple temperature.
Description
Technical field
The present invention relates to a kind of reactor, particularly a kind of internal heating type autoclave.
Background technology
Reactor is widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine, food, be used for sulfuration, hydrogenation,
Hydrocarbonylation, be polymerized, the pressure vessel of the technical process such as condensation, such as reactor, reactor, decomposition pot, polymeric kettle etc..Reactor adds
Hot mode has electrical heating, hot water heating, conduction oil circulating-heating, outer (interior) coil pipe heating etc., the type of cooling be chuck cooling and
Still inner coil pipe cools down.
Reactor uses any mode of heating to be all to allow the chemical reaction process in reactor at a temperature of controlling
Completing, the most different temperature, its process carrying out chemical reaction is distinguishing, and in the case of having, difference is suitable
Big.
Obtaining reaction information at different temperature in the same time, can only be completed by multiple reactors, this can increase
Cost, the change of simultaneous reactions condition can affect chemical reaction process.
When carrying out chemical reaction in reactor, owing to being affected by structure, internal chemical course of reaction cannot be felt
Perception is subject to, and when carrying out education experiment or other scientific experiments in particular with reactor, it is emerging that sensorial perception can not only improve teaching
Interest, moreover it is possible to cultivate and improve the quality of teaching.
Summary of the invention
It is an object of the invention to provide a kind of in the case of not increase equipment, can obtain simultaneously carry out at multiple temperature together
A kind of internal heating type autoclave of one conditioned response.
The object of the present invention is achieved like this, a kind of internal heating type autoclave, it is characterized in that: include reacting tank body
Covering, with sealing, the retort constituted, reacting tank body put in single head heat-generating pipe in retort, single head heat-generating pipe is in retort
Interior formation by center to the temperature gradient zone of outer arm；Dividing plate is had between temperature gradient zone；By sealing lid to each temperature gradient zone
Having the quartz pushrod under extending to, sealing the quartz pushrod end outside lid has the optics end face being available for observing, by optics end face observable
The reactor reactions change of temperature gradient zone, and carry out record by the reactor response time；Described reacting tank body covers with sealing
Connected by flange seal.
Being had the stirring under extending to pitch by sealing lid to each temperature gradient zone, sealing the fork of the stirring outside lid has driving electricity
Machine, by driving the motor can the reaction mass of whipping temp gradient zones.
Being had the thermocouple under extending to by sealing lid to the cavity of reacting tank body, thermocouple connects temperature and pressure digital display
Device, by the temperature in temperature and pressure device for digit-displaying display reacting tank body.
Being had the pressure transducer under extending to by sealing lid to the cavity of reacting tank body, pressure transducer connects temperature and pressure
Power device for digit-displaying, by the pressure in temperature and pressure device for digit-displaying display reacting tank body.
Described optics end face has an image unit, and the reactor reaction being observed temperature gradient zone by image unit is become
Change.
Described reacting tank body is made up of interior outer tank body, and outer tank uses rustless steel, and interior tank body is quartz tank body.
Described single head heat-generating pipe diameter is between 12mm-15mm.
The invention have the advantage that
(1) realize the interior heating of reactor, in reactor, form thermograde；Make reactant only in the region limited
Material needed for interior synthesis；
Require:
(1) pressure of 10MPa can be born；
(2) heating-up temperature of heat-generating pipe can reach 800 DEG C, and the temperature in reactor can reach 300 DEG C；
(3) can show that the pressure in reactor；
(4) three zoness of different (liquid in heating tube wall, reactor inwall, reactor) in reactor can be measured
Temperature；
(5) volume of reaction chamber can reach 200ml(80mm140mm)；
(6) the efficient heat generation length of heat-generating pipe is less than 80mm, it is to avoid dry combustion method；
(7) it is capable of temperature control.
Accompanying drawing explanation
Below in conjunction with embodiment accompanying drawing the present invention answered and further illustrates:
Fig. 1 is embodiment of the present invention structural representation.
In figure, 1, reacting tank body；2, lid is sealed；3, single head heat-generating pipe；4, temperature gradient zone；5, dividing plate；6, stirring fork；7、
Quartz pushrod；8, image unit；9, thermocouple；10, pressure transducer；11, temperature and pressure device for digit-displaying；12；Optics end face；13、
Drive motor；14, outer tank；15, interior tank body.
Detailed description of the invention
Embodiment 1
As it is shown in figure 1, a kind of internal heating type autoclave, including reacting tank body 1 and the retort of sealing lid 2 composition,
Having been put in single head heat-generating pipe 3 in retort by sealing lid 2, single head heat-generating pipe 3 diameter is between 12mm-15mm；Single head generates heat
Pipe 3 is formed by center to the temperature gradient zone 4 of outer arm in retort；Dividing plate 5 is had between temperature gradient zone 4；By seal lid 2 to
There is the quartz pushrod 7 under extending to each temperature gradient zone 4, and sealing quartz pushrod 7 end outside lid 2 has the optics end face being available for observing
12, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor response time.
Described reacting tank body 1 is connected by flange seal with sealing lid 2.
Embodiment 2
As it is shown in figure 1, a kind of internal heating type autoclave, including reacting tank body 1 and the retort of sealing lid 2 composition,
Having been put in single head heat-generating pipe 3 in retort by sealing lid 2, single head heat-generating pipe 3 diameter is between 12mm-15mm；Single head generates heat
Pipe 3 is formed by center to the temperature gradient zone 4 of outer arm in retort；Dividing plate 5 is had between temperature gradient zone 4；By seal lid 2 to
There is the quartz pushrod 7 under extending to each temperature gradient zone 4, and sealing quartz pushrod 7 end outside lid 2 has the optics end face being available for observing
12, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor response time；
Being had the stirring fork 6 under extending to by sealing lid 2 to each temperature gradient zone 4, sealing the fork of the stirring outside lid 26 has driving motor 13,
By driving the motor 13 can the reaction mass of whipping temp gradient zones.
Embodiment 3
As it is shown in figure 1, a kind of internal heating type autoclave, including reacting tank body 1 and the retort of sealing lid 2 composition,
Having been put in single head heat-generating pipe 3 in retort by sealing lid 2, single head heat-generating pipe 3 diameter is between 12mm-15mm；Single head generates heat
Pipe 3 is formed by center to the temperature gradient zone 4 of outer arm in retort；Dividing plate 5 is had between temperature gradient zone 4；By seal lid 2 to
There is the quartz pushrod 7 under extending to each temperature gradient zone 4, and sealing quartz pushrod 7 end outside lid 2 has the optics end face being available for observing
12, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor response time；
Being had the stirring fork 6 under extending to by sealing lid 2 to each temperature gradient zone 4, sealing the fork of the stirring outside lid 26 has driving motor 13,
By driving the motor 13 can the reaction mass of whipping temp gradient zones；Extended to down to the cavity of reacting tank body 1 by sealing lid 2
Thermocouple 9, thermocouple 9 connects temperature and pressure device for digit-displaying 11, in showing reacting tank body 1 by temperature and pressure device for digit-displaying 11
Temperature；Being had the pressure transducer 10 under extending to by sealing lid 2 to the cavity of reacting tank body 1, pressure transducer 10 connects temperature
Degree and pressure device for digit-displaying 11, show the pressure in reacting tank body 1 by temperature and pressure device for digit-displaying 11.
Embodiment 4
As it is shown in figure 1, a kind of internal heating type autoclave, including reacting tank body 1 and the retort of sealing lid 2 composition,
Having been put in single head heat-generating pipe 3 in retort by sealing lid 2, single head heat-generating pipe 3 diameter is between 12mm-15mm；Single head generates heat
Pipe 3 is formed by center to the temperature gradient zone 4 of outer arm in retort；Dividing plate 5 is had between temperature gradient zone 4；By seal lid 2 to
There is the quartz pushrod 7 under extending to each temperature gradient zone 4, and sealing quartz pushrod 7 end outside lid 2 has the optics end face being available for observing
12, by the reactor reactions change of optics end face 12 temp. indicator gradient zones, and carry out record by the reactor response time.
Described optics end face 12 has an image unit 8, is observed the reactor reactions change of temperature gradient zone by image unit 8.Take the photograph
As unit uses known technology.
Described reacting tank body 1 is made up of interior outer tank body, and outer tank 14 uses rustless steel, interior tank body 15 to be quartz tank body.
Claims (5)
1. an internal heating type autoclave, is characterized in that: includes reacting tank body (1) and seals the retort that lid (2) is constituted,
Having been put in single head heat-generating pipe (3) in retort by reacting tank body (1), single head heat-generating pipe (3) is formed by center in retort
To the temperature gradient zone (4) of outer arm；Dividing plate (5) is had between temperature gradient zone (4)；By sealing lid (2) to each temperature gradient zone
(4) having the quartz pushrod (7) under extending to, sealing lid (2) quartz pushrod (7) end outward has the optics end face (12) being available for observing, logical
Cross the reactor reactions change of optics end face (12) temp. indicator gradient zones, and carry out record by the reactor response time；Institute
The reacting tank body (1) stated is connected by flange seal with sealing lid (2)；Had to each temperature gradient zone (4) to prolong by sealing lid (2)
Stirring fork (6) under stretching to, sealing lid (2) stirring fork (6) outward has driving motor (13), by driving motor (13) to stir
The reaction mass of temperature gradient zone；The thermocouple (9) under extending to, thermoelectricity is had to the cavity of reacting tank body (1) by sealing lid (2)
Even (9) connect temperature and pressure device for digit-displaying (11), by the temperature in temperature and pressure device for digit-displaying (11) display reacting tank body (1)
Degree.
2. according to a kind of internal heating type autoclave described in claim 1, it is characterized in that: by sealing lid (2) to retort
The cavity of body (1) has the pressure transducer (10) under extending to, and pressure transducer (10) connects temperature and pressure device for digit-displaying (11),
By the pressure in temperature and pressure device for digit-displaying (11) display reacting tank body (1).
3. according to a kind of internal heating type autoclave described in claim 1, it is characterized in that: described optics end face (12)
There is an image unit (8), observed the reactor reactions change of temperature gradient zone by image unit (8).
4., according to a kind of internal heating type autoclave described in claim 1, it is characterized in that: described reacting tank body (1) by
Interior outer tank body forms, and outer tank (14) uses rustless steel, and interior tank body (15) is quartz tank body.
5. according to a kind of internal heating type autoclave described in claim 1, it is characterized in that: described single head heat-generating pipe (3)
Diameter is between 12mm-15mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410671282.8A CN104525047B (en) | 2014-11-21 | 2014-11-21 | A kind of internal heating type autoclave |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410671282.8A CN104525047B (en) | 2014-11-21 | 2014-11-21 | A kind of internal heating type autoclave |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104525047A CN104525047A (en) | 2015-04-22 |
| CN104525047B true CN104525047B (en) | 2016-10-19 |
Family
ID=52840780
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410671282.8A Expired - Fee Related CN104525047B (en) | 2014-11-21 | 2014-11-21 | A kind of internal heating type autoclave |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104525047B (en) |
Citations (9)
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| CN101760772A (en) * | 2009-12-30 | 2010-06-30 | 苏州纳维科技有限公司 | Reaction unit for ammonia thermal growth of nitride |
| CN202263571U (en) * | 2011-10-18 | 2012-06-06 | 程维强 | Miniature high-pressure reaction kettle |
| CN102698697A (en) * | 2012-06-25 | 2012-10-03 | 江门市长优实业有限公司 | Reaction kettle device for preparing and coating spherical nickel hydroxide |
| CN202762442U (en) * | 2012-09-26 | 2013-03-06 | 重庆德蒙特科技发展有限公司 | Double-cylinder chemical reaction kettle |
| CN103055594A (en) * | 2012-12-27 | 2013-04-24 | 亚洲铝业（中国）有限公司 | Processing method for cold rolling water-based coolant |
| JP2013202601A (en) * | 2012-03-29 | 2013-10-07 | Osaka Gas Co Ltd | Method and device for treating organic waste water |
| CN103406070A (en) * | 2013-08-26 | 2013-11-27 | 中国科学院地球化学研究所 | Multifunctional high-temperature and high-pressure reaction kettle |
| CN203303912U (en) * | 2013-06-21 | 2013-11-27 | 程维强 | Visible optical micro high-pressure reaction kettle |
| CN204247166U (en) * | 2014-11-21 | 2015-04-08 | 程维强 | A kind of internal heating type autoclave |
-
2014
- 2014-11-21 CN CN201410671282.8A patent/CN104525047B/en not_active Expired - Fee Related
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101760772A (en) * | 2009-12-30 | 2010-06-30 | 苏州纳维科技有限公司 | Reaction unit for ammonia thermal growth of nitride |
| CN202263571U (en) * | 2011-10-18 | 2012-06-06 | 程维强 | Miniature high-pressure reaction kettle |
| JP2013202601A (en) * | 2012-03-29 | 2013-10-07 | Osaka Gas Co Ltd | Method and device for treating organic waste water |
| CN102698697A (en) * | 2012-06-25 | 2012-10-03 | 江门市长优实业有限公司 | Reaction kettle device for preparing and coating spherical nickel hydroxide |
| CN202762442U (en) * | 2012-09-26 | 2013-03-06 | 重庆德蒙特科技发展有限公司 | Double-cylinder chemical reaction kettle |
| CN103055594A (en) * | 2012-12-27 | 2013-04-24 | 亚洲铝业（中国）有限公司 | Processing method for cold rolling water-based coolant |
| CN203303912U (en) * | 2013-06-21 | 2013-11-27 | 程维强 | Visible optical micro high-pressure reaction kettle |
| CN103406070A (en) * | 2013-08-26 | 2013-11-27 | 中国科学院地球化学研究所 | Multifunctional high-temperature and high-pressure reaction kettle |
| CN204247166U (en) * | 2014-11-21 | 2015-04-08 | 程维强 | A kind of internal heating type autoclave |
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| Publication number | Publication date |
|---|---|
| CN104525047A (en) | 2015-04-22 |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161019 Termination date: 20171121 |
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| CF01 | Termination of patent right due to non-payment of annual fee |