CN205656154U - Experimental device for chemical themogenesis of survey under high temperature high pressure condition - Google Patents
Experimental device for chemical themogenesis of survey under high temperature high pressure condition Download PDFInfo
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- CN205656154U CN205656154U CN201520741274.6U CN201520741274U CN205656154U CN 205656154 U CN205656154 U CN 205656154U CN 201520741274 U CN201520741274 U CN 201520741274U CN 205656154 U CN205656154 U CN 205656154U
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- kettle
- temperature
- support shaft
- heat generating
- experimental provision
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Abstract
The utility model provides an experimental device for chemical themogenesis of survey under high temperature high pressure condition belongs to chemical field. Form by primary shaft bearing, flange, kettle cover, sealing washer, sealed lid, connective bar, bush, the cauldron body, reaction cylinder, cauldron body back shaft, secondary shaft bearing, handle, handle seat, support, underframe, rubber pad, bottom export, suction nozzle, dustcoat, heating plate, pressure cap, blind pipe and play air cock. Wherein, kettle cover and the cauldron body make by ha shi alloy material, connective bar, bush, reaction cylinder and dustcoat make for the polytetrafluoroethylene material. This experimental apparatus has advantages such as the principle is simple, convenient operation, and can mix and emergence reaction production of heat by two kinds of medicaments of precision measurement, accurately record reaction law.
Description
Technical field
This utility model belongs to chemical field, relates to a kind of experimental provision, particularly a kind of
The experimental provision of chemical heat generating is measured under high-temperature and high-pressure conditions.
Background technology
Chemical heat generating refers to the exothermic reaction choosing in chemical reaction, utilizes it to produce
Heat improves the character of stratum and fluid, thus reaches to improve the purpose of recovery ratio.
Chemical heat generating technology is widely used in oil field, including wax removal and de-plugging,
Self-heating pressure breaks etc., in terms of research chemical heat generating reaction influence factor, need life
Pressure and temperature in thermal process are monitored, record, need to set primary response temperature
Heat loss in degree and reduction course of reaction, in addition it is also necessary to ensure the mixing efficiency of medicament,
And in existing experimental provision, be not the most suitable under high-temperature and high-pressure conditions measuring chemistry
The experimental provision of heat.
Thus, a kind of experimental provision is proposed, to overcome the defect of prior art.
Utility model content
The purpose of this utility model is to there are the problems referred to above for existing technology, it is proposed that
The experiment of chemical heat generating is measured under the high-temperature and high-pressure conditions that a kind of principle is simple and convenient to operate
Device.
The purpose of this utility model can be realized by following technical proposal: a kind of high temperature is high
Measure the experimental provision of chemical heat generating under the conditions of pressure, by clutch shaft bearing seat, flange, kettle cover,
Sealing ring, seal lid, pitman, lining, kettle, reaction tube, kettle support shaft,
Second bearing block, handle, handle set, support, underframe, rubber blanket, outlet at bottom,
Suction nozzle, outer housing, heating plate, pressure cap, blind pipe and outlet nozzle composition.Wherein, institute
Kettle cover and the kettle stated are made up of Hastelloy material；Described pitman, lining,
Reaction tube and outer housing are that polytetrafluoroethylmaterial material is made.
Kettle is barrel-shaped structure, and the top of kettle is provided with flange, kettle cover and sealing lid,
And the junction of kettle cover and kettle is provided with sealing ring；The top of kettle cover is provided with flange, and
Flange is connected with kettle by bolt, and the bottom of kettle cover is provided with sealing lid, and seals lid
For T-type structure, seal lid and be arranged on the top of kettle by its T-type structure edge, and
Sealing the top of lid and the bottom compact siro spinning technology of kettle cover, the bottom sealing lid is the interior of kettle
Portion.
Kettle cover is provided with three through holes, and wherein, first through hole is provided with suction nozzle, the
Two through holes are provided with outlet nozzle, and the 3rd through hole is provided with blind pipe, and blind pipe is by pressure
Cap is arranged on the 3rd through hole.
Seal and cover three through holes being provided with joined together by above-mentioned kettle cover, suction nozzle and going out
Valve is passed into the inside of kettle, and blind pipe is inserted into the inside of kettle.
Meanwhile, the annulus centre position at kettle cover and sealing lid is provided with for connecting pitman
Screw, pitman is provided with screw thread, the top of pitman and kettle cover and close closure threads
Connecting, the bottom of pitman is connected with the bottom thread of reaction tube.
Sealing ring is O RunddichtringO, and the size of sealing ring and kettle cover, the size of kettle
Match.
The inside of kettle is provided with lining, and lining is fitted tightly on inner wall of kettle, is formed
Clad；Being provided with reaction tube in the inside of lining, reaction tube is by through its inside
Pitman is arranged on the inside of kettle, and after kettle cover is arranged on kettle, reaction tube hangs
Hang over inside kettle.
The external diameter of reaction tube is less than the internal diameter of lining, i.e. reaction tube and reserved between lining
Certain space, blind pipe can carry temperature probe and be inserted into the inside of kettle, by temperature
Degree probe can measure the temperature in reactor.
The bottom of kettle is provided with outlet at bottom, and outlet at bottom runs through the bottom of kettle and lining,
Being passed into the inside of kettle, described outlet at bottom is connected with pressure transducer, by pressure
Force transducer can measure the pressure in reactor.
Underframe is rectangle structure, is respectively equipped with the first axle on two corresponding frames of underframe
Bearing and the second bearing block；The shape of clutch shaft bearing seat and the second bearing block is identical, and all
For triangular structure.
The bottom of underframe is provided with four rubber blankets, and four rubber blankets are separately positioned on underframe
Four drift angles at.
The outside of kettle is provided with heating plate, and the outside of heating plate is provided with outer housing, and outer housing is tight
Closely connected being combined on heating plate outer wall, form clad, kettle can be added by heating plate
Heat, and reach initial reaction temperature, outer housing can reduce thermal loss.
The outside of kettle is provided with kettle support shaft, and kettle support shaft is made up of two parts, the
One end of one kettle support shaft is fixing with kettle to be connected, and the other end is arranged on clutch shaft bearing seat
On；One end of second kettle support shaft is fixing with kettle to be connected, and the other end is arranged on second
On bearing block, and the second kettle support shaft runs through the second bearing block, supports at the second kettle
The afterbody of the through part of axle is provided with handle set, and is provided with handle on handle set.
Above-mentioned the first kettle support shaft, kettle and the second kettle support shaft are coaxially connected,
By turning handle handle, it is possible to drive kettle to rotate.
Compared with prior art, this experimental provision has the advantage that
1, this experimental provision principle is simple and convenient to operate.
2, this experimental provision can accurately be measured two kinds of medicaments and carries out the raw reaction of hybrid concurrency and produce
Heat amount, in course of reaction, drives the inversion of kettle by handle and rocks, reaching
Well mixed effect, it is ensured that measurement result accurate.
3, this experimental provision can record reaction rule, such as exactly: putting of chemical reaction
Heat Calculation, chemical reaction rate and time relationship, chemical reaction pressure change and time
Between relation etc..
Accompanying drawing explanation
Fig. 1 is overall structure schematic diagram of the present utility model；
Fig. 2 is cross-sectional view of the present utility model.
In figure, 1, clutch shaft bearing seat；2, flange；3, kettle cover；4, sealing ring；5、
Seal lid；6, pitman；7, lining；8, kettle；9, reaction tube；10, kettle
Support shaft；11, the second bearing block；12, handle；13, handle set；14, support；
15, underframe；16, rubber blanket；17, outlet at bottom；18, suction nozzle；19, outer housing；
20, heating plate；21, pressure cap；22, blind pipe；23, outlet nozzle.
Detailed description of the invention
The following is specific embodiment of the utility model and combine accompanying drawing, to this utility model
Technical scheme be further described, but this utility model is not limited to these embodiments.
As depicted in figs. 1 and 2, the reality of chemical heat generating is measured under a kind of high-temperature and high-pressure conditions
Experiment device, by clutch shaft bearing seat 1, flange 2, kettle cover 3, sealing ring 4, seal lid 5,
Pitman 6, lining 7, kettle 8, reaction tube 9, kettle support shaft the 10, second bearing
Seat 11, handle 12, handle set 13, support 14, underframe 15, rubber blanket 16, bottom
Outlet 17, suction nozzle 18, outer housing 19, heating plate 20, pressure cap 21, blind pipe 22 and
Outlet nozzle 23 forms.Wherein, described kettle cover 3 and kettle 8 are by Hastelloy material
Make；Described pitman 6, lining 7, reaction tube 9 and outer housing 19 are polytetrafluoroethyl-ne
Alkene material is made.
As it is shown in figure 1, kettle 8 is barrel-shaped structure, the top of kettle 8 is provided with method
Blue 2, kettle cover 3 and seal lid 5, and the junction of kettle cover 3 and kettle 8 is provided with sealing ring
4；The top of kettle cover 3 is provided with flange 2, and flange 2 is connected with kettle 8 by bolt,
The bottom of kettle cover 3 is provided with sealing lid 5, and sealing lid 5 is T-type structure, seals lid 5
Be arranged on the top of kettle 8 by its T-type structure edge, and seal the top of lid 5 with
The bottom compact siro spinning technology of kettle cover 3, seals the inside that bottom is kettle 8 of lid 5.
Kettle cover 3 is provided with three through holes, and wherein, first through hole is provided with suction nozzle 18,
Second through hole is provided with outlet nozzle 23, and the 3rd through hole is provided with blind pipe 22, and blind pipe
22 are arranged on the 3rd through hole by pressure cap 21.
Seal and be provided with and three through holes joined together by above-mentioned kettle cover 3 on lid 5, and such as figure
Shown in 1 and Fig. 2, suction nozzle 18 and outlet nozzle 23 are passed into the inside of kettle 8, blind
Pipe 22 is inserted into the inside of kettle 8.
Meanwhile, the annulus centre position at kettle cover 3 and sealing lid 5 is provided with for connecting
Take over the baton 6 screw, pitman 6 is provided with screw thread, the top of pitman 6 and kettle cover 3
Lid 5 is threaded with sealing, and the bottom of pitman 6 connects with the bottom thread of reaction tube 9
Connect.
Sealing ring 4 is O RunddichtringO, and the size of sealing ring 4 and kettle cover 3, kettle 8
Size match.
As depicted in figs. 1 and 2, the inside of kettle 8 is provided with lining 7, and lining 7 is tight
Closely connected it is combined on kettle 8 inwall, forms clad；It is provided with reaction in the inside of lining 7
Cylinder 9, reaction tube 9 is arranged in kettle 8 by the pitman 6 internal through it
Portion, and after kettle cover 3 is arranged on kettle 8, it is internal that reaction tube 9 is suspended on kettle 8.
The external diameter of reaction tube 9 less than the internal diameter of lining 7, i.e. reaction tube 9 with lining 7
Between reserved certain space, insert as in figure 2 it is shown, blind pipe 22 can carry temperature probe
Enter the inside to kettle 8, the temperature in reactor can be measured by temperature probe.
The bottom of kettle 8 is provided with outlet at bottom 17, and outlet at bottom 17 runs through kettle 8 He
The bottom of lining 7, is passed into the inside of kettle 8, described outlet at bottom 17 and pressure
Sensor connects, and can be measured the pressure in reactor by pressure transducer.
Underframe 15 is rectangle structure, is respectively equipped with on 15 two corresponding frames of underframe
Clutch shaft bearing seat 1 and the second bearing block 11；Clutch shaft bearing seat 1 and the second bearing block 11
Shape identical, and be triangular structure.
The bottom of underframe 15 is provided with four rubber blankets 16, and four rubber blankets 16 set respectively
Put at four drift angles of underframe 15.
As in figure 2 it is shown, the outside of kettle 8 is provided with heating plate 20, outside heating plate 20
Portion is provided with outer housing 19, and outer housing 19 is fitted tightly on heating plate 20 outer wall, forms bag
Coating, kettle 8 can be heated, and reach initial reaction temperature by heating plate 20,
Outer housing 19 can reduce thermal loss.
As it is shown in figure 1, the outside of kettle 8 is provided with kettle support shaft 10, kettle support shaft
10 are made up of two parts, and one end of the first kettle support shaft 10 is fixing with kettle 8 to be connected,
The other end is arranged on clutch shaft bearing seat 1；One end of second kettle support shaft 10 and kettle
8 fixing connections, the other end is arranged on the second bearing block 11, and the second kettle support shaft
10 run through the second bearing block 11, at the afterbody of the through part of the second kettle support shaft 10
It is provided with handle set 13, and on handle set 13, is provided with handle 12.
Above-mentioned the first kettle support shaft 10, kettle 8 and the second kettle support shaft 10 are
Coaxially connected, by turning handle handle 12, it is possible to drive kettle 8 rotating.
Specific embodiment described herein is only for example to this utility model spirit
Explanation.This utility model person of ordinary skill in the field can be to described concrete
Embodiment is made various amendment or supplements or use similar mode to substitute, but not
Spirit of the present utility model can be deviateed or surmount model defined in appended claims
Enclose.
Claims (10)
1. under a high-temperature and high-pressure conditions, measure the experimental provision of chemical heat generating, it is characterised in that: it is made up of clutch shaft bearing seat, flange, kettle cover, sealing ring, sealing lid, pitman, lining, kettle, reaction tube, kettle support shaft, the second bearing block, handle, handle set, support, underframe, rubber blanket, outlet at bottom, suction nozzle, outer housing, heating plate, pressure cap, blind pipe and outlet nozzle；Wherein, described kettle cover and kettle are made up of Hastelloy material；Described pitman, lining, reaction tube and outer housing is that polytetrafluoroethylmaterial material is made；
Described kettle is barrel-shaped structure, and the top of kettle is provided with flange, kettle cover and sealing lid；
The inside of described kettle is provided with lining and reaction tube；
The bottom of described kettle is provided with outlet at bottom；
The outside of described kettle is provided with heating plate, outer housing and kettle support shaft.
The experimental provision of chemical heat generating is measured under a kind of high-temperature and high-pressure conditions the most according to claim 1, it is characterized in that, described kettle is barrel-shaped structure, and the top of kettle is provided with flange, kettle cover and sealing lid, and the junction of kettle cover and kettle is provided with sealing ring；The top of kettle cover is provided with flange, and flange is connected with kettle by bolt, the bottom of kettle cover is provided with sealing lid and sealing lid is T-type structure, seal lid and be arranged on the top of kettle by its T-type structure edge, and seal the top of lid and the bottom compact siro spinning technology of kettle cover, seal the inside that bottom is kettle of lid.
The experimental provision of chemical heat generating is measured under a kind of high-temperature and high-pressure conditions the most according to claim 1 and 2, it is characterized in that, described kettle cover is provided with three through holes, wherein, first through hole is provided with suction nozzle, second through hole is provided with outlet nozzle, and the 3rd through hole is provided with blind pipe, and blind pipe is arranged on the 3rd through hole by pressure cap；
Described sealing covers three through holes being provided with joined together by above-mentioned kettle cover, and suction nozzle and outlet nozzle are passed into the inside of kettle, and blind pipe is inserted into the inside of kettle.
The experimental provision of chemical heat generating is measured, it is characterised in that the annulus centre position of described kettle cover and sealing lid is provided with the screw for connecting pitman under a kind of high-temperature and high-pressure conditions the most according to claim 1；
Described pitman is provided with screw thread, and threadeding with kettle cover and sealing lid in the top of pitman, the bottom of pitman is connected with the bottom thread of reaction tube.
Measure the experimental provision of chemical heat generating under a kind of high-temperature and high-pressure conditions the most according to claim 1, it is characterised in that the inside of described kettle is provided with lining, and lining is fitted tightly on inner wall of kettle, form clad；Being provided with reaction tube in the inside of lining, reaction tube is arranged on the inside of kettle by the pitman internal through it, and after kettle cover is arranged on kettle, reaction tube is suspended on inside kettle；
The external diameter of reaction tube is less than the internal diameter of lining, and blind pipe carries temperature probe and is inserted into the inside of kettle.
Measuring the experimental provision of chemical heat generating under a kind of high-temperature and high-pressure conditions the most according to claim 1, it is characterised in that the bottom of described kettle is provided with outlet at bottom, outlet at bottom runs through the bottom of kettle and lining, is passed into the inside of kettle；
Described outlet at bottom is connected with pressure transducer.
Measure the experimental provision of chemical heat generating under a kind of high-temperature and high-pressure conditions the most according to claim 1, it is characterised in that described underframe is rectangle structure, be provided with clutch shaft bearing seat and the second bearing block on the top of underframe；The shape of clutch shaft bearing seat and the second bearing block is identical, and is triangular structure；
The bottom of described underframe is provided with four rubber blankets, and four rubber blankets are separately positioned at four drift angles of underframe.
The experimental provision of chemical heat generating is measured under a kind of high-temperature and high-pressure conditions the most according to claim 1, it is characterized in that, the outside of described kettle is provided with heating plate, the outside of heating plate is provided with outer housing, and outer housing is fitted tightly on heating plate outer wall, forming clad, kettle can be heated by heating plate, and reaching initial reaction temperature, outer housing can reduce thermal loss.
The experimental provision of chemical heat generating is measured under a kind of high-temperature and high-pressure conditions the most according to claim 1, it is characterized in that, the outside of described kettle is provided with kettle support shaft, kettle support shaft is made up of two parts, one end of first kettle support shaft is fixing with kettle to be connected, and the other end is arranged on clutch shaft bearing seat；One end of second kettle support shaft is fixing with kettle to be connected, and the other end is arranged on the second bearing block, and the second kettle support shaft runs through the second bearing block, and the afterbody in the through part of the second kettle support shaft is provided with handle set, and is provided with handle on handle set.
The experimental provision of chemical heat generating is measured, it is characterised in that described the first kettle support shaft, kettle and the second kettle support shaft are coaxially connected under a kind of high-temperature and high-pressure conditions the most according to claim 9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520741274.6U CN205656154U (en) | 2015-09-19 | 2015-09-19 | Experimental device for chemical themogenesis of survey under high temperature high pressure condition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520741274.6U CN205656154U (en) | 2015-09-19 | 2015-09-19 | Experimental device for chemical themogenesis of survey under high temperature high pressure condition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205656154U true CN205656154U (en) | 2016-10-19 |
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ID=57355115
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520741274.6U Expired - Fee Related CN205656154U (en) | 2015-09-19 | 2015-09-19 | Experimental device for chemical themogenesis of survey under high temperature high pressure condition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205656154U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109739285A (en) * | 2019-02-20 | 2019-05-10 | 郑州大学 | A kind of high temperature and pressure foam device of supercritical carbon dioxide |
-
2015
- 2015-09-19 CN CN201520741274.6U patent/CN205656154U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109739285A (en) * | 2019-02-20 | 2019-05-10 | 郑州大学 | A kind of high temperature and pressure foam device of supercritical carbon dioxide |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| DD01 | Delivery of document by public notice |
Addressee: Zhang Xuegang Document name: Notification of Acceptance of Patent Application |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161019 Termination date: 20170919 |