CN204122144U - A kind of multi-functional separatory funnel - Google Patents
A kind of multi-functional separatory funnel Download PDFInfo
- Publication number
- CN204122144U CN204122144U CN201420692957.2U CN201420692957U CN204122144U CN 204122144 U CN204122144 U CN 204122144U CN 201420692957 U CN201420692957 U CN 201420692957U CN 204122144 U CN204122144 U CN 204122144U
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- separatory funnel
- side pipe
- liquid outlet
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of multi-functional separatory funnel.This separatory funnel is provided with inlet and liquid outlet, its separatory funnel sidewall is connected with condenser pipe and side pipe, the upper and lower port of condenser pipe all connects with the inner chamber of separatory funnel, one end of side pipe is connected with separatory funnel is through, the other end stretches out separatory funnel and forms side pipe liquid outlet outward, is provided with the second control valve above side pipe liquid outlet.The utility model not only can realize omnidistance continued operation, can also solve the solvent volatilization problems caused because changeing device, thus reduces the impact on environmental and human health impacts.
Description
technical field:
The utility model relates to a kind of multi-functional separatory funnel.
background technology:
At present, the mode of cohobation is usually adopted to reach the object of recovery of the purifying of liquid organic compound, separation and solvent.Laboratory solvent distillation, first heats stirring and refluxing a few hours after first being mixed with drier by solvent, then changes reflux into distilling apparatus, steamed by solvent.Whole process can not be carried out continuously, and need when reflux and distilling apparatus are changed to remove through condenser pipe, remove reflux, build the steps such as distilling apparatus, not only operate loaded down with trivial details, and the aqueous vapor in air easily reuptaked by solvent, the volatilization of solvent simultaneously can cause environmental pollution impact and health injury.
The utility model of patent CN202438337U discloses a kind of integral type cohobation device, this device has a spherical flask, flask port top is linked in sequence by constant voltage funnel stopcock valve and the liquid storage structure formed with the constant pressure funnel bucket body of constant pressure funnel side pipe collecting cut, liquid storage structure upper end is linked in sequence the spherical condensation tube of tubulose, air exhaust head and spherical rubber bladder, thus constitute overall cohobation device.But the solvent after distillation stores and directly can not discharge reception in separatory funnel, just can only can collect solvent distillation after handle assembly dismounting, operate inconvenience like this, can not carry out continuous print backflow and distillation.
The utility model of patent CN202238101U discloses a kind of oxolane distilling apparatus, comprises there-necked flask, and described there-necked flask Zuo Kou and is with the dropping funel lower end of arm to be connected, and described dropping funel upper end is connected with condenser pipe; Described there-necked flask Zhong Kou is connected with a mechanical agitator; The right mouth of described there-necked flask is connected with glass stopper or rubber stopper.The separatory funnel of this oxolane distilling apparatus is collected the solvent stored and can not directly be discharged, and also can only could discharge solvent after detaching device.
Therefore, necessary the deficiency solving prior art is improved to prior art.
summary of the invention:
The utility model provides a kind of multi-functional separatory funnel to solve above-mentioned prior art Problems existing, the utility model not only can make the backflow of solvent and distill integrated carrying out, and when not provision for disengagement, the solvent after distillation can also be discharged smoothly from separatory funnel, meet the requirement carrying out continuous print backflow and distillation procedure.
The technical scheme that the utility model adopts has:
A kind of multi-functional separatory funnel, this separatory funnel is provided with inlet and liquid outlet, described separatory funnel sidewall is connected with condenser pipe and side pipe, the upper and lower port of condenser pipe all connects with the inner chamber of separatory funnel, one end of side pipe is connected with separatory funnel is through, the other end stretches out separatory funnel and forms side pipe liquid outlet outward, is provided with the second control valve above side pipe liquid outlet.
Further, described separatory funnel is positioned at place above condenser pipe lower port and is provided with the first control valve.
Further, described side pipe liquid outlet is frosted mouth.
Further, the liquid outlet of described separatory funnel is frosted mouth.
Further, described separatory funnel sidewall is provided with scale.
the utility model has following beneficial effect:
The utility model sets up a side pipe on separatory funnel, and distilling effect is good, can not only solve separatory funnel conversion and the problem of the solvent water suction that causes and volatilization, and can reduce the harm to health
accompanying drawing illustrates:
Fig. 1 is the multi-functional separatory funnel structure chart of the utility model.
Wherein
1, separatory funnel; 2, side pipe; 3, the first control valve; 4, the second control valve; 5, liquid outlet; 6, side pipe liquid outlet; 7, inlet; 8, condenser pipe.
detailed description of the invention:
Below in conjunction with accompanying drawing, the utility model is further described.
Please refer to shown in Fig. 1, a kind of multi-functional separatory funnel of the utility model, this separatory funnel 1 is provided with inlet 7 and liquid outlet 5, liquid outlet 5 is frosted mouth, the sidewall of separatory funnel 1 is provided with the scale for reading, separatory funnel 1 sidewall is connected with condenser pipe 8 and side pipe 2, the upper and lower port of condenser pipe 8 all connects with the inner chamber of separatory funnel 1, thus the inner chamber of the inner chamber of condenser pipe 8 and separatory funnel 1 is connected, side pipe 2 is inclined on the sidewall of separatory funnel 1, one end of side pipe 2 is connected with separatory funnel 1 is through, the other end stretches out separatory funnel 1 outer formation side pipe liquid outlet 6, side pipe liquid outlet 6 is frosted mouth, the second control valve 4 is provided with above side pipe liquid outlet 6.The top that the first control valve 3, first control valve 3 is positioned at condenser pipe 8 lower port is provided with above separatory funnel 1 upper liquid outlet 5.
Using method of the present utility model is: be placed in by the utility model on the trial jar of the solvent filling to be separated, purifying, close the second control valve 4 on side pipe 2, open the first control valve 3 on separatory funnel 1, make the utility model form good reflux, reach the object of dry solvent removal of impurities; After solvent reaches the drying effect that dewaters, close the first control valve 3 on separatory funnel 1, form good distilling apparatus, the solvent now distilled out is collected in separatory funnel 1 after condenser pipe 8 condensation; When solvent collection is near expiring, open the second control valve 4 on side pipe 2, just directly can discharge the solvent distillation of storage in separatory funnel 1 from the side pipe liquid outlet 6 on side pipe 2.
The multi-functional separatory funnel of the utility model can replace surname extraction pipe to use, in leaching process, directly discharge extract from the side pipe liquid outlet 6 side pipe 2; Side pipe 2 small angle inclination is arranged on the sidewall of separatory funnel 1, is conducive to the outflow of liquid flux; Scale on separatory funnel 1 can record the volume collecting solvent; Side pipe liquid outlet 6 on side pipe 2 is frosted mouth, can be good at coordinating with receiving flask ground, collection dissolving agent process can be made like this to seal, be not affected by the external environment; The utility model is when not detaching device, and in still-process, discharge the solvent distillation in separatory funnel 1 smoothly, the trouble avoiding repeatedly provision for disengagement to bring, what be conducive to continuous several times carries out cohobation operation.Dry dedoping step and collection dry solvent process can once complete by the utility model in same closed system, thus avoid and change the phenomenon that trouble that device brings and solvent absorb moisture from air, if distillation is hazardous solvent, then can reduce solvent volatilization, thus reduce the impact on environmental and human health impacts.
The above is only this preferred embodiment of the present utility model; should be understood that; for those skilled in the art, can also make some improvement under the prerequisite not departing from the utility model principle, these improvement also should be considered as protection domain of the present utility model.
Claims (5)
1. a multi-functional separatory funnel, this separatory funnel (1) is provided with inlet (7) and liquid outlet (5), it is characterized in that: described separatory funnel (1) sidewall is connected with condenser pipe (8) and side pipe (2), the upper and lower port of condenser pipe (8) all connects with the inner chamber of separatory funnel (1), one end of side pipe (2) is connected with separatory funnel (1) is through, the other end stretches out separatory funnel (1) and forms side pipe liquid outlet (6) outward, and side pipe liquid outlet (6) top is provided with the second control valve (4).
2. multi-functional separatory funnel as claimed in claim 1, is characterized in that: described separatory funnel (1) is gone up and is positioned at place above condenser pipe (8) lower port and is provided with the first control valve (3).
3. multi-functional separatory funnel as claimed in claim 1, is characterized in that: described side pipe liquid outlet (6) is frosted mouth.
4. multi-functional separatory funnel as claimed in claim 1, is characterized in that: the liquid outlet (5) of described separatory funnel (1) is frosted mouth.
5. multi-functional separatory funnel as claimed in claim 1, is characterized in that: described separatory funnel (1) sidewall is provided with scale.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420692957.2U CN204122144U (en) | 2014-11-19 | 2014-11-19 | A kind of multi-functional separatory funnel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420692957.2U CN204122144U (en) | 2014-11-19 | 2014-11-19 | A kind of multi-functional separatory funnel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204122144U true CN204122144U (en) | 2015-01-28 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420692957.2U Expired - Fee Related CN204122144U (en) | 2014-11-19 | 2014-11-19 | A kind of multi-functional separatory funnel |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204122144U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106645596A (en) * | 2017-02-16 | 2017-05-10 | 江苏森淼工程质量检测有限公司 | Device for detecting quality of duct grouting in prestressed component and detection method based on device |
-
2014
- 2014-11-19 CN CN201420692957.2U patent/CN204122144U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106645596A (en) * | 2017-02-16 | 2017-05-10 | 江苏森淼工程质量检测有限公司 | Device for detecting quality of duct grouting in prestressed component and detection method based on device |
| CN106645596B (en) * | 2017-02-16 | 2023-08-22 | 江苏森淼工程质量检测有限公司 | Device for detecting grouting quality of prestressed component pore canal and detection method based on device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150128 Termination date: 20161119 |