CN204017408U

CN204017408U - Vertical efficient distiller

Info

Publication number: CN204017408U
Application number: CN201420472868.7U
Authority: CN
Inventors: 周聪; 赵敏
Original assignee: Analysis & Testing Center Chinese Academy Of Tropical Agricultural Sciences
Current assignee: Analysis & Testing Center Chinese Academy Of Tropical Agricultural Sciences
Priority date: 2014-08-21
Filing date: 2014-08-21
Publication date: 2014-12-17
Anticipated expiration: 2024-08-21

Abstract

The utility model belongs to chemical experimental instrument field, relate to a kind of vertical efficient distiller, comprise cucurbit and superposing type condenser, described superposing type condenser is superposed from the bottom to top to connect firmly by plural bulb condensation room and forms, the lower end of the bulb condensation room of least significant end arranges grinding port plug, communicating pipe is inlayed in the centre of grinding port plug, the bottom of bulb condensation room arranges liquid outlet, external drain pipe, main drain pipe is communicated to after drain pipe series connection, gas port is set out in the middle part of bulb condensation room, pick out tracheae, the port of export of escape pipe is arranged at the inner upper of a bulb condensation room.The utility model adopts flush distillation, the mode of multi-stage condensing can improve distillation efficiency effectively, overcome that Conventional espresso device needs multicompartment to combine, take up room the shortcoming large, distillation efficiency is low, and without the need to cooling water condensation, have easy for installation, take table space less, water saving, efficiency high, there is realistic meaning.

Description

Vertical efficient distiller

Technical field

The utility model belongs to chemical experimental instrument field, relates to a kind of distiller, specifically a kind of vertical efficient distiller.

Background technology

Distillation be a kind of utilize each component volatilization in liquid mixture difference and by the mass transport process of Component seperation, the steam that liquid boiling produces by utilization evaporation, condensation process imports condenser pipe, make it cooling and condense into liquid, thus reach the effect being separated the larger mixture of boiling point difference, there is important Practical significance to the separation of liquid mixture.

In chemical analysis, often need to carry out distillation test, as the distilation, the distillation extraction of plant sample volatile oil, the distillation analysis of water sample etc. of inorganic acid.Traditional distilling apparatus is combined by assemblies such as iron stand (frame), cucurbit, distillation connector, condenser pipes, often kind of annex is indispensable, installation and removal are trouble quite, and it is larger to take table space, need to connect cooling water in still-process, waste water resource, and distillation efficiency is low.

Utility model content

The purpose of this utility model provides a kind of vertical efficient distiller, adopt flush distillation, the mode of multi-stage condensing can improve distillation efficiency effectively, overcome that Conventional espresso device needs multicompartment to combine, take up room the shortcoming large, distillation efficiency is low.

The technical scheme that the utility model adopts:

A kind of vertical efficient distiller, comprise cucurbit and superposing type condenser, the round-bottomed flask that cucurbit is, described superposing type condenser is superposed from the bottom to top to connect firmly by plural bulb condensation room and forms, the lower end of the bulb condensation room of least significant end arranges grinding port plug, can coincide with the bottleneck of cucurbit and insert, communicating pipe is inlayed in the centre of grinding port plug, after grinding port plug inserts the bottleneck of cucurbit, cucurbit can be communicated with bulb condensation room by communicating pipe, the steam in cucurbit is made to enter in bulb condensation room, the bottom of bulb condensation room arranges liquid outlet, external drain pipe, the main drain pipe of the bulb condensation room of least significant end is communicated to after the drain pipe series connection of each bulb condensation room, discharge after the distillate of each bulb condensation room concentrates on main drain pipe, accessed, a gas outlet is set in the middle part of bulb condensation room, pick out tracheae, the port of export of escape pipe is arranged at the inner upper of a bulb condensation room, bulb condensation indoor can be made to have little time the vapor flow of condensation to a upper bulb condensation room condensation again, thus realize the effect of multi-stage condensing.

The bottom of described cucurbit arranges annulus cover base, cucurbit can be placed on table top, pallet or heater, convenient dress sample and movement reposefully.

Described superposing type condenser to be connected firmly with lower supreme superposition by three bulb condensation rooms and forms.

The utility model adopts flush distillation, the mode of multi-stage condensing can improve distillation efficiency effectively, overcome that Conventional espresso device needs multicompartment to combine, take up room the shortcoming large, distillation efficiency is low, and without the need to cooling water condensation, have easy for installation, take table space less, water saving, efficiency high, there is realistic meaning.

Accompanying drawing explanation

Fig. 1 is structural representation of the present utility model.

In figure: 1, cucurbit; 2, primary spherical condensation chamber; 3, escape pipe; 4, secondary bulb condensation room; 5, three grades of level bulb condensation rooms; 6, drain pipe; 7, communicating pipe; 8, main drain pipe; 9, annulus cover base.

Detailed description of the invention

Below in conjunction with accompanying drawing with by embodiment, the utility model is described in further detail, but not as to restriction of the present utility model.

In the construction shown in fig. 1, the utility model comprises cucurbit 1 and superposing type condenser, the round-bottomed flask that cucurbit is, arranges annulus cover base 9, cucurbit can be placed reposefully on table top, pallet or heater bottom it, described superposing type condenser is superposed from the bottom to top to connect firmly by three bulb condensation rooms and forms, be respectively primary spherical condensation chamber 2, secondary bulb condensation room 4, three grades of level bulb condensation rooms 5, arranging in the lower end of primary spherical condensation chamber 2 to coincide inserts the grinding port plug of cucurbit bottleneck, communicating pipe 7 is inlayed in the centre of grinding port plug, after grinding port plug inserts the bottleneck of cucurbit, cucurbit 1 can be communicated with primary spherical condensation chamber 2 by communicating pipe 7, the steam in cucurbit is made to enter in primary spherical condensation chamber, the bottom of primary spherical condensation chamber 2 arranges liquid outlet, external main drain pipe 8, secondary bulb condensation room 4, the bottom of three grades of level bulb condensation rooms 5 arranges liquid outlet, external drain pipe 6, two, the main drain pipe 8 of primary spherical condensation chamber is communicated to after the drain pipe series connection of three grades of bulb condensation rooms, discharge after the distillate of every one-level bulb condensation room concentrates on main drain pipe, accessed, in the middle part of every one-level bulb condensation room, a gas outlet is set, pick out tracheae 3, the port of export of escape pipe is arranged at the inner upper of upper level bulb condensation room, bulb condensation indoor can be made to have little time the vapor flow of condensation to a upper bulb condensation room condensation again, thus realize the effect of multi-stage condensing.

During distillation procedure, cucurbit is firm, move to after adding sample to be distilled on heater, connect superposing type condenser, heating.Sample is vaporized under the effect of high temperature, steam enters into primary spherical condensation chamber 2 along communicating pipe 7, liquid is condensed at the effect lower part sample vapors of the temperature difference, liquid outlet along primary spherical condensation chamber 2 is discharged, another part sample vapors then enters into secondary bulb condensation room 4 by the gas outlet of primary spherical condensation chamber 2 through escape pipe 3 discharge, the function of primary spherical condensation chamber 2 is repeat in secondary bulb condensation room 4, by that analogy, three grades of bulb condensation rooms 5 repeat condensation.The sample liquids that last each bulb condensation room produces collects in main drain pipe 8 place and discharges, and is accessed, completes whole still-process.

The above is only preferred embodiment of the present utility model; should be understood that; for those skilled in the art; under the prerequisite not departing from the utility model know-why; can also make some improvements and modifications, these improvements and modifications also should be considered as protection domain of the present utility model.

Claims

1. a vertical efficient distiller, it is characterized in that: comprise cucurbit and superposing type condenser, the round-bottomed flask that cucurbit is, described superposing type condenser is superposed from the bottom to top to connect firmly by plural bulb condensation room and forms, the lower end of the bulb condensation room of least significant end arranges to coincide inserts the grinding port plug of cucurbit bottleneck, communicating pipe is inlayed in the centre of grinding port plug, the bottom of bulb condensation room arranges liquid outlet, external drain pipe, the main drain pipe of the bulb condensation room of least significant end is communicated to after the drain pipe series connection of each bulb condensation room, a gas outlet is set in the middle part of bulb condensation room, pick out tracheae, the port of export of escape pipe is arranged at the inner upper of a bulb condensation room.

2. vertical efficient distiller according to claim 1, is characterized in that: the bottom of described cucurbit arranges annulus cover base.

3. vertical efficient distiller according to claim 1, is characterized in that: described superposing type condenser to be connected firmly with lower supreme superposition by three bulb condensation rooms and forms.