CN203519545U - Fixture applied to electrochemical test - Google Patents

Fixture applied to electrochemical test Download PDF

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Publication number
CN203519545U
CN203519545U CN201320461347.7U CN201320461347U CN203519545U CN 203519545 U CN203519545 U CN 203519545U CN 201320461347 U CN201320461347 U CN 201320461347U CN 203519545 U CN203519545 U CN 203519545U
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CN
China
Prior art keywords
fixture
sample
test
sample cell
instrument connection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201320461347.7U
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Chinese (zh)
Inventor
于非
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
QINGYUAN JINSHENG ZR & TI RESOURCES Co Ltd
South China University of Technology SCUT
Original Assignee
QINGYUAN JINSHENG ZR & TI RESOURCES Co Ltd
South China University of Technology SCUT
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Filing date
Publication date
Application filed by QINGYUAN JINSHENG ZR & TI RESOURCES Co Ltd, South China University of Technology SCUT filed Critical QINGYUAN JINSHENG ZR & TI RESOURCES Co Ltd
Priority to CN201320461347.7U priority Critical patent/CN203519545U/en
Application granted granted Critical
Publication of CN203519545U publication Critical patent/CN203519545U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Devices For Use In Laboratory Experiments (AREA)

Abstract

The utility model discloses a fixture applied to an electrochemical test. The fixture comprises a fixture body (1), fixing bolts (1) and a copper plate (3), wherein the fixture body (2) is in a cuboid structure which is characterized in that a sample sink (7) is vertically downwards formed from the upper end surface, and a testing hole (6) communicated with the sample sink (7) is formed in the front end surface, thread holes connected with the fixing bolts (1) are formed from the rear end surface to the sample sink (7); and a testing sample (4) and the copper plate (3) are sequentially arranged from front to back in the sample sink (7).

Description

A kind of fixture that is applied to electro-chemical test
Technical field
The utility model relates to a kind of test fixture, particularly relates to a kind of fixture that is applied to electro-chemical test, belongs to Electrochemical Measurement Technology field.
Background technology
It is the working electrode of approximately 1 square centimeter that electrochemical property test need to be made test area.The conventional way in laboratory is that tape test sample is cut, and follows welding lead, and then the back side encapsulates with resin solidification.The method makes that flow process is complicated, and the cycle is long, not easy to operate, and cutting, welding and resin curing process easily affect specimen surface state, brings error.
Summary of the invention
The purpose of this utility model is to provide a kind of fixture that is applied to electro-chemical test, has solved the working electrode existing in prior art and has made flow process complexity, and the cycle is long, not easy-operating problem.
For realizing the utility model object, adopt following technical scheme:
Be applied to a fixture for electro-chemical test, comprise clamp body, set bolt and copper coin; Described clamp body is rectangular structure, from the upper surface of rectangular parallelepiped, has vertically downward sample cell, from the front end face of rectangular parallelepiped, is provided with taper instrument connection, and taper instrument connection is communicated with sample cell; From the rear end face of rectangular parallelepiped, to sample cell, be provided with threaded hole, set bolt is connected with threaded hole, is provided with successively from front to back test sample and copper coin in sample cell.
For further realizing the purpose of this utility model, preferably, the upper conical instrument connection upside of the front end face of described rectangular parallelepiped has exhaust groove.
The area of described taper instrument connection and sample cell junction is 1 square centimeter.
Described clamp body is made by teflon.
With respect to prior art, tool of the present utility model has the following advantages:
1, the utility model is without the special working electrode of making.During test, only sample need be clipped to test with fixture, without sample is cut, welding lead, the manufacturing process such as resin solidification encapsulation.
2, the utility model is simple to operate.Deducted the complicated manufacturing process of working electrode.
Accompanying drawing explanation
Fig. 1 is the structural representation that the utility model is applied to the fixture of electro-chemical test;
Fig. 2 is application the utility model fixture test schematic diagram;
Shown in figure: set bolt 1, clamp body 2, copper coin 3, test sample 4, exhaust groove 5, taper instrument connection 6, sample cell 7, beaker 8, test solution 9, to electrode 10 and contrast electrode 11.
Embodiment
For understanding better the utility model, below in conjunction with accompanying drawing, the utility model is further described, it should be noted that, embodiment does not form the restriction to the claimed scope of the utility model.
As shown in Figure 1, a kind of fixture that is applied to electro-chemical test, comprises clamp body 2, set bolt 1 and copper coin 3; Described clamp body 2 is rectangular structure, from the upper surface of rectangular parallelepiped, has vertically downward sample cell 7, from the front end face of rectangular parallelepiped, is provided with taper instrument connection 6, and taper instrument connection 6 is communicated with sample cell 7; From the rear end face of rectangular parallelepiped, to sample cell 7, be provided with threaded hole, set bolt 1 is connected with threaded hole, and sample cell 7 is provided with test sample 4 and copper coin 3 from front to back successively, and set bolt 1 is for fixing test sample 4 and copper coin 3; Upper conical instrument connection 6 upsides of front end face of rectangular parallelepiped have exhaust groove 5, are beneficial to the discharge of the gas producing in the gas of electrode surface absorption or test process.
Taper instrument connection 6 is 1 square centimeter with the area of sample cell 7 junctions; An important parameter in test is current density, i.e. the current value of unit area, and unit is ampere/square centimeter, so conventional electrode area is 1 square centimeter.
Clamp body 2 is made by teflon, has good dimensional stability, chemical stability, resistance to acids and bases, can be used in most test solutions.
During test, as shown in Figure 2, test solution 9 can be salt acid alkali etc.; Electrode 10 is connected with the counter electrode wiring of electrochemical workstation respectively with contrast electrode 11, test Different electrodes between electric current change in voltage; Sample 4 to be tested and copper coin 3 are put into sample cell 7 successively, adjusting sample 4 is exposed in taper instrument connection 6 test surfaces, bolt 1 is tightened, fixed sample, copper coin 3 is connected with working electrode lead-in wire, clamp body 2 is put into test solution 9 and tests, test Different electrodes between electric current change in voltage.
The fixture that the utility model provides is made by teflon, has good dimensional stability, chemical stability, resistance to acids and bases, can be used in most test solutions.
During test, only sample need be clipped to test with fixture, without sample is cut, welding lead, the manufacturing process such as resin solidification encapsulation, such as test metal surface galvanization coating performance, sample directly clips test with fixture and can test.

Claims (4)

1. a fixture that is applied to electro-chemical test, is characterized in that: comprise clamp body (2), set bolt (1) and copper coin (3); Described clamp body (2) is rectangular structure, from the upper surface of rectangular parallelepiped, has vertically downward sample cell (7), from the front end face of rectangular parallelepiped, is provided with taper instrument connection (6), and taper instrument connection (6) is communicated with sample cell (7); From the rear end face of rectangular parallelepiped, to sample cell (7), be provided with threaded hole, set bolt (1) is connected with threaded hole, is provided with successively from front to back test sample (4) and copper coin (3) in sample cell (7).
2. the fixture that is applied to electro-chemical test according to claim 1, is characterized in that: the upper conical instrument connection of front end face (6) upside of described rectangular parallelepiped has exhaust groove (5).
3. the fixture that is applied to electro-chemical test according to claim 1, is characterized in that: described taper instrument connection (6) is (1) square centimeter with the area of sample cell (7) junction.
4. the fixture that is applied to electro-chemical test according to claim 1, is characterized in that: described clamp body is made by teflon.
CN201320461347.7U 2013-07-30 2013-07-30 Fixture applied to electrochemical test Expired - Fee Related CN203519545U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201320461347.7U CN203519545U (en) 2013-07-30 2013-07-30 Fixture applied to electrochemical test

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201320461347.7U CN203519545U (en) 2013-07-30 2013-07-30 Fixture applied to electrochemical test

Publications (1)

Publication Number Publication Date
CN203519545U true CN203519545U (en) 2014-04-02

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201320461347.7U Expired - Fee Related CN203519545U (en) 2013-07-30 2013-07-30 Fixture applied to electrochemical test

Country Status (1)

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CN (1) CN203519545U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104359955A (en) * 2014-11-04 2015-02-18 沈阳建筑大学 Novel electrolytic bath
CN105424519A (en) * 2014-09-17 2016-03-23 济南大学 Objective table for friction and wear tester
CN105572198A (en) * 2016-03-09 2016-05-11 西安电子科技大学 Testing clamp of liquid corrosion-resisting electrochemical material electrode
CN109270137A (en) * 2018-11-02 2019-01-25 西南石油大学 It is a kind of to test scan-type electrochemical microscope sample stage of more gauge coupons with electrolytic cell

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105424519A (en) * 2014-09-17 2016-03-23 济南大学 Objective table for friction and wear tester
CN104359955A (en) * 2014-11-04 2015-02-18 沈阳建筑大学 Novel electrolytic bath
CN104359955B (en) * 2014-11-04 2017-11-28 沈阳建筑大学 A kind of Novel electrolytic tank
CN105572198A (en) * 2016-03-09 2016-05-11 西安电子科技大学 Testing clamp of liquid corrosion-resisting electrochemical material electrode
CN109270137A (en) * 2018-11-02 2019-01-25 西南石油大学 It is a kind of to test scan-type electrochemical microscope sample stage of more gauge coupons with electrolytic cell

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140402

Termination date: 20180730