CN203474700U - 提取反应器 - Google Patents
提取反应器 Download PDFInfo
- Publication number
- CN203474700U CN203474700U CN201220757326.5U CN201220757326U CN203474700U CN 203474700 U CN203474700 U CN 203474700U CN 201220757326 U CN201220757326 U CN 201220757326U CN 203474700 U CN203474700 U CN 203474700U
- Authority
- CN
- China
- Prior art keywords
- heat exchanger
- extraction
- extracting solution
- extraction reactor
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 143
- 239000008187 granular material Substances 0.000 claims abstract description 30
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 239000002245 particle Substances 0.000 claims description 44
- 230000008676 import Effects 0.000 claims description 43
- 230000001105 regulatory effect Effects 0.000 claims description 14
- 238000005192 partition Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 33
- 239000003795 chemical substances by application Substances 0.000 description 27
- 238000009835 boiling Methods 0.000 description 16
- 239000000203 mixture Substances 0.000 description 16
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 14
- 238000000034 method Methods 0.000 description 14
- 239000000178 monomer Substances 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 229920002292 Nylon 6 Polymers 0.000 description 12
- 239000000284 extract Substances 0.000 description 11
- 238000002156 mixing Methods 0.000 description 10
- 238000001816 cooling Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 235000013339 cereals Nutrition 0.000 description 7
- 238000013461 design Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 230000002706 hydrostatic effect Effects 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000004952 Polyamide Substances 0.000 description 4
- 230000033228 biological regulation Effects 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 230000001143 conditioned effect Effects 0.000 description 4
- 229920002647 polyamide Polymers 0.000 description 4
- 244000287680 Garcinia dulcis Species 0.000 description 3
- 150000001408 amides Chemical class 0.000 description 3
- 230000003301 hydrolyzing effect Effects 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000005086 pumping Methods 0.000 description 3
- 230000000717 retained effect Effects 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000006068 polycondensation reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000006353 environmental stress Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0207—Control systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0219—Fixed bed of solid material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/46—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Automation & Control Theory (AREA)
- Extraction Or Liquid Replacement (AREA)
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
- Polyamides (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261722899P | 2012-11-06 | 2012-11-06 | |
| US61/722,899 | 2012-11-06 | ||
| EP12191455.0 | 2012-11-06 | ||
| EP12191455.0A EP2727637B1 (de) | 2012-11-06 | 2012-11-06 | Extraktionsreaktor sowie verfahren zur extraktion von granulärem material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203474700U true CN203474700U (zh) | 2014-03-12 |
Family
ID=47115619
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201220757326.5U Expired - Lifetime CN203474700U (zh) | 2012-11-06 | 2012-11-21 | 提取反应器 |
| CN201380058137.6A Active CN104780988B (zh) | 2012-11-06 | 2013-10-21 | 用于萃取颗粒材料的萃取反应器和方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380058137.6A Active CN104780988B (zh) | 2012-11-06 | 2013-10-21 | 用于萃取颗粒材料的萃取反应器和方法 |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP2727637B1 (enExample) |
| JP (1) | JP6359021B2 (enExample) |
| KR (1) | KR102097290B1 (enExample) |
| CN (2) | CN203474700U (enExample) |
| ES (1) | ES2747448T3 (enExample) |
| IN (1) | IN2015DN02955A (enExample) |
| PL (1) | PL2727637T3 (enExample) |
| SI (1) | SI2727637T1 (enExample) |
| TW (1) | TWI612997B (enExample) |
| WO (1) | WO2014072167A1 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111330309A (zh) * | 2020-03-30 | 2020-06-26 | 浙江温兄机械阀业有限公司 | 物料分层式动态提取设备及其提取方法 |
| CN117225004A (zh) * | 2023-11-14 | 2023-12-15 | 湖南禧又多油脂有限公司 | 一种基于物联网的植物油低温萃取处理自动控制系统 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102018222874A1 (de) | 2017-12-22 | 2019-06-27 | Thyssenkrupp Ag | Vorrichtung und Verfahren zum kontinuierlichen Hochdruckbehandeln von Schüttgut sowie Verwendung |
| CN112430498B (zh) * | 2020-11-20 | 2024-09-03 | 湖南和广生物科技有限公司 | 一种多料篮梯级分步超临界流体萃取釜 |
| CN116036645B (zh) * | 2022-11-28 | 2025-10-21 | 福建省力恒锦纶实业有限公司 | 一种低熔点共聚酰胺的连续萃取方法 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2248220A (en) * | 1938-05-26 | 1941-07-08 | Mid Continent Petroleum Corp | Method of separating constituents of mineral oils |
| US2578670A (en) * | 1946-08-12 | 1951-12-18 | Robert A Carleton | Method of deodorizing and stabilizing soybean oil |
| DE1012479B (de) | 1952-06-07 | 1957-07-18 | Hessische Berg Und Huettenwerk | Verfahren zur Messung der Gaszusammensetzung von zwei oder mehr regenerativ beheizten Systemen, z. B. Hochofen-Winderhitzern |
| DE2242642C3 (de) * | 1972-08-30 | 1980-06-19 | Basf Ag, 6700 Ludwigshafen | Verfahren zum kontinuierlichen Extrahieren von Polylactamen |
| DE2404510C3 (de) * | 1974-01-31 | 1985-02-21 | Basf Ag, 6700 Ludwigshafen | Extraktionsrohr für Polyamide |
| US4160647A (en) * | 1975-08-02 | 1979-07-10 | Chimkombinat | Continuous operation extractor |
| DD206999A1 (de) * | 1981-09-04 | 1984-02-15 | Peter Kramer | Kontinuierliches extraktionsverfahren fuer kunststoff-granulat |
| JPS5925803A (ja) * | 1982-08-03 | 1984-02-09 | Mitsui Toatsu Chem Inc | 向流洗浄塔および合成樹脂スラリ−の洗浄方法 |
| DE19752182A1 (de) * | 1997-11-25 | 1999-05-27 | Basf Ag | Verfahren zur kontinuierlichen Extraktion von Polyamid |
| DE19752183A1 (de) * | 1997-11-25 | 1999-05-27 | Basf Ag | Verfahren zur kontinuierlichen Extraktion von Polyamid |
| DE19801267B4 (de) * | 1998-01-15 | 2005-03-24 | Inventa-Fischer Gmbh | Verfahren zur Herstellung von PA-6 Granulat und dessen Verwendung |
| DE19808442A1 (de) * | 1998-02-27 | 1999-09-02 | Basf Ag | Verfahren zur Extraktion von Polyamidteilchen |
| DE10124579A1 (de) | 2001-05-21 | 2002-12-05 | Bayer Ag | Verfahren und Vorrichtung zur Extraktion von Polyamid |
| US6479620B1 (en) * | 2001-06-01 | 2002-11-12 | E. I. Du Pont De Nemours And Company | Process for converting caprolactam to nylon 6 |
| JP2008080267A (ja) * | 2006-09-28 | 2008-04-10 | Toray Ind Inc | 複合式熱交換型反応器およびそれを用いたポリカプロアミドプレポリマーの製造方法 |
| DE102007061136A1 (de) * | 2007-12-19 | 2009-06-25 | Glatt Ingenieurtechnik Gmbh | Verfahren und Vorrichtung zur mehrstufigen Behandlung von dispersen Feststoffen |
| DE102008044452A1 (de) | 2008-08-19 | 2010-02-25 | Lurgi Zimmer Gmbh | Kontinuierliches Verfahren zur Extraktion von Polyamid-6 |
| US8425655B2 (en) * | 2010-07-09 | 2013-04-23 | Carbon Capture Scientific, Llc | Gas pressurized separation column and process to generate a high pressure product gas |
-
2012
- 2012-11-06 ES ES12191455T patent/ES2747448T3/es active Active
- 2012-11-06 SI SI201231667T patent/SI2727637T1/sl unknown
- 2012-11-06 EP EP12191455.0A patent/EP2727637B1/de active Active
- 2012-11-06 PL PL12191455T patent/PL2727637T3/pl unknown
- 2012-11-21 CN CN201220757326.5U patent/CN203474700U/zh not_active Expired - Lifetime
-
2013
- 2013-10-21 JP JP2015540093A patent/JP6359021B2/ja not_active Expired - Fee Related
- 2013-10-21 WO PCT/EP2013/071987 patent/WO2014072167A1/de not_active Ceased
- 2013-10-21 IN IN2955DEN2015 patent/IN2015DN02955A/en unknown
- 2013-10-21 CN CN201380058137.6A patent/CN104780988B/zh active Active
- 2013-10-21 KR KR1020157010916A patent/KR102097290B1/ko active Active
- 2013-11-01 TW TW102139683A patent/TWI612997B/zh active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111330309A (zh) * | 2020-03-30 | 2020-06-26 | 浙江温兄机械阀业有限公司 | 物料分层式动态提取设备及其提取方法 |
| CN111330309B (zh) * | 2020-03-30 | 2021-09-21 | 浙江温兄机械阀业有限公司 | 物料分层式动态提取设备及其提取方法 |
| CN117225004A (zh) * | 2023-11-14 | 2023-12-15 | 湖南禧又多油脂有限公司 | 一种基于物联网的植物油低温萃取处理自动控制系统 |
| CN117225004B (zh) * | 2023-11-14 | 2024-01-26 | 湖南禧又多油脂有限公司 | 一种基于物联网的植物油低温萃取处理自动控制系统 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2016502458A (ja) | 2016-01-28 |
| CN104780988B (zh) | 2017-06-16 |
| PL2727637T3 (pl) | 2020-02-28 |
| SI2727637T1 (sl) | 2019-11-29 |
| EP2727637B1 (de) | 2019-08-28 |
| KR102097290B1 (ko) | 2020-04-06 |
| EP2727637A1 (de) | 2014-05-07 |
| ES2747448T3 (es) | 2020-03-10 |
| WO2014072167A1 (de) | 2014-05-15 |
| JP6359021B2 (ja) | 2018-07-18 |
| TWI612997B (zh) | 2018-02-01 |
| IN2015DN02955A (enExample) | 2015-09-18 |
| CN104780988A (zh) | 2015-07-15 |
| KR20150105293A (ko) | 2015-09-16 |
| TW201424819A (zh) | 2014-07-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20140312 |
|
| CX01 | Expiry of patent term |