CN203281064U - Automatic solid-liquid extraction device - Google Patents
Automatic solid-liquid extraction device Download PDFInfo
- Publication number
- CN203281064U CN203281064U CN201320294261XU CN201320294261U CN203281064U CN 203281064 U CN203281064 U CN 203281064U CN 201320294261X U CN201320294261X U CN 201320294261XU CN 201320294261 U CN201320294261 U CN 201320294261U CN 203281064 U CN203281064 U CN 203281064U
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- CN
- China
- Prior art keywords
- filter
- extraction device
- extraction
- conduit
- filter house
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0219—Fixed bed of solid material
Abstract
The utility model discloses an automatic solid-liquid extraction device which comprises an extraction reaction vessel and an effective solution storage container. The extraction reaction vessel communicates with the effective solution storage container through a conduit which is provided with a pump. The automatic solid-liquid extraction device also comprises a filter unit which communicates with one end of the conduit extending into the extraction reaction vessel. The filter unit comprises a filter unit housing and a filter part disposed inside the filter unit housing. The conduit is connected with the filter unit housing so as to communicate with the filter unit. The automatic solid-liquid extraction device also comprises a condensation device, two ends of which both communicate with the conduit. The condensation device comprises a condensation device housing and a dehydration material and a filter which are disposed inside the condensation device housing. By the adoption of the solid-liquid extraction device with the above structure, automatic extraction can be realized, and effective components can be obtained by filtration and extraction.
Description
Technical field
The utility model relates to a kind of extraction equipment, particularly relates to a kind of automatic liquid-solid extraction device.
Background technology
Extraction is the difference of utilizing compound solubility or distribution coefficient in the solvent of two kinds immiscible (or slightly solubles), thereby makes compound transfer to the process that another solvent, it is extracted in a kind of solvent.Extraction has dual mode: liquid-liquid extraction and liquid-solid extraction, liquid-liquid extraction is with certain component in selected separated from solvent liquid mixture, solvent must be immiscible with the mixture liquid that is extracted, has optionally solvability, and the heat endurance that must have and chemical stability,, as separate the phenol in coal tar with benzene,, with the alkene in organic solvent separation petroleum distillate, use CCl
4Br in extraction water
2Liquid-solid extraction, also crying leaching, is with the active ingredient in extractant extraction solid mixture, as the carbohydrate with in the water extraction beet, to improve oil yield, water leaches active ingredient to produce liquid extract " oozing drop " or " leaching " from Chinese medicine with the soya-bean oil in alcohol leaching soya bean.Extraction is to be used for purifying one of means with purifying compounds in Organic Chemistry Laboratory., by extraction, can extract needed compound from solid or liquid mixture.Extraction now has been applied to the separation of petroleum distillate and has made with extra care, the extraction of uranium, thorium, plutonium and purifying, the extraction of non-ferrous metal, rare metal, precious metal with separate, the extraction of antibiotic, organic acid, alkaloid, blood active ingredient, and wastewater treatment etc.Extraction is compared with the method for other separation solution components, and advantage is easy to operate and saves the energy.But present liquid-solid extraction device can not be realized auto extractive and filter simultaneously the active ingredient that extraction obtains.
Summary of the invention
Technical problem to be solved in the utility model is to provide a kind of and can realize auto extractive and filter simultaneously the liquid-solid extraction device that extracts the active ingredient that obtains.
For solving above technical problem, the technical solution of the utility model is: a kind of automatic liquid-solid extraction device, comprise extractive reaction container and effective solution storage container, described extractive reaction container and described effective solution storage container are communicated with by conduit, be provided with pump on described conduit, its key is: also comprise with described conduit and extend into the filter that an end of described extractive reaction container is communicated with.
As improvement one of the present utility model, also comprise the enrichment facility that two ends all are communicated with described conduit, described enrichment facility comprises the enrichment facility shell and is arranged on described enrichment facility shell interior dehydrating material and filtering bodies.
Further improve as the utility model, described pump is plunger displacement pump.
Further improve as the utility model, also comprise the stirrer that is arranged in described extractive reaction container.
As improvement two of the present utility model, described filter comprises the filter shell and is arranged at first order filter house in described filter shell, and described conduit is by being connected to realize to be communicated with described filter with described filter shell.
Further improve as the utility model, described first order filter house is that aperture is less than or equal to the filter pad of 10 microns.
Further improve as the utility model, described filter also comprises second level filter house, and described second level filter house is arranged on the below of described first order filter house, and described second level filter house is that density is less than or equal to 680kg/m
3Mineral wool.
Further improve as the utility model, described filter also comprises third level filter house, and described third level filter house is arranged on the below of described second level filter house, and described third level filter house is that density is less than or equal to 20kg/m
3Mineral wool.
By implement the utility model desirable following beneficial effect:
A kind of automatic liquid-solid extraction device, comprise extractive reaction container and effective solution storage container, described extractive reaction container and described effective solution storage container are communicated with by conduit, be provided with pump on described conduit, also comprise with described conduit and extend into the filter that an end of described extractive reaction container is communicated with.The fully reaction in the extractive reaction container of extractant and plan extraction components, be dissolved with the solvent of intending extraction components and be pumped in effective solution storage container after filter filters, so just can realize that automatic liquid-solid extraction and filtration are dissolved with the extractant of intending extraction components.
Described filter comprises the filter shell and is arranged at the interior first order filter house of described filter shell, described conduit is by being connected to realize to be communicated with described filter with described filter shell, and described first order filter house is that aperture is less than or equal to the filter pad of 10 microns.First order filter house can fall the most of contaminant filter that is dissolved with in the solvent of intending extraction components, greatly reduces the content of the impurity in the solution that obtains.Third level filter house tentatively filters being dissolved with the solvent of intending extraction components, the be dissolved with solvent of intending extraction components of second level filter house after to preliminary filtration filters again, the last filtration of passing through again first order filter house, three-stage filtration can improve effect and the efficiency of filtration.Automatic extraction apparatus also comprises the enrichment facility that two ends all are communicated with described conduit, described enrichment facility comprises the enrichment facility shell and is arranged on described enrichment facility shell interior dehydrating material and filtering bodies, enrichment facility can be taken off being dissolved with the moisture that contains in the solvent of intending extraction components, and simultaneously further filtration can reduce the content of the impurity in the solution that obtains.Described pump is plunger displacement pump, uses plunger displacement pump can accurately control flow, thereby can all be drawn in effective solution storage container being dissolved with the solvent of intending extraction components, has reached the purpose that improves extraction efficiency.The compact conformation of plunger displacement pump own, can guarantee that automatic extraction apparatus has less floor space, reaches joint space-efficient purpose.Automatically the liquid-solid extraction device also comprises the stirrer that is arranged in described extractive reaction container, and stirrer can drive the solution motion in the extractive reaction container, thereby allows extractant and plan extraction components fully mix to reach the purpose that improves extraction efficiency.
Description of drawings
Below in conjunction with Figure of description, the utility model is done further detailed description, wherein:
Fig. 1 is overall structure schematic diagram of the present utility model;
Fig. 2 is filter apparatus configuration schematic diagram in the utility model;
Fig. 3 is enrichment facility structural representation in the utility model.
The specific embodiment
As shown in Figure 1, a kind of automatic liquid-solid extraction device, comprise extractive reaction container 11 and effective solution storage container 12, described extractive reaction container 11 and described effective solution storage container 12 are communicated with by conduit 13, be provided with pump 14 on described conduit 13, also comprise with described conduit 13 and extend into the filter 150 that an end of described extractive reaction container 11 is communicated with, described pump 14 is preferably plunger displacement pump.
As shown in Figure 2, described filter 150 comprises filter shell 154 and is arranged at the interior first order filter house 151 of described filter shell 154, described conduit 13 is by being connected to realize to be communicated with described filter 150 with described filter shell 154, and described first order filter house 151 is less than or equal to the filter pad of 10 microns for aperture.Described filter also comprises second level filter house 152 and third level filter house 153, and described second level filter house 152 is arranged on the below of described first order filter house 151, and described third level filter house 153 is arranged on the below of described second level filter house 152.Described second level filter house 152 is less than or equal to 680kg/m for density
3Mineral wool, described third level filter house 153 is less than or equal to 20kg/m for density
3Mineral wool.
As shown in Figure 1,3, described automatic extraction apparatus also comprises the two ends enrichment facility 160 that all with described conduit 13, is communicated with and the stirrer 17 that is arranged in described extractive reaction container 11, and described enrichment facility 160 comprises enrichment facility shell 161 and is arranged on interior dehydrating material 162 and the filtering bodies 163 of described enrichment facility shell 161.
Must be pointed out some non-limiting illustrating that above-described embodiment is just made the utility model.But person of skill in the art will appreciate that, do not departing under aim of the present utility model and scope, can make modification to the utility model, replace and change, these modifications, replacement and change still belong to protection domain of the present utility model.
Claims (10)
1. automatic liquid-solid extraction device, comprise extractive reaction container (11) and effective solution storage container (12), described extractive reaction container (11) and described effective solution storage container (12) are communicated with by conduit (13), be provided with pump (14) on described conduit (13), it is characterized in that: also comprise with described conduit (13) and extend into the filter (150) that an end of described extractive reaction container (11) is communicated with.
2. a kind of automatic liquid-solid extraction device according to claim 1, it is characterized in that: described filter (150) comprises filter shell (154) and is arranged at first order filter house (151) in described filter shell (154), and described conduit (13) is communicated with described filter (150) by being connected with described filter shell (154) with realization.
3. a kind of automatic liquid-solid extraction device according to claim 2, it is characterized in that: described first order filter house (151) is less than or equal to the filter pad of 10 microns for aperture.
4. a kind of automatic liquid-solid extraction device according to claim 3, it is characterized in that: described filter also comprises second level filter house (152), described second level filter house (152) is arranged on the below of described first order filter house (151).
5. a kind of automatic liquid-solid extraction device according to claim 4, it is characterized in that: described second level filter house (152) is less than or equal to 680kg/m for density
3Mineral wool.
6. a kind of automatic liquid-solid extraction device according to claim 5, it is characterized in that: described filter (150) also comprises third level filter house (153), described third level filter house (153) is arranged on the below of described second level filter house (152).
7. a kind of automatic liquid-solid extraction device according to claim 6, it is characterized in that: described third level filter house (153) is less than or equal to 20kg/m for density
3Mineral wool.
8. the described a kind of automatic liquid-solid extraction device of any one claim according to claim 1 to 7, it is characterized in that: also comprise the enrichment facility (160) that two ends all are communicated with described conduit (13), described enrichment facility (160) comprises enrichment facility shell (161) and is arranged on described enrichment facility shell (161) interior dehydrating material (162) and filtering bodies (163).
9. a kind of automatic liquid-solid extraction device according to claim 8, it is characterized in that: described pump (14) is plunger displacement pump.
10. a kind of automatic liquid-solid extraction device according to claim 9, is characterized in that: also comprise the stirrer (17) that is arranged in described extractive reaction container (11).
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320294261XU CN203281064U (en) | 2013-05-27 | 2013-05-27 | Automatic solid-liquid extraction device |
| PCT/CN2014/070048 WO2014190768A1 (en) | 2013-05-27 | 2014-01-02 | Automatic solid-liquid extraction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320294261XU CN203281064U (en) | 2013-05-27 | 2013-05-27 | Automatic solid-liquid extraction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203281064U true CN203281064U (en) | 2013-11-13 |
Family
ID=49537446
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320294261XU Expired - Lifetime CN203281064U (en) | 2013-05-27 | 2013-05-27 | Automatic solid-liquid extraction device |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN203281064U (en) |
| WO (1) | WO2014190768A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014190768A1 (en) * | 2013-05-27 | 2014-12-04 | 北京华阳利民仪器有限公司 | Automatic solid-liquid extraction device |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0208766D0 (en) * | 2002-04-02 | 2002-05-29 | Univ Surrey | Liquid-liquid separation |
| CN202506167U (en) * | 2011-12-16 | 2012-10-31 | 江西师范大学 | Novel extraction and concentration device |
| CN202526937U (en) * | 2012-04-12 | 2012-11-14 | 成都科尔医药技术有限公司 | Dynamic extracting and concentrating integrated device for traditional Chinese medicines |
| CN203281064U (en) * | 2013-05-27 | 2013-11-13 | 北京华阳利民仪器有限公司 | Automatic solid-liquid extraction device |
-
2013
- 2013-05-27 CN CN201320294261XU patent/CN203281064U/en not_active Expired - Lifetime
-
2014
- 2014-01-02 WO PCT/CN2014/070048 patent/WO2014190768A1/en active Application Filing
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014190768A1 (en) * | 2013-05-27 | 2014-12-04 | 北京华阳利民仪器有限公司 | Automatic solid-liquid extraction device |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2014190768A1 (en) | 2014-12-04 |
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| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20131113 |
|
| CX01 | Expiry of patent term |