CN203244977U - Experimental device simulating reaction vessel - Google Patents
Experimental device simulating reaction vessel Download PDFInfo
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- CN203244977U CN203244977U CN 201220666213 CN201220666213U CN203244977U CN 203244977 U CN203244977 U CN 203244977U CN 201220666213 CN201220666213 CN 201220666213 CN 201220666213 U CN201220666213 U CN 201220666213U CN 203244977 U CN203244977 U CN 203244977U
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Abstract
An experimental device simulating a reaction vessel comprises a mini-type sealed container (1), a container bracket (2), a bracket rotating shaft (3), a rotating shaft support (4), an oil tank (5), an electric heating tube (6) and a temperature controller (7), wherein the mini-type sealed container (1) is a steel pressure-proof container and comprises a container casing (8) and a container cover (9); the bracket rotating shaft (3) is connected with two sides of the container bracket (2); the bracket rotating shaft (3) is driven by a transmission (speed reducing) mechanism through a motor; the rotating shaft support (4) is fixed on support plates on two sides of the oil tank (5); the electric heating tube (6) is mounted at the bottom of the oil tank; and the temperature controller (7) is mounted on one side of the oil tank. The experimental device can test a plurality of samples at a time, the efficiency is high, required materials are few, the relative property is high, the test cost is low, and the experimental device is suitable for reaction tests of materials in industrials such as chemical, wet metallurgy, pharmacy and the like.
Description
Technical field
The utility model relates to a kind of experimental provision of simulating chemical reaction container, belongs to the commerical test field.
Background technology
In industrial production, the technological parameter of a lot of material reactions and the technical indicator that can reach all need to come by experiment to determine.Common experiment is a kind of with reaction vessel to be miniature pressure vessel, and it can be tested under the conditions such as different temperatures, pressure.Microscale experiment lacks even stirring with the material in the reaction vessel, produces easily the uneven phenomenon such as deposition, knot wall, layering, affects experiment effect, and the material variety of adaptation is limited.Usually, such experiment container is single operation, and conventional efficient is lower.Another kind of common experiment reaction vessel is small-sized withstand voltage reactor, and reactor is generally with agitating device and heating (cooling) device, but the simulate actual production conditions.But small test is relatively large because of volume with reactor, and it is larger to test required inventory, and experimental cost is higher.In addition, small test is higher with the reactor cost, once can only test a sample (a kind of material component situation), and the experimental result comparativity is relatively poor, and conventional efficient is lower.
Summary of the invention
Deficiency for existing material reaction experimental provision, the present invention proposes a kind of experimental provision of simulating industrial microminiature reaction vessel, this device contains a plurality of microminiature reaction vessels, can carry out simultaneously one group of experiment to a sample or a plurality of sample, conventional efficient is high, contrast property is strong, can rapid screening go out the optimum process condition of a certain reaction.
The technical scheme that the utility model is taked is:
A kind of experimental provision of simulation reaction container comprises: microminiature airtight container (1), pan straddle (2), support turning cylinder (3), turning cylinder support (4), oil groove (5), electrothermal tube (6) and temperature control instrument (7).It is characterized in that: microminiature airtight container (1) is fixed on the pan straddle (2), the both sides of pan straddle (2) link to each other with support turning cylinder (3), support turning cylinder (3) is supported by the turning cylinder support (4) of both sides, on the support turning cylinder (3) of pan straddle (2) one ends gear or sprocket wheel are housed, driven by transmission (deceleration) mechanism by motor, turning cylinder supports (4) and is fixed on the support plate of oil groove (5) both sides, and electrothermal tube (6) is equipped with in oil groove (5) bottom, a side is equipped with temperature control instrument (7).
Described microminiature airtight container (1) is comprised of container casing (8) and container cover (9), and container casing (8) is connected by screw thread, bayonet socket or flange with container cover (9).
The axis of described microminiature airtight container (1) is vertical with the axis of turning cylinder (3).
An amount of steel ball of packing in the described microminiature airtight container is in order to stir or grind material.
It is rolling bearing pedestal that described turning cylinder supports (4).
Described pan straddle (2) can be laid a plurality of microminiature airtight containers (1).
The utility model has the advantage of:
The experimental provision that the utility model relates to can place a plurality of (group) sample under the unified experiment condition, can once test under similar and different condition a plurality of identical or different samples, have that test efficiency height, required inventory are few, contrast property is strong, adapt to the characteristics such as the wide and experimentation cost of material scope is low.Experimental provision simultaneously described in the utility model is made simple, and cost is low, is suitable for the material reaction test of the industries such as chemical industry, hydrometallurgy, pharmacy.
Description of drawings
Fig. 1 is the experimental provision schematic diagram of a kind of simulation reaction container of the utility model;
Fig. 2 is the microminiature airtight container schematic diagram of the experimental provision of a kind of simulation reaction container of the utility model.
Specific embodiment
The experimental provision of a kind of simulation reaction container described in the utility model is suitable for the industry chemistry reaction tests such as chemical industry, hydrometallurgy, pharmacy, for example this experimental provision can be applied in the ammonium molybdate industry, the research ammonia leaching residue at a certain temperature, in the impact on the leaching rate of molybdenum of the kind of different solid-to-liquid ratios, different basicity and alkali.
Fig. 1 described in the utility model is the experimental provision schematic diagram of simulation reaction container, and Fig. 2 is microminiature airtight container schematic diagram.
Container casing (8) and the container cover (9) of the steel of present embodiment is withstand voltage microminiature airtight container (1) are threaded connection.Pan straddle (2) can be placed six microminiature airtight containers (1) simultaneously, and the axis of microminiature airtight container (1) is vertical with the axis of support turning cylinder (3).The both sides of pan straddle (2) link to each other with support turning cylinder (3), and support turning cylinder (3) supports (4) by turning cylinder and supported, and turning cylinder support (4) is fixed on the support plate of (5) both sides in the oil groove.On the support turning cylinder (3) of pan straddle (2) one ends gear is housed, the gear engagement with on the outer reducing motor axle of oil groove drives whole pan straddle (2) rotation.The microminiature airtight container is equipped with an amount of steel ball in (1), and the steel ball when pan straddle (2) rotates in the microminiature airtight container (1) can stir and grind material.The oil groove bottom also is provided with electrothermal tube (6), and a side is equipped with temperature control instrument (7), can be controlled under the different temperatures and reacts.
The lixiviate molybdenum experimental program of ammonia leaching residue: take the ammonia leaching residue of 6 parts of equivalent as one group, under the consistent condition of other experiment conditions, add the alkali kind by different solid ratio, different basicity, difference respectively and be mixed with 3 groups of (6 parts every group) experiment samples, in every group of disposable 6 microminiature airtight containers (1) of packing into of sample, under identical temperature, reaction time condition, test.During experiment, container cover (9) is opened, added sample contents and expect in the container casing (8), put into simultaneously an amount of steel ball, screw container cover (9) sealing.The microminiature airtight container (1) that installs material is placed in the pan straddle (2).In oil groove (5), add an amount of conduction oil, be advisable to flood pan straddle (2), open motor and rotate by pan straddle (2), with electrothermal tube in the oil groove (6) energising heating, utilize temperature control instrument (7) with the oil temperature heating and be controlled in the certain temperature range insulation certain hour.After reaction finishes, the rotation of stopped heating and microminiature airtight container (1), take out 6 containers, molybdenum leaching rate to the interior ammonia leaching residue of 6 microminiature airtight containers (1) is analyzed, can determine in the situation of other term harmonizations, different solid ratio, different basicity and the different alkali kinds that add are determined more excellent process conditions to the impact of molybdenum leaching rate.
Utilize this experimental provision, can optimize expeditiously the technical data of a certain chemical reaction, such as the impact of reaction time on the leaching rate of ammonia leaching residue lixiviate molybdenum, need only be with 6 experiment containers in the other technologies parameter all in the identical situation, by taking out in turn of time parameter request, analyze experimental result, can draw the reaction time parameter to the rule that affects of leaching rate.And for example ammonia leaching residue is carried out in various degree grinding, can test the grain size parameter that draws the reactant ammonia leaching residue to the rule that affects of leaching rate.Equally also can test out fast the reaction temperature parameter leaching rate affected rule etc., can be optimized the related process parameter after the affecting rule and all understand of leaching rate at each technological parameter.
Claims (6)
1. the experimental provision of a simulation reaction container comprises that microminiature airtight container (1), pan straddle (2), support turning cylinder (3), turning cylinder support (4), oil groove (5), electrothermal tube (6) and temperature control instrument (7); It is characterized in that: microminiature airtight container (1) is fixed in the pan straddle (2), the both sides of pan straddle (2) link to each other with support turning cylinder (3), support turning cylinder (3) is supported by the turning cylinder support (4) of both sides, the turning cylinder (3) of pan straddle (2) one ends is driven by the transmission speed reducer structure by motor, turning cylinder supports (4) and is fixed on the support plate of oil groove (5) both sides, and electrothermal tube (6) is equipped with in oil groove (5) bottom, a side is equipped with temperature control instrument (7).
2. the experimental provision of a kind of simulation reaction container according to claim 1, it is characterized in that: described microminiature airtight container (1) is comprised of container casing (8) and container cover (9), and container casing (8) is connected by screw thread, bayonet socket or flange with container cover (9).
3. the experimental provision of a kind of simulation reaction container according to claim 1, it is characterized in that: the axis of described microminiature airtight container (1) is vertical with the axis of support turning cylinder (3).
4. the experimental provision of a kind of simulation reaction container according to claim 1 is characterized in that: in the described microminiature airtight container (1) an amount of steel ball is housed so that when the device operation to container in material stir and grind.
5. the experimental provision of simulation reaction container according to claim 1 is characterized in that: turning cylinder supports (4) and is rolling bearing pedestal.
6. the experimental provision of simulation reaction container according to claim 1, be further characterized in that: described pan straddle (2) once can be laid a plurality of microminiature airtight containers (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220666213 CN203244977U (en) | 2012-12-06 | 2012-12-06 | Experimental device simulating reaction vessel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220666213 CN203244977U (en) | 2012-12-06 | 2012-12-06 | Experimental device simulating reaction vessel |
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| Publication Number | Publication Date |
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| CN203244977U true CN203244977U (en) | 2013-10-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 201220666213 Expired - Fee Related CN203244977U (en) | 2012-12-06 | 2012-12-06 | Experimental device simulating reaction vessel |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102974296A (en) * | 2012-12-06 | 2013-03-20 | 江西稀有稀土金属钨业集团有限公司 | Experimental device for simulating reaction container |
| CN104841350A (en) * | 2015-05-26 | 2015-08-19 | 江西稀有金属钨业控股集团有限公司 | Experimental device for simulating material reaction in reaction vessel during industrial production |
| CN110898791A (en) * | 2018-09-18 | 2020-03-24 | 北京嘉德宜邦石油科技开发有限公司 | Crude oil low-temperature oxidation reaction device |
| CN112138618A (en) * | 2020-10-13 | 2020-12-29 | 湖南洋韬材料科技有限公司 | Airtight light-resistant reaction unit |
-
2012
- 2012-12-06 CN CN 201220666213 patent/CN203244977U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102974296A (en) * | 2012-12-06 | 2013-03-20 | 江西稀有稀土金属钨业集团有限公司 | Experimental device for simulating reaction container |
| CN104841350A (en) * | 2015-05-26 | 2015-08-19 | 江西稀有金属钨业控股集团有限公司 | Experimental device for simulating material reaction in reaction vessel during industrial production |
| CN110898791A (en) * | 2018-09-18 | 2020-03-24 | 北京嘉德宜邦石油科技开发有限公司 | Crude oil low-temperature oxidation reaction device |
| CN112138618A (en) * | 2020-10-13 | 2020-12-29 | 湖南洋韬材料科技有限公司 | Airtight light-resistant reaction unit |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131023 Termination date: 20171206 |