CN107096473A - A kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring - Google Patents
A kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring Download PDFInfo
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- CN107096473A CN107096473A CN201710498804.2A CN201710498804A CN107096473A CN 107096473 A CN107096473 A CN 107096473A CN 201710498804 A CN201710498804 A CN 201710498804A CN 107096473 A CN107096473 A CN 107096473A
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- derotation
- motor
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- twin
- liquid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses a kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring, a kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring, including reactor and agitator and base, the centre position of described base is provided with derotation motor, the top of derotation motor is provided with derotation motor shaft, the top of derotation motor shaft is connected with shaft coupling, one end of described shaft coupling is connected with derotation motor shaft, the other end of shaft coupling is connected with derotation power transmission shaft, the centre position of the bottom of reactor is provided with derotation axle bearing, described derotation power transmission shaft is spacing in derotation axle bearing, the bottom of derotation power transmission shaft is provided with driving turntable, sealing gasket is provided between the baseplane of derotation axle bearing and reactor inner chamber；The beneficial effects of the invention are as follows：Reaction speed faster, it is more thorough；Solid, liquid reactants and catalyst can be efficiently separated simultaneously, the time that the arrangement of experiment is dealt with problems arising from an accident has been saved.
Description
Technical field
The present invention relates to a kind of chemical engineering experiment equipment, specifically a kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring.
Background technology
The chemical reaction carried out under catalyst action referred to as catalytic reaction.In chemical reaction, reaction molecular it is original certain
A little chemical bonds, it is necessary to dissociate and form new chemical bond, this needs certain activation energy.
Solid-liquid reaction is one of reactive mode for commonly using in chemical experiment production process.It is special due to reaction condition itself
Property, during the course of the reaction, solid reacts with liquid in contact process, due to the difference of both physical properties itself,
The way typically used on the market is to carry out liquid agitation, and vortex is formed in kettle by liquid, while catalyst is used,
Both reaction efficiencies and speed of experiment are improved, but existing agitating mode is relatively simple, and need to enter again unavoidably in stirring
Row separation of solid and liquid flow, experimental provision is different from industrial processes, it is necessary to keep the accuracy that reaction product is calculated, and follow-up real
Test the simplicity for arrangement measure of dealing with problems arising from an accident；Existing chemical plant installations often considers from the requirement of industrial operations, it is difficult to meet the need of experiment
Will.
The content of the invention
It is an object of the invention to provide a kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the present invention provides following technical scheme：
A kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring, a kind of high efficiency solid-liquid Catalysis experiments dress of twin-stage stirring
Put, including reactor and agitator and base, the left and right sides of the upper plane of described base is mounted on twice support base, institute
The reactor stated is fixed on the top of support base, and the upper end of the reactor left and right sides is mounted on fixed mount, the inner chamber of fixed mount
Upper wall be mounted on lifting motor, the top of described lifting motor is mounted on screw shell, described screw shell
Inner chamber is mounted on threaded rod, and described threaded rod is mutually chimeric by screw thread with screw shell, and the top of threaded rod is provided with
Upper frame, the left and right ends of described upper frame are supported by threaded rod to be fixed, and the centre position of the upper plane of upper frame is provided with dextrorotation
Motor, the bottom of dextrorotation motor is provided with dextrorotation rotating shaft, and the centre position of described upper frame is provided with dextrorotation axle bearing, it is described just
Rotary shaft is spacing in dextrorotation axle bearing, and the bottom of dextrorotation rotating shaft is connected with electric lifting rod, and the bottom of electric lifting rod is installed
There is puddle support, described puddle support is in " returning " font, and the upper Plane Installation of the inner chamber of puddle support has catalysis box, the bottom of the upper frame
Plane Installation has connecting rod, and described connecting rod is provided with twice and respectively positioned at the left and right sides of electric lifting rod, connecting rod
Bottom top cover is installed, the centre position of described base is provided with derotation motor, and the top of derotation motor is provided with derotation
Motor shaft, the top of derotation motor shaft is connected with shaft coupling, and one end of described shaft coupling is connected with derotation motor shaft, shaft coupling
The other end be connected with derotation power transmission shaft, the centre position of the bottom of reactor is provided with derotation axle bearing, described derotation transmission
Axle is spacing in derotation axle bearing, and the bottom of derotation power transmission shaft is provided with driving turntable, described derotation axle bearing with reaction
Sealing gasket is provided between the baseplane of kettle inner chamber, described agitator is located at the inside of reactor, and the bottom of agitator is seated in
The upper plane of driving turntable, the left and right sides of agitator is provided with slide bar, and the left and right sides of reactor is provided with corresponding with slide bar
Chute, the outer end of described slide bar is mounted on fixed block, and the inside of fixed block is provided with rotating shaft, and the left and right sides of fixed block is equal
Provided with pulley, the slide rail corresponding with pulley is equipped with chute, in described pulley chimeric slide rail, described agitator
If outer wall be provided with arterial highway permeable hole, the left side of described reactor is provided with liquid-in pipe, and the right side of reactor is provided with drain pipe.
It is used as further scheme of the invention：Valve is equipped with described liquid-in pipe and drain pipe.
It is used as further scheme of the invention：The inside of described catalysis box is equipped with catalyst.
It is used as further scheme of the invention：If the outer surface of described catalysis box is provided with arterial highway liquid-leadage hole.
It is used as further scheme of the invention：The centre position of described top cover is provided with through hole, described electric lifting rod
With top cover without space interference.
It is used as further scheme of the invention：Described lifting motor, dextrorotation motor, derotation motor and electric expansion bar are equal
It is electrically connected with switch controller.
It is used as further scheme of the invention：Described top cover is provided with covering piece.
Compared with prior art, the beneficial effects of the invention are as follows：The agitating mode reversely rotated using twin-stage, is aided with and urged
Agent, which is acted on, causes reaction speed faster, more thoroughly, meets that chemical engineering experiment is quick, efficient, accurate requirement of experiment；While energy
Solid, liquid reactants and catalyst are enough efficiently separated, the time that the arrangement of experiment is dealt with problems arising from an accident has been saved；Whole equipment takes
Space is small, and equipment connection is simple to be easy to place in laboratory；It is also convenient for daily cleaning maintenance work simultaneously.
Brief description of the drawings
Fig. 1 is structural representation of the invention.
Fig. 2 is top view of the invention.
Fig. 3 is the attachment structure schematic diagram of slide bar and chute in the present invention.
Fig. 4 is the structural representation of agitator in the present invention.
In figure：1- reactors, 2- agitators, 3- support bases, 4- bases, 5- upper frames, 6- fixed mounts, 7- lifting motors, 8-
Screw shell, 9- threaded rods, 10- connecting rods, 11- top covers, 12- covering pieces, 13- dextrorotations motor, 14- dextrorotations rotating shaft, 15- are just
Spin axis bearing, 16- electric lifting rods, 17- puddle supports, 18- catalysis box, 19- slide bars, 20- chutes, 21- derotations motor, 22- are anti-
Rotation motor shaft, 23- shaft couplings, 24- derotations power transmission shaft, 25- derotations axle bearing, 26- sealing gaskets, 27- driving turntables, 28- are fixed
Block.29- pulleys, 30- rotating shafts, 31- slide rails, 32- permeable holes, 33- liquid-in pipes, 34- drain pipes.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
Refer in Fig. 1~4, the embodiment of the present invention, a kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring, including it is anti-
Answer kettle 1 and agitator 2 and base 4, the left and right sides of the upper plane of described base 4 is mounted on twice support base 3, described
Reactor 1 is fixed on the top of support base 3, and the upper end of the left and right sides of reactor 1 is mounted on fixed mount 6, the inner chamber of fixed mount 6
Upper wall be mounted on lifting motor 7, the top of described lifting motor 7 is mounted on screw shell 8, described screw shell
8 inner chamber is mounted on threaded rod 9, and described threaded rod 9 is mutually chimeric by screw thread with screw shell 8, the top of threaded rod 9
Upper frame 5 is installed, the left and right ends of described upper frame 5 are supported by threaded rod 9 to be fixed, the centre position of the upper plane of upper frame 5
Dextrorotation motor 13 is installed, the bottom of dextrorotation motor 13 is provided with dextrorotation rotating shaft 14, and the centre position of described upper frame 5 is provided with just
Spin axis bearing 15, described dextrorotation rotating shaft 14 is spacing in dextrorotation axle bearing 15, and the bottom of dextrorotation rotating shaft 14 is connected with electronic liter
Bar 16 drops, the bottom of electric lifting rod 16 is provided with puddle support 17, described puddle support 17 is in " returning " font, puddle support 17 it is interior
The upper Plane Installation of chamber has catalysis box 15, and the baseplane of the upper frame 5 is provided with connecting rod 10, and described connecting rod 10 is provided with two
Road and the left and right sides for being located at electric lifting rod 16 respectively, the bottom of connecting rod 10 are provided with top cover 11, described base 4
Centre position is provided with derotation motor 21, and the top of derotation motor 21 is provided with derotation motor shaft 22, the top of derotation motor shaft 22
End is connected with shaft coupling 23, and one end of described shaft coupling 23 is connected with derotation motor shaft 22, the other end connection of shaft coupling 23
There is derotation power transmission shaft 24, the centre position of the bottom of reactor 1 is provided with derotation axle bearing 25, and described derotation power transmission shaft 24 is spacing
In derotation axle bearing 25, the bottom of derotation power transmission shaft 24 is provided with driving turntable 27, described derotation axle bearing 25 and reaction
Sealing gasket 26 is provided between the baseplane of the inner chamber of kettle 1, described agitator 2 is located at the inside of reactor 1, the bottom of agitator 2
The upper plane of driving turntable 27 is seated in, the left and right sides of agitator 2 is provided with slide bar 19, and the left and right sides of reactor 1 is provided with
The chute 20 corresponding with slide bar 19, the outer end of described slide bar 19 is mounted on fixed block 28, and the inside of fixed block 28 is provided with
Rotating shaft 30, the left and right sides of fixed block 28, which is equipped with pulley 29, chute 20, is equipped with the slide rail 31 corresponding with pulley 29, institute
In the pulley 29 stated chimeric slide rail 31, if the outer wall of described agitator 2 is provided with arterial highway permeable hole 32, described reactor
1 left side is provided with liquid-in pipe 33, and the right side of reactor 1 is provided with drain pipe 34.
The present invention operation principle be：During experiment, catalysts are put into catalysis box 15, solid-state reactants are put into
In agitator 2, controller is opened, lifting motor 7 is opened, lifting motor 7 drives screw shell 8 to rotate forward, and threaded rod 9 declines, and enters
And the entire lowering of upper frame 5, closure agitator 2 and reactor 1 after top cover 11 declines, reaction liquid is put into from liquid-in pipe 33, is stirred
If the outer wall of bucket 2 is provided with arterial highway permeable hole 32, liquid is filled in agitator 2, and dextrorotation motor 13, dextrorotation are opened by controller
Motor 13 drives dextrorotation rotating shaft 14 to rotate, and the driving electric expansion link 16 of dextrorotation rotating shaft 14 rotates, and then drives puddle support 17 to rotate,
Derotation motor 21 is opened by controller again, derotation motor 21 drives derotation motor shaft 22 to rotate, and derotation motor shaft 22 passes through connection
Axle device 23 and then drive derotation power transmission shaft 24, derotation power transmission shaft 24 drive driving turntable 27, and driving turntable 27 drives agitator 2 to revolve
Turn, with puddle support 17 reversely, shaft coupling 23 has buffering, vibration damping and the effect for improving shafting dynamic property for direction of rotation；It is two-way
In the presence of stirring measure and again catalyst, react more efficient, more thoroughly；After completion of the reaction, lifting motor 7 drives spiral shell
Line sleeve 8 is inverted, and threaded rod 9 rises, and drives whole upper frame 5 to rise, electric expansion bar 16 is shunk, puddle support is risen, is carried
Product liquid up on agitator 2 after planar reaction discharges collection at drain pipe 34, and reacted solid state crystallization product is protected
Stay in agitator 2, agitator is tilted and collection obtains solid state crystallization product；Catalysis box is removed, internal catalyst is protected
Hold constant, follow-up chemical engineering experiment can be preserved for.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as to the claim involved by limitation.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It may be appreciated other embodiment.
Claims (7)
1. a kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring, including reactor (1) and agitator (2) and base (4), its
It is characterised by, the left and right sides of the upper plane of described base (4) is mounted on twice support base (3), described reactor (1)
Be fixed on the top of support base (3), the upper end of reactor (1) left and right sides is mounted on fixed mount (6), fixed mount (6) it is interior
The upper wall of chamber is mounted on lifting motor (7), and the top of described lifting motor (7) is mounted on screw shell (8), described
The inner chamber of screw shell (8) is mounted on threaded rod (9), and described threaded rod (9) is mutually embedding by screw thread with screw shell (8)
Close, the top of threaded rod (9) is provided with upper frame (5), and the left and right ends of described upper frame (5) are supported by threaded rod (9) to be fixed,
The centre position of the upper plane of upper frame (5) is provided with dextrorotation motor (13), and the bottom of dextrorotation motor (13) is provided with dextrorotation rotating shaft
(14), the centre position of described upper frame (5) is provided with dextrorotation axle bearing (15), and described dextrorotation rotating shaft (14) is spacing in positive spin axis
In bearing (15), the bottom of dextrorotation rotating shaft (14) is connected with electric lifting rod (16), and the bottom of electric lifting rod (16) is provided with
Puddle support (17), described puddle support (17) is in " returning " font, and the upper Plane Installation of the inner chamber of puddle support (17) has catalysis box
(15), the baseplane of the upper frame (5) is provided with connecting rod (10), and described connecting rod (10) is provided with twice and is located at respectively
The left and right sides of electric lifting rod (16), the bottom of connecting rod (10) is provided with top cover (11), the interposition of described base (4)
Put and derotation motor (21) is installed, the top of derotation motor (21) is provided with derotation motor shaft (22), derotation motor shaft (22)
Top is connected with shaft coupling (23), and one end of described shaft coupling (23) is connected with derotation motor shaft (22), shaft coupling (23)
The other end is connected with derotation power transmission shaft (24), and the centre position of the bottom of reactor (1) is provided with derotation axle bearing (25), described
Derotation power transmission shaft (24) is spacing, and the bottom of derotation power transmission shaft (24) is provided with driving turntable (27) in derotation axle bearing (25),
Sealing gasket (26), described agitator (2) are provided between described derotation axle bearing (25) and the baseplane of reactor (1) inner chamber
Inside positioned at reactor (1), the bottom of agitator (2) is seated in the upper plane of driving turntable (27), the left and right of agitator (2)
Both sides are provided with slide bar (19), and the left and right sides of reactor (1) is provided with the chute (20) corresponding with slide bar (19), described cunning
The outer end of bar (19) is mounted on fixed block (28), and the inside of fixed block (28) is provided with rotating shaft (30), the left and right of fixed block (28)
Both sides are equipped with pulley (29), chute (20) and are equipped with the slide rail (31) corresponding with pulley (29), described pulley (29)
In chimeric slide rail (31), described agitator (2) if outer wall be provided with arterial highway permeable hole (32), described reactor (1)
Left side be provided with liquid-in pipe (33), the right side of reactor (1) is provided with drain pipe (34).
2. the high efficiency solid-liquid Catalysis experiments device of twin-stage stirring according to claim 1, it is characterised in that described enters liquid
Valve is equipped with pipe (33) and drain pipe (34).
3. the high efficiency solid-liquid Catalysis experiments device of twin-stage stirring according to claim 1, it is characterised in that described catalysis
The inside of box (15) is equipped with catalyst.
4. the high efficiency solid-liquid Catalysis experiments device of twin-stage stirring according to claim 1, it is characterised in that described catalysis
Box (15) if outer surface be provided with arterial highway liquid-leadage hole.
5. the high efficiency solid-liquid Catalysis experiments device of twin-stage stirring according to claim 1, it is characterised in that described top cover
(11) centre position is provided with through hole, and described electric lifting rod (16) and top cover (11) are without space interference.
6. the high efficiency solid-liquid Catalysis experiments device of twin-stage stirring according to claim 1, it is characterised in that described lifting
Motor (7), dextrorotation motor (13), derotation motor (21) are electrically connected with electric expansion bar (16) with switch controller.
7. the high efficiency solid-liquid Catalysis experiments device of twin-stage stirring according to claim 1, it is characterised in that described top cover
(11) it is provided with covering piece (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710498804.2A CN107096473A (en) | 2017-06-27 | 2017-06-27 | A kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710498804.2A CN107096473A (en) | 2017-06-27 | 2017-06-27 | A kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring |
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| Publication Number | Publication Date |
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| CN107096473A true CN107096473A (en) | 2017-08-29 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710498804.2A Withdrawn CN107096473A (en) | 2017-06-27 | 2017-06-27 | A kind of high efficiency solid-liquid Catalysis experiments device of twin-stage stirring |
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| CN (1) | CN107096473A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107930485A (en) * | 2017-12-20 | 2018-04-20 | 无锡市飞天油脂有限公司 | A kind of efficient stable agitating device of lubricating oil processing |
| CN108358291A (en) * | 2018-05-04 | 2018-08-03 | 黄山科太环保科技有限公司 | A kind of catalyst carrier new material equipment |
| CN108579652A (en) * | 2018-05-18 | 2018-09-28 | 青海聚之源新材料有限公司 | A kind of intelligence hexafluoro squama acid lithium preparation reaction kettle and its control method |
| CN109078538A (en) * | 2018-08-28 | 2018-12-25 | 扬中市惠丰包装有限公司 | A kind of carton production molding raw material proportioning device |
| CN112604633A (en) * | 2020-12-26 | 2021-04-06 | 江苏阿科米科技有限公司 | Automatic reciprocating type stirring and mixing reactor |
| CN112973583A (en) * | 2021-05-20 | 2021-06-18 | 山东胜星新能源有限公司 | Recovery device for catalytic cracking catalyst fine powder |
| CN113019292A (en) * | 2021-03-30 | 2021-06-25 | 河南应用技术职业学院 | Green energy-saving medicine production uses high-efficient reation kettle |
| CN114480105A (en) * | 2022-02-14 | 2022-05-13 | 苗新宇 | Microbial fermentation tank auxiliary inoculation sterilization cover |
-
2017
- 2017-06-27 CN CN201710498804.2A patent/CN107096473A/en not_active Withdrawn
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107930485A (en) * | 2017-12-20 | 2018-04-20 | 无锡市飞天油脂有限公司 | A kind of efficient stable agitating device of lubricating oil processing |
| CN108358291A (en) * | 2018-05-04 | 2018-08-03 | 黄山科太环保科技有限公司 | A kind of catalyst carrier new material equipment |
| CN108579652A (en) * | 2018-05-18 | 2018-09-28 | 青海聚之源新材料有限公司 | A kind of intelligence hexafluoro squama acid lithium preparation reaction kettle and its control method |
| CN109078538A (en) * | 2018-08-28 | 2018-12-25 | 扬中市惠丰包装有限公司 | A kind of carton production molding raw material proportioning device |
| CN112604633A (en) * | 2020-12-26 | 2021-04-06 | 江苏阿科米科技有限公司 | Automatic reciprocating type stirring and mixing reactor |
| CN113019292A (en) * | 2021-03-30 | 2021-06-25 | 河南应用技术职业学院 | Green energy-saving medicine production uses high-efficient reation kettle |
| CN112973583A (en) * | 2021-05-20 | 2021-06-18 | 山东胜星新能源有限公司 | Recovery device for catalytic cracking catalyst fine powder |
| CN114480105A (en) * | 2022-02-14 | 2022-05-13 | 苗新宇 | Microbial fermentation tank auxiliary inoculation sterilization cover |
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Application publication date: 20170829 |