CN202741413U - Mercury removing device of mercury-containing rock core - Google Patents

Mercury removing device of mercury-containing rock core Download PDF

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Publication number
CN202741413U
CN202741413U CN 201220300250 CN201220300250U CN202741413U CN 202741413 U CN202741413 U CN 202741413U CN 201220300250 CN201220300250 CN 201220300250 CN 201220300250 U CN201220300250 U CN 201220300250U CN 202741413 U CN202741413 U CN 202741413U
Authority
CN
China
Prior art keywords
mercury
condenser
rock core
pipe
quartz ampoule
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 201220300250
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Chinese (zh)
Inventor
刘涛
葛维
李新功
杨雪梅
赵增义
吕道平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Natural Gas Co Ltd
Original Assignee
China Petroleum and Natural Gas Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Natural Gas Co Ltd filed Critical China Petroleum and Natural Gas Co Ltd
Priority to CN 201220300250 priority Critical patent/CN202741413U/en
Application granted granted Critical
Publication of CN202741413U publication Critical patent/CN202741413U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model provides a mercury removing device of a mercury-containing rock core, which is applied to mercury removing treatment of an oil field laboratory rock core. The mercury removing device is characterized in that a quartz tube is arranged in a tubular heating furnace; the mercury-containing rock core is placed in the quartz tube; the quartz tube is circular and one end of the quartz tube is provided with an opening; the opening end of the quartz tube is connected with a rubber pipe; the other end of the rubber pipe is connected with an air inlet of the middle part of a condenser; a condensed water inlet pipe of the condenser is connected with a tap water pipe; a water outlet pipe of the condenser is communicated with a sewer by using the rubber pipe; a collection bottle is connected with a collection opening at the lower end of the condenser; an upper end air outlet of the condenser is connected with a second rubber pipe; and the other end of the second rubber pipe is connected with an air inlet of a circulating water type vacuum pump. The mercury removing device has the effects that the mercury-free treatment of the mercury-containing rock core is realized; and the treated rock core can be treated as a normal rock core and the collected mercury is reutilized.

Description

The mercury removal device of mercurous rock core
Technical field
The utility model relates to oil field laboratory equipment technical field, and particularly a kind of rock core treating apparatus is a kind of mercury removal device of mercurous rock core.
Background technology
At present, be the core of microphysics research in the research mesopore of reservoir of oil and gas structure, the topmost method of study of rocks pore structure is to determine the quantitative performance of pore constriction with the method for measuring capillary pressure.What the method for mensuration rock capillary pressure curve was a lot of but the most frequently used mainly contains three kinds: semi-permeable plate method, mercury injection method and centrifugal process.
To pressing the mercurous rock core after the mercury experiment not do any processing, be direct sealed in storehouse, the mercury in the rock core also can evaporate gradually the formation mercury vapour and causes mercury pollution like this.
The utility model content
The purpose of this utility model is: a kind of mercury removal device of mercurous rock core is provided, can presses the mercuryless processing of the mercurous rock core behind the mercury, can reduce mercury emissions, avoid mercury pollution.
The technical solution adopted in the utility model is: the mercury removal device of mercurous rock core, comprise tubular heater, condenser, circulating water type vavuum pump, receiving flask and quartz ampoule, and it is characterized in that: in tubular heater, be placed with quartz ampoule; Be placed with mercurous rock core in the quartz ampoule, quartz ampoule is a circular end opening, and the quartz ampoule openend is connected with rubber tube; The other end of rubber tube connects the air inlet at the middle part of condenser; The condensed water water inlet pipe of condenser is connected with running water pipe, and the outlet pipe of condenser is communicated to sewer with rubber tube; The collection mouth of receiving flask and condenser lower end joins; The gas outlet, upper end of condenser connects the second rubber tube, and the other end of the second hose connects the air inlet of circulating water type vavuum pump.
Sketch the use procedure of the mercury removal device of mercurous rock core.Consult Fig. 1.A plurality of cylindrical mercurous rock cores 9 are put into quartz ampoule 8 successively, again quartz ampoule 8 is put into tubular heater 1, the openend of quartz ampoule 8 extends to outside the tubular heater 1.And quartz ampoule 8 parts that extend to tubular heater 1 outer end do not comprise mercurous rock core.
Then link to each other with the first rubber tube 7 between quartz ampoule 8 openends and condenser 2 air inlets, the condensed water water inlet pipe 5 of condenser 2 and running water pipe with rubber tube be connected, condenser outlet pipe 6 usefulness rubber tubes pass to sewer, condenser 2 is vertically placed, the gas outlet of condenser 2 is upper, the collection mouth of condenser 2 below.Receiving flask 4 joins with the collection mouth of condenser 2; The gas outlet of condenser 2 is connected with the second rubber tube with circulating water type vavuum pump 3 air inlets.
Connect the running water switch of opening the condensed water water inlet pipe 5 of condenser 2 after finishing, ON cycle ability of swimming vavuum pump 3, set the temperature spot (boiling point that is higher than mercury: 629.88K (356.73 ℃)) of tubular heater 1, the switch of opening tubular heater 1 heats.
Liquid mercury under the effect of heat energy and vacuum in the rock core gasifies gradually, mercury is evaporated from the rock core body, the mercury vapour that constantly evaporates advances people's condenser 2 under the effect of vacuum, because the fusing point of mercury is 234.32K (38.83 ℃), so mercury is condensed into liquid mercury in condenser 2, liquid mercury flows into a receiving flask 4 along condenser 2 inwalls through collecting mouth under Action of Gravity Field.If mercury vapour is not condensed fully, nubbin with circulating water type vavuum pump 3 in the water contact process in again the water that is recycled in the ability of swimming vavuum pump 3 of condensation absorb, so because the water in the circulating water type vavuum pump 3 is can not polluting of sealing.
Through stopped heating behind the certain hour, close circulating water type vavuum pump 3, after naturally cooling to room temperature, tubular heater 1 closes running water switch, take off the rubber tube 7 of quartz ampoule 8 openends, the rock core in the quartz ampoule 8 is taken out.
The beneficial effects of the utility model: the mercury removal device of the mercurous rock core of the utility model,
Description of drawings
Fig. 1 is the mercury removal device structural profile schematic diagram of the mercurous rock core of the utility model.
Among the figure, 1-tubular heater, 2-condenser, 3-circulating water type vavuum pump, 4-receiving flask, 5-water inlet pipe, 6-outlet pipe, 7-rubber tube, 8-quartz ampoule.
The specific embodiment
Embodiment 1: take the mercury removal device of a mercurous rock core as example, the utility model is described in further detail.
Consult Fig. 1.The mercury removal device of the mercurous rock core of the utility model comprises tubular heater 1, condenser 2, circulating water type vavuum pump 3, receiving flask 4 and quartz ampoule 8.
In tubular heater 1, be placed with quartz ampoule 8; Be placed with mercurous rock core 9 in the quartz ampoule 8, quartz ampoule 8 is the round tube of internal diameter 120mm, quartz ampoule 8 one end openings, and quartz ampoule 8 openends are connected with rubber tube 7.The other end of rubber tube 7 connects the air inlet at the middle part of condenser 2.The condensed water water inlet pipe 5 of condenser 2 is connected with running water pipe, and the outlet pipe 6 usefulness rubber tubes of condenser 2 are communicated to sewer.The receiving flask 4 of Crystal city joins with the collection mouth of condenser 2 lower ends.The gas outlet, upper end of condenser 2 connects the second rubber tube, and the other end of the second hose connects the air inlet of circulating water type vavuum pump 3.

Claims (1)

1. the mercury removal device of a mercurous rock core, comprise tubular heater (1), condenser (2), circulating water type vavuum pump (3), receiving flask (4) and quartz ampoule (8), it is characterized in that: in tubular heater (1), be placed with quartz ampoule (8); Be placed with mercurous rock core (9) in the quartz ampoule (8), quartz ampoule (8) is a circular end opening, and quartz ampoule (8) openend is connected with rubber tube (7); The other end of rubber tube (7) connects the air inlet at the middle part of condenser (2); The condensed water water inlet pipe (5) of condenser (2) is connected with running water pipe, and the outlet pipe (6) of condenser (2) is communicated to sewer with rubber tube; Receiving flask (4) joins with the collection mouth of condenser (2) lower end; The gas outlet, upper end of condenser (2) connects the second rubber tube, and the other end of the second hose connects the air inlet of circulating water type vavuum pump (3).
CN 201220300250 2012-06-21 2012-06-21 Mercury removing device of mercury-containing rock core Expired - Lifetime CN202741413U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220300250 CN202741413U (en) 2012-06-21 2012-06-21 Mercury removing device of mercury-containing rock core

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220300250 CN202741413U (en) 2012-06-21 2012-06-21 Mercury removing device of mercury-containing rock core

Publications (1)

Publication Number Publication Date
CN202741413U true CN202741413U (en) 2013-02-20

Family

ID=47700861

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220300250 Expired - Lifetime CN202741413U (en) 2012-06-21 2012-06-21 Mercury removing device of mercury-containing rock core

Country Status (1)

Country Link
CN (1) CN202741413U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103418597A (en) * 2013-06-03 2013-12-04 北京博朗德科技有限公司 System for treating mercury-containing rock core
CN109132275A (en) * 2018-09-07 2019-01-04 丁柳朋 A kind of equipment of recycling used batteries convenient for discharge
CN111857030A (en) * 2020-07-23 2020-10-30 中洁环淼(江苏)环境科技有限公司 Mercury-pressing rock core intelligent environment-friendly processing device

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103418597A (en) * 2013-06-03 2013-12-04 北京博朗德科技有限公司 System for treating mercury-containing rock core
CN103418597B (en) * 2013-06-03 2015-08-12 北京博朗德科技有限公司 A kind of system processing mercurous core
CN109132275A (en) * 2018-09-07 2019-01-04 丁柳朋 A kind of equipment of recycling used batteries convenient for discharge
CN109132275B (en) * 2018-09-07 2021-07-16 丁柳朋 Waste battery recovery equipment convenient for discharging
CN111857030A (en) * 2020-07-23 2020-10-30 中洁环淼(江苏)环境科技有限公司 Mercury-pressing rock core intelligent environment-friendly processing device

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Granted publication date: 20130220

CX01 Expiry of patent term