CN205287661U - Trace liquid distillation plant - Google Patents
Trace liquid distillation plant Download PDFInfo
- Publication number
- CN205287661U CN205287661U CN201521104830.5U CN201521104830U CN205287661U CN 205287661 U CN205287661 U CN 205287661U CN 201521104830 U CN201521104830 U CN 201521104830U CN 205287661 U CN205287661 U CN 205287661U
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- CN
- China
- Prior art keywords
- receiving flask
- tube
- negative pressure
- alembic
- retort
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Abstract
The utility model discloses a trace liquid distillation plant belongs to distillation plant technical field, including heating jacket, electron temperature -controlled instrument, condenser pipe, distilland receiving flask, vacuum device and retort, its characterized in that: the heating jacket pass through electric wire and electron temperature -controlled instrument and link to each other, the upper portion of heating jacket is equipped with the retort, the retort parts on the right side from the left hand and do not is equipped with inlet, safe mouthful and gas outlet, the retort passes through the catheter and links to each other with the distilland receiving flask with the condenser pipe in proper order, it is continuous with vacuum device that the distilland receiving flask passes through the negative pressure suction tube, the utility model discloses simple structure, convenient operation connects the effect of rubber tube in order to reach the equilibrium air pressure bursting tube at the bursting tube end, can prevent that atmospheric pressure from changing when violent that the bursting tube is rush out to a small amount of liquid simultaneously and the incident that arouses. In addition, the speed of distillate can be accelerated through vacuum device, distillation efficiency is improved.
Description
Technical field
This utility model relates to distilling apparatus technical field, is specially a kind of microdistillation apparatus.
Background technology
At present, the device used by a lot of distillation tests is loaded down with trivial details, takes up room big, inconvenient operation, it is impossible to efficiently micro liquid is distilled, and can there is bursting tube liquid malfunctioning, to be distilled in practical operation and add the problems such as inconvenient.
Utility model content
The purpose of this utility model is in that to provide a kind of microdistillation apparatus, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, this utility model provides following technical scheme: a kind of microdistillation apparatus, including adding hot jacket, electronic temperature controller, condensing tube, distillate receiving flask, negative pressure device and alembic, the described hot jacket that adds is connected with electronic temperature controller by electric wire, the top adding hot jacket is provided with alembic, alembic is respectively equipped with inlet, safe mouth and gas outlet from left to right, alembic is connected with condensing tube and distillate receiving flask successively by catheter, and distillate receiving flask is connected with negative pressure device by negative pressure-pumping pipe.
Preferably, the top of described inlet is provided with valve and syringe.
Preferably, described in add hot jacket for cylindrical shape, its inner surface is uniformly distributed heating wire.
Preferably, being provided with intelligent control chip inside described electronic temperature controller, its surface is provided with LCDs.
Preferably, described safe mouth is provided with the bursting tube that can turn on the external world, and the outer end of bursting tube is connected with rubber safety conduit.
Preferably, the lower right of described condensing tube is provided with cooling water inlet, and upper left side is provided with coolant outlet.
Preferably, the bottle stopper of described distillate receiving flask is provided with two through holes, is connected with catheter and negative pressure-pumping pipe respectively.
Compared with prior art, the beneficial effects of the utility model are: simple in construction, easy to operate, connect a rubber tube to reach the effect of equilibrium air pressure bursting tube at bursting tube end, when being possible to prevent air pressure change violent, a small amount of liquid goes out bursting tube and the security incident that causes simultaneously. It addition, the speed of distillate can be accelerated by negative pressure device, improve distillation efficiency.
Accompanying drawing explanation
Fig. 1 is this utility model structural representation.
In figure: 1, syringe; 2, valve; 3, inlet; 4, hot jacket is added; 5, electronic temperature controller; 6, display screen; 7, safe mouth; 8, bursting tube; 9, gas outlet; 10, condensing tube; 11, cooling water inlet; 12, distillate receiving flask; 13, negative pressure device; 14, negative pressure-pumping pipe; 15, catheter; 16, coolant outlet; 17, rubber safety conduit; 18, alembic.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is clearly and completely described, it is clear that described embodiment is only a part of embodiment of this utility model, rather than whole embodiments. Based on the embodiment in this utility model, the every other embodiment that those of ordinary skill in the art obtain under not making creative work premise, broadly fall into the scope of this utility model protection.
Refer to Fig. 1, this utility model provides a kind of technical scheme: a kind of microdistillation apparatus, including adding hot jacket 4, electronic temperature controller 5, condensing tube 10, distillate receiving flask 12, negative pressure device 13 and alembic 18, the described hot jacket 4 that adds is connected with electronic temperature controller 5 by electric wire, the top adding hot jacket 4 is provided with alembic 18, alembic 18 is respectively equipped with inlet 3 from left to right, safe mouth 7 and gas outlet 9, alembic 18 is connected with condensing tube 10 and distillate receiving flask 12 successively by catheter 15, distillate receiving flask 12 is connected with negative pressure device 13 by negative pressure-pumping pipe 14, the top of described inlet 3 is provided with valve 2 and syringe 1, the described hot jacket 4 that adds is for cylindrical shape, its inner surface is uniformly distributed heating wire, described electronic temperature controller 5 is internal is provided with intelligent control chip, its surface is provided with LCDs 6, described safe mouth 7 is provided with the bursting tube 8 that can turn on the external world, the outer end of bursting tube 8 is connected with rubber safety conduit 17, the lower right of described condensing tube 10 is provided with cooling water inlet 11, upper left side is provided with coolant outlet 16, the bottle stopper of described distillate receiving flask 12 is provided with two through holes, it is connected with catheter 15 and negative pressure-pumping pipe 14 respectively.
Operation principle: micro liquid to be distilled is entered alembic 18 by syringe 1 by inlet 3, the heating-up temperature adding hot jacket 4 is controlled by electronic temperature controller 5, gas after heating enters condensing tube 10 by gas outlet 9, liquid after cooling enters distillate receiving flask 12 from catheter 15, the end of bursting tube 8 connects a root rubber safety catheter 17 to reach the effect of equilibrium air pressure bursting tube, and when being possible to prevent air pressure change violent, a small amount of liquid goes out bursting tube and the security incident that causes simultaneously. It addition, the speed of distillate can be accelerated by negative pressure device 13, improve distillation efficiency.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art, being appreciated that when without departing from principle of the present utility model and spirit and these embodiments can be carried out multiple change, amendment, replacement and modification, scope of the present utility model is defined by the appended claims and the equivalents thereof.
Claims (7)
1. a microdistillation apparatus, including adding hot jacket (4), electronic temperature controller (5), condensing tube (10), distillate receiving flask (12), negative pressure device (13) and alembic (18), it is characterized in that: the described hot jacket (4) that adds is connected with electronic temperature controller (5) by electric wire, the top adding hot jacket (4) is provided with alembic (18), alembic (18) is respectively equipped with inlet (3) from left to right, safe mouth (7) and gas outlet (9), alembic (18) is connected with condensing tube (10) and distillate receiving flask (12) successively by catheter (15), distillate receiving flask (12) is connected with negative pressure device (13) by negative pressure-pumping pipe (14).
2. a kind of microdistillation apparatus according to claim 1, it is characterised in that: the top of described inlet (3) is provided with valve (2) and syringe (1).
3. a kind of microdistillation apparatus according to claim 1, it is characterised in that: described in add hot jacket (4) for cylindrical shape, its inner surface is uniformly distributed heating wire.
4. a kind of microdistillation apparatus according to claim 1, it is characterised in that: described electronic temperature controller (5) is internal is provided with intelligent control chip, and electronic temperature controller (5) surface is provided with LCDs (6).
5. a kind of microdistillation apparatus according to claim 1, it is characterised in that: described safe mouth (7) is provided with the bursting tube (8) that can turn on the external world, and the outer end of bursting tube (8) is connected with rubber safety conduit (17).
6. a kind of microdistillation apparatus according to claim 1, it is characterised in that: the lower right of described condensing tube (10) is provided with cooling water inlet (11), and upper left side is provided with coolant outlet (16).
7. a kind of microdistillation apparatus according to claim 1, it is characterised in that: the bottle stopper of described distillate receiving flask (12) is provided with two through holes, is connected with catheter (15) and negative pressure-pumping pipe (14) respectively.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201521104830.5U CN205287661U (en) | 2015-12-24 | 2015-12-24 | Trace liquid distillation plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201521104830.5U CN205287661U (en) | 2015-12-24 | 2015-12-24 | Trace liquid distillation plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205287661U true CN205287661U (en) | 2016-06-08 |
Family
ID=56472878
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201521104830.5U Expired - Fee Related CN205287661U (en) | 2015-12-24 | 2015-12-24 | Trace liquid distillation plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205287661U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107320993A (en) * | 2017-08-28 | 2017-11-07 | 贾海亮 | A kind of distilling apparatus of β methyl naphthalenes |
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
-
2015
- 2015-12-24 CN CN201521104830.5U patent/CN205287661U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107320993A (en) * | 2017-08-28 | 2017-11-07 | 贾海亮 | A kind of distilling apparatus of β methyl naphthalenes |
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160608 Termination date: 20161224 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |