CN202237361U - Ultrasonic crystallization device used for crystallizing and purifying natural products or chemical drugs - Google Patents
Ultrasonic crystallization device used for crystallizing and purifying natural products or chemical drugs Download PDFInfo
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- CN202237361U CN202237361U CN2011204022868U CN201120402286U CN202237361U CN 202237361 U CN202237361 U CN 202237361U CN 2011204022868 U CN2011204022868 U CN 2011204022868U CN 201120402286 U CN201120402286 U CN 201120402286U CN 202237361 U CN202237361 U CN 202237361U
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Abstract
The utility model discloses an ultrasonic crystallization device used for crystallizing and purifying natural products or chemical drugs. The ultrasonic crystallization device comprises a crystallization chamber, an ultrasonic transducer, a temperature probe, a turbidity probe, a stirring device and a master control system, wherein the crystallization chamber has an interlayer structure, the upper part of the crystallization chamber is provided with an inlet, and the lower end of the crystallization chamber is provided with an outlet; the ultrasonic transducer is positioned on the outer wall of a circulating pipeline; and the temperature probe and the turbidity probe are arranged in the crystallization chamber and transmit electric signals of the crystallization chamber to the master control system. Ultrasound is utilized for reinforcing stimulus on crystallization and nucleation, and the crystallization growth rate is improved, so that the crystallization period can be shortened and the production efficiency can be improved; and the grain size of the crystal is uniformly distributed, so that the product quality is improved, and the ultrasonic crystallization device has the advantages of being time-saving, efficient, high in product quality, controllable in the whole process, industrialized in production and the like.
Description
Technical field
The utility model relates to a kind of equipment that is used for natural products or chemicals crystallization purifying, relates in particular to a kind of ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying.
Background technology
Ultrasonic wave is meant the sound wave of frequency more than 20KHz, and it can not cause people's the sense of hearing, is the communication processes of a kind of mechanical oscillation in medium, has characteristics such as pack, orientation, reflection, transmission.As a kind of physical energy form, ultrasonic wave has been widely used in aspects such as natural product extraction, chemistry and chemical industry, environmental protection, food industry, bioengineering.
The solution crystallization process is that material is the process of crystalline state from liquid transformation, experience two steps: crystallization nucleation and crystal growth.Crystallization nucleation is the nucleus that in supersaturated solution, generates some; And on the basis of nucleus, grow into crystal, then be crystal growth.
Method for crystallising of the prior art mainly improves the production capacity of equipment through introducing crystal seed and raising solution concentration, but the products obtained therefrom particle diameter differs, inferior quality.
Summary of the invention
The purpose of the utility model provides the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying that a kind of crystallizing cycle is short, crystal particle diameter is evenly distributed, product quality is high.
The purpose of the utility model realizes through following technical scheme:
The utility model is used for the ultrasonic crystallizer of natural products or chemicals crystallization purifying, comprises crystallisation chamber, and the top of said crystallisation chamber is provided with import, and outlet is arranged at the bottom, and import links to each other through the circulation line that is provided with circulating pump with outlet;
The outer wall of said circulation line is provided with ultrasonic transducer, is connected with solution inlet port and taphole on the said circulation line, and said solution inlet port is provided with liquid feeding pump;
Said crystallization chamber is provided with temp probe, turbidity probe tip, agitating device;
The wall of said crystallisation chamber is a sandwich, and interlayer is provided with circulating water intake and circulating water outlet.
Technical scheme by above-mentioned the utility model provides can be found out, the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying that the utility model provides is because the import of crystallisation chamber links to each other through the circulation line that is provided with circulating pump with outlet; The outer wall of circulation line is provided with ultrasonic transducer, is connected with solution inlet port and taphole on the circulation line, and solution inlet port is provided with liquid feeding pump; Crystallization chamber is provided with temp probe, turbidity probe tip, mixer; The wall of crystallisation chamber is a sandwich; Interlayer is provided with circulating water intake and circulating water outlet; Utilize ultrasound-enhanced stimulation crystallization nucleation, improve crystalline growth speed, have that crystallizing cycle is short, crystal particle diameter is evenly distributed, but characteristics such as product quality is high, the controlled suitability for industrialized production of whole process.
Description of drawings
The structural representation of the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying that Fig. 1 provides for the utility model embodiment.
The specific embodiment
To combine accompanying drawing that the utility model embodiment is done to describe in detail further below.
The ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying of the utility model, its preferable specific embodiment is:
Comprise crystallisation chamber, the top of said crystallisation chamber is provided with import, and outlet is arranged at the bottom, and import links to each other through the circulation line that is provided with circulating pump with outlet;
The outer wall of said circulation line is provided with ultrasonic transducer, is connected with solution inlet port and taphole on the said circulation line, and said solution inlet port is provided with liquid feeding pump;
Said crystallization chamber is provided with temp probe, turbidity probe tip, agitating device;
The wall of said crystallisation chamber is a sandwich, and interlayer is provided with circulating water intake and circulating water outlet;
Said recirculated water is used for the crystallization chamber temperature controlling.
Said agitating device comprises motor, puddler and flabellum.
Also comprise turn-key system, said turn-key system comprises ultrasound control unit, temperature control unit, stirring control module, turbidity display unit, power supply indicating member.
Said ultrasonic transducer is the divergence expression ultrasonic transducer.
The ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying of the utility model utilizes ultrasound-enhanced stimulation crystallization nucleation, improves crystalline growth speed.Have that crystallizing cycle is short, crystal particle diameter is evenly distributed, but characteristics such as product quality is high, the controlled suitability for industrialized production of whole process.
The purpose of the utility model provides a kind of ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying, and it is realized through following technical scheme:
In the utility model, ultrasonic transducer is positioned on the outer wall of circulation line, and parameters such as its frequency, power are controlled by turn-key system; Temperature and turbidity probe tip are positioned at crystallizing tank, and its signal of telecommunication is passed to turn-key system; Turn-key system is located in the control rack, comprises unit such as ultrasonic control, temperature control, stirring control and turbidity demonstration, power supply indication; The circulating water intake of crystallisation chamber interlayer can freeze to crystal solution or heats with outlet through recirculated water.
Specific embodiment:
As shown in Figure 1, the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying in the present embodiment comprises: crystallisation chamber 1, ultrasonic transducer 2, temp probe 3, turbidity probe tip 4, mixer 5 and control rack 6 are formed.Crystallisation chamber 1 is a sandwich, and import 7 is arranged at top, and there is outlet 8 lower end, and import links to each other through circulating pump 9, loop 10 with outlet; Solution inlet port 11, crystal solution outlet 12 links to each other with the loop through triple valve 13,14 respectively; Also have liquid feeding pump 15 and filter screen 16 between solution inlet port 11 and the triple valve 13.Also be provided with circulating water intake 17 and circulating water outlet 18 on the crystallisation chamber interlayer.
The above; Be merely the preferable specific embodiment of the utility model; But the protection domain of the utility model is not limited thereto; Any technical staff who is familiar with the present technique field is in the technical scope that the utility model discloses, and the variation that can expect easily or replacement all should be encompassed within the protection domain of the utility model.Therefore, the protection domain of the utility model should be as the criterion with the protection domain of claims.
Claims (4)
1. a ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying is characterized in that, comprise crystallisation chamber, the top of said crystallisation chamber is provided with import, and outlet is arranged at the bottom, and import links to each other through the circulation line that is provided with circulating pump with outlet;
The outer wall of said circulation line is provided with ultrasonic transducer, is connected with solution inlet port and taphole on the said circulation line, and said solution inlet port is provided with liquid feeding pump;
Said crystallization chamber is provided with temp probe, turbidity probe tip, agitating device;
The wall of said crystallisation chamber is a sandwich, and interlayer is provided with circulating water intake and circulating water outlet.
2. the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying according to claim 1 is characterized in that said agitating device comprises motor, puddler and flabellum.
3. the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying according to claim 1 and 2; It is characterized in that; Also comprise turn-key system, said turn-key system comprises ultrasound control unit, temperature control unit, stirring control module, turbidity display unit, power supply indicating member.
4. the ultrasonic crystallizer that is used for natural products or chemicals crystallization purifying according to claim 1 and 2 is characterized in that said ultrasonic transducer is the divergence expression ultrasonic transducer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011204022868U CN202237361U (en) | 2011-10-21 | 2011-10-21 | Ultrasonic crystallization device used for crystallizing and purifying natural products or chemical drugs |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011204022868U CN202237361U (en) | 2011-10-21 | 2011-10-21 | Ultrasonic crystallization device used for crystallizing and purifying natural products or chemical drugs |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202237361U true CN202237361U (en) | 2012-05-30 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011204022868U Expired - Fee Related CN202237361U (en) | 2011-10-21 | 2011-10-21 | Ultrasonic crystallization device used for crystallizing and purifying natural products or chemical drugs |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202237361U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423545A (en) * | 2011-10-21 | 2012-04-25 | 北京弘祥隆生物技术股份有限公司 | Ultrasonic crystallizing equipment used in natural product or chemical agent crystallization and purification |
| CN105457334A (en) * | 2015-12-18 | 2016-04-06 | 辽宁医学院 | Ultrasonic-wave-pipeline-type automatic circulating continuous traditional Chinese medicine extracting device |
-
2011
- 2011-10-21 CN CN2011204022868U patent/CN202237361U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423545A (en) * | 2011-10-21 | 2012-04-25 | 北京弘祥隆生物技术股份有限公司 | Ultrasonic crystallizing equipment used in natural product or chemical agent crystallization and purification |
| CN105457334A (en) * | 2015-12-18 | 2016-04-06 | 辽宁医学院 | Ultrasonic-wave-pipeline-type automatic circulating continuous traditional Chinese medicine extracting device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: LANGFANG HONGXIANGLONG BIOLOGICAL TECHNOLOGY CO., LTD. Assignor: Beijing Hongxianglong Biotechnology Co., Ltd. Contract record no.: 2014990000310 Denomination of utility model: Ultrasonic crystallizing equipment used in natural product or chemical agent crystallization and purification Granted publication date: 20120530 License type: Exclusive License Record date: 20140519 |
|
| LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160205 Address after: 065300 South District of Baihe industrial district, Dachang County, Hebei, Langfang Patentee after: LANGFANG HONGXIANGLONG BIOLOGICAL TECHNOLOGY CO., LTD. Address before: 100085, Ka Wah building, No. 9, 3rd Street, Beijing, Haidian District, B608 Patentee before: Beijing Hongxianglong Biotechnology Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120530 Termination date: 20191021 |