CN201299980Y - Novel volatile oil distiller - Google Patents
Novel volatile oil distiller Download PDFInfo
- Publication number
- CN201299980Y CN201299980Y CNU2008201923593U CN200820192359U CN201299980Y CN 201299980 Y CN201299980 Y CN 201299980Y CN U2008201923593 U CNU2008201923593 U CN U2008201923593U CN 200820192359 U CN200820192359 U CN 200820192359U CN 201299980 Y CN201299980 Y CN 201299980Y
- Authority
- CN
- China
- Prior art keywords
- generator
- water
- volatile oil
- distiller
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000003921 oil Substances 0.000 claims abstract description 20
- 238000004821 distillation Methods 0.000 claims description 33
- 238000010992 reflux Methods 0.000 claims description 5
- 230000008676 import Effects 0.000 claims description 3
- 238000000605 extraction Methods 0.000 abstract description 10
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 description 12
- 238000001256 steam distillation Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 244000178870 Lavandula angustifolia Species 0.000 description 3
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 239000001102 lavandula vera Substances 0.000 description 3
- 235000018219 lavender Nutrition 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 235000005979 Citrus limon Nutrition 0.000 description 2
- 244000131522 Citrus pyriformis Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 244000062730 Melissa officinalis Species 0.000 description 2
- 235000010654 Melissa officinalis Nutrition 0.000 description 2
- 241000220317 Rosa Species 0.000 description 2
- OEYQBKYISMRWQB-UHFFFAOYSA-N Santal Chemical compound C=1C(OC)=CC(O)=C(C2=O)C=1OC=C2C1=CC=C(O)C(O)=C1 OEYQBKYISMRWQB-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000000865 liniment Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000019476 oil-water mixture Nutrition 0.000 description 2
- 240000002262 Litsea cubeba Species 0.000 description 1
- 235000012854 Litsea cubeba Nutrition 0.000 description 1
- 240000000233 Melia azedarach Species 0.000 description 1
- 241000233855 Orchidaceae Species 0.000 description 1
- 240000003731 Piper cubeba Species 0.000 description 1
- 235000002711 Piper cubeba Nutrition 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 239000001771 mentha piperita Substances 0.000 description 1
- 238000005580 one pot reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model relates to a distiller, in particular to a novel volatile oil distiller for extracting different natural herb volatile oil. The distiller comprises a distilling generator with a sieve plate, wherein, the sieve plate divides the distilling generator into an upper layer and a lower layer. The distiller is characterized in that two charging openings are arranged at the top part of the distilling generator; one charging opening is connected with the lower layer of the distilling generator through a charging pipe; a vapor collection pipeline is connected with the top part of the distilling generator; the vapor collection pipeline is connected with the inlet of an oil water separator; the upper end of the oil water separator is connected with a condenser pipe; and the lower end of the oil water separator is connected with a control valve. The distiller has the advantages of simple structure and convenient operation, integrates a distilling device on water and a distilling device in water, is suitable for the extraction of different natural herb volatile oil, can not only meet the requirement of experimental research, but also meet the requirement of large-scale production.
Description
Technical field
The utility model relates to a kind of distiller, particularly a kind of water and steam distillation device and water distillation device is merged, and adapts to the novel volatile oil distiller that different natural herbal volatile oil extract.
Background technology
Extraction volatile oil is pretty troublesome process from natural herbal, because the volatile oil content of plant is considerably less.So, need a large amount of plants just can extract a spot of volatile oil, finally cause just costliness like this of volatile oil.For example: about 3～5 tons roseleaf: extraction 1kg rose volatile oil; The fresh lavender of about 200kg: extraction 1kg lavender volatile oil; About 1 ton of flores aurantii petal: extraction 1kg flores aurantii volatile oil; About 3000 lemons: the 1kg lemon volatile oil of squeezing out; About 6～7 tons of balms: extracting 1kg balm volatile oil, is the medicinal herbs volatile oil of the most difficult extraction.
At present, a lot, the most frequently used, the essential oil extraction method simple to operate, that cost is low of the method for extraction volatile oil is a steam distillation from natural herbal.Steam distillation is produced essential oil and is mainly contained water and steam distillation, water distillation dual mode, is applied to different natural herbals.Water and steam distillation claims the water proof distillation again.This distillation mode is that raw material is placed in the boiler on the sieve plate, the sieve plate bottom position of cooking can hold certain water yield, this water yield must be able to satisfy the required enough saturated vapors of distillation procedure, does not spatter when the water layer height seethes with excitement with water under the sieve plate that the bed of material is a principle on the sieve plate with water.Be applicable to the fruit of a cubeb litsea tree, dried peppermint leaf, lavender etc., agglomerating material can not bond when distillation.Water distillation generally is earlier raw material to be put into boiler, adds clear water or last one pot distillate then.Adding the water height generally is just to soak the bed of material.What have all is provided with sieve plate on the bottom of a pan, directly contact with thermal source to prevent raw material, and what also have is not provided with sieve plate. and strengthen the bottom of a pan, and the Lian Shuihe material is gone out from the bottom of a pan together during discharging.Because raw material steeps all the time in water, distills comparatively even.This distillation mode is suitable for the distillation of fresh flower classes such as white orchid, flores aurantii and rose, also is suitable for the easily distillation of bonding raw material of broken back, as the santal powder etc.At present, for these two kinds of distillation modes, employing be the different devices of two covers.This will rooting according to the heterogeneity of natural herbal, adopt different devices.For lab scale, the dismounting of instrument extremely bothers, and serious potential safety hazard is arranged.For big production, generally need to adopt two covering devices.For the volatile oil that adapts to various natural herbals extracts, invent a kind of novel volatile oil distiller that water and steam distillation device and water distillation device are merged and be highly profitable.
Summary of the invention
The purpose of this utility model is exactly the defective at existing distiller, and a kind of novel volatile oil distiller is provided.It merges water and steam distillation device and water distillation device, adapts to the extraction of different natural herbal volatile oil, and it can satisfy the experimental study needs, can satisfy requirement of massive production again.
The technical solution of the utility model is achieved in that it comprises the distillation generator that sieve plate is housed, sieve plate will distill generator and be divided into upper and lower two-layer, it is characterized in that: the top of distillation generator has two charge doors, one of them charge door communicates by the lower floor of charge pipe with the distillation generator, the top of distillation generator is connected with the vapor collection pipeline, the vapor collection pipeline is connected with the import of oil water separator, the upper end of oil water separator is connected with condenser pipe, and the lower end is connected with by-pass valve control by pipeline.Described vapor collection pipeline is provided with a branch road, and branch road is connected with the pipeline of oil water separator lower end by water circulating reflux pipeline.
During distillation, the water of distillation generator is heated to boiling, and the steam that carries volatile oil is collected through the vapor collection pipeline, rises to condenser pipe.Be dropped in the oil water separator through condensed oil-water mixture, and finish water-oil separating.Volatile oil is positioned at the upper strata, and water level is in lower floor.The water of lower floor flows back to the distillation generator through reflux line, recycles.Oil reservoir left standstill 12 hours, opened by-pass valve control, collected the volatile oil in the oil water separator.
The utlity model has advantage simple in structure, easy to use, it merges water and steam distillation device and water distillation device, adapts to the extraction of different natural herbal volatile oil, and it can satisfy the experimental study needs, can satisfy requirement of massive production again.
Description of drawings
Fig. 1 is a structural representation of the present utility model.
Fig. 2 is the structural representation of the utility model distillation generator top layer.
Fig. 3 is the structural representation of the utility model sieve plate.
The specific embodiment
Below in conjunction with accompanying drawing the utility model is further described:
As shown in Figure 1, the utility model comprises the distillation generator 1 that sieve plate 8 is housed, sieve plate 8 will distill generator and be divided into upper and lower two-layer, the top of distillation generator 1 has two charge door b and c, one of them charge door b communicates by the lower floor of charge pipe 7 with distillation generator 1, the a place, top of distillation generator 1 is connected with vapor collection pipeline 2, vapor collection pipeline 2 is connected with the import of oil water separator 4, the upper end of oil water separator 4 is connected with condenser pipe 3, and the lower end is connected with by-pass valve control 6 by pipeline.Described vapor collection pipeline 2 is provided with a branch road, and branch road is connected with the pipeline of oil water separator lower end by water circulating reflux pipeline 5.
When extracting, adopt the natural herbal of water and steam distillation mode, reinforced by c, material level is on sieve plate 8; Add water by b, water level is between sieve plate 8 and bottom.Adopt the natural herbal of water distillation mode, add water by b, material and water are all between sieve plate 8 and bottom.During the distillation beginning, the water that distills generator 1 is heated to boiling, the steam that carries volatile oil is collected through vapor collection pipeline 2, rises to condenser pipe 3.Be dropped in the oil water separator 4 through condensed oil-water mixture, and finish water-oil separating.Water layer flows back to distillation generator 1 through reflux line 5, recycles.Oil reservoir left standstill 12 hours, opened by-pass valve control 6, collected the volatile oil in the oil water separator 4.
Claims (2)
1, a kind of novel volatile oil distiller, it comprises the distillation generator that sieve plate is housed, sieve plate will distill generator and be divided into upper and lower two-layer, it is characterized in that: the top of distillation generator has two charge doors, one of them charge door communicates by the lower floor of charge pipe with the distillation generator, and the top of distillation generator is connected with the vapor collection pipeline, and the vapor collection pipeline is connected with the import of oil water separator, the upper end of oil water separator is connected with condenser pipe, and the lower end is connected with by-pass valve control by pipeline.
2, novel volatile oil distiller according to claim 1, it is characterized in that: described vapor collection pipeline is provided with a branch road, and branch road is connected with the pipeline of oil water separator lower end by water circulating reflux pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008201923593U CN201299980Y (en) | 2008-11-10 | 2008-11-10 | Novel volatile oil distiller |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008201923593U CN201299980Y (en) | 2008-11-10 | 2008-11-10 | Novel volatile oil distiller |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201299980Y true CN201299980Y (en) | 2009-09-02 |
Family
ID=41083598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008201923593U Expired - Lifetime CN201299980Y (en) | 2008-11-10 | 2008-11-10 | Novel volatile oil distiller |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201299980Y (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103091417A (en) * | 2013-01-15 | 2013-05-08 | 云南烟草科学研究院 | Method for measuring volatile and semi-volatile neutral scent components in tobacco and sample collection device |
| CN101732893B (en) * | 2010-01-18 | 2014-03-05 | 湖南大学 | Continuous oil-water separating and solvent reclaiming device for chemical synthesis or azeotropic rectification |
| CN103877741A (en) * | 2012-12-19 | 2014-06-25 | 江苏飞亚化学工业有限责任公司 | Condensing reflux distributor |
| CN104120035A (en) * | 2014-06-15 | 2014-10-29 | 南京林业大学 | Improved method for extracting volatile oil by steam distillation |
| CN105505581A (en) * | 2016-01-21 | 2016-04-20 | 中山市宏海塑胶科技有限公司 | Household essential oil extractor |
| CN109609282A (en) * | 2019-02-19 | 2019-04-12 | 重庆中烟工业有限责任公司 | Reflow type water and steam distillation extraction element for plants essential oil |
| CN109609281A (en) * | 2019-02-19 | 2019-04-12 | 重庆中烟工业有限责任公司 | Reflow type distilling apparatus for extraction of essential oil |
-
2008
- 2008-11-10 CN CNU2008201923593U patent/CN201299980Y/en not_active Expired - Lifetime
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101732893B (en) * | 2010-01-18 | 2014-03-05 | 湖南大学 | Continuous oil-water separating and solvent reclaiming device for chemical synthesis or azeotropic rectification |
| CN103877741A (en) * | 2012-12-19 | 2014-06-25 | 江苏飞亚化学工业有限责任公司 | Condensing reflux distributor |
| CN103091417A (en) * | 2013-01-15 | 2013-05-08 | 云南烟草科学研究院 | Method for measuring volatile and semi-volatile neutral scent components in tobacco and sample collection device |
| CN103091417B (en) * | 2013-01-15 | 2014-08-27 | 云南烟草科学研究院 | Method for measuring volatile and semi-volatile neutral scent components in tobacco and sample collection device |
| CN104120035A (en) * | 2014-06-15 | 2014-10-29 | 南京林业大学 | Improved method for extracting volatile oil by steam distillation |
| CN105505581A (en) * | 2016-01-21 | 2016-04-20 | 中山市宏海塑胶科技有限公司 | Household essential oil extractor |
| CN109609282A (en) * | 2019-02-19 | 2019-04-12 | 重庆中烟工业有限责任公司 | Reflow type water and steam distillation extraction element for plants essential oil |
| CN109609281A (en) * | 2019-02-19 | 2019-04-12 | 重庆中烟工业有限责任公司 | Reflow type distilling apparatus for extraction of essential oil |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: WUHAN HUANGHELOU FLAVORS CO., LTD. Free format text: FORMER OWNER: CHINA TOBACCO HUNAN INDUSTRIAL CO., LTD. Effective date: 20120117 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 430051 WUHAN, HUBEI PROVINCE TO: 430040 WUHAN, HUBEI PROVINCE |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20120117 Address after: 430040 Wuhan, East and West Lake District, Jinshan Road, No. 1355, Hubei Patentee after: Wuhan Huanghelou Flavors Co., Ltd. Address before: A road 430051 in Hubei province Wuhan city Hanyang District No. 22 technology center of Wuhan cigarette factory Patentee before: China Tobacco Hunan Industrial Co., Ltd. |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20090902 |