CN201042661Y - Gravitational method horizontal continuous granulation equipment - Google Patents

Gravitational method horizontal continuous granulation equipment Download PDF

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Publication number
CN201042661Y
CN201042661Y CNU2007200122381U CN200720012238U CN201042661Y CN 201042661 Y CN201042661 Y CN 201042661Y CN U2007200122381 U CNU2007200122381 U CN U2007200122381U CN 200720012238 U CN200720012238 U CN 200720012238U CN 201042661 Y CN201042661 Y CN 201042661Y
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chamber
granulation
particle
equipment
utility
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谢麟
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SHENYANG TIANYING POWDER TECHNOLOGY Co Ltd
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SHENYANG TIANYING POWDER TECHNOLOGY Co Ltd
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Abstract

The utility model relates to a gravity-method horizontal continuous granulation device, belonging to the field of fluidized spray granulation equipment. The granulation device comprises a dust-collecting chamber, a granulation chamber, a liquid jetting system, a falling material chamber, a hot air system, a continuous feeding unit, a discharge unit, a choke tube, and an air venting plate, and further a drying grading chamber and a material-returning unit. The choke tube and the air venting plate are equipped inside the falling material chamber and independently connected with the hot air system. The choke tube has a length of 50-90 mm. The drying grading chamber is equipped beside the falling material chamber and communicated with the bottom of the falling material chamber, and has a length of 2-6 m. The outlet of the drying grading chamber is connected with the discharge unit and the material-returning unit respectively. The device can directly and continuously granulate the powder material, dry and grade the granules, and yield qualified granules. The device has the advantages of production of granules of different sizes, high efficiency, reduced energy consumption, controllable accuracy of particle size, being suitable for large-scale production, and high yield (up to 2 tons per hour).

Description

Horizontal continuous granulating apparatus of using gravity method
Technical field
The utility model is particularly related to a kind of gravitational method horizontal Granulation Equipments of spherical particle material quantity-produced of reuniting that utilizes, and belongs to the fluidized-bed spray granulation apparatus field.
Background technology
Granular material has flowability, good permeability; no dust pollution; easily preserve; easily dissolving; advantage such as not perishable; therefore the application of grain products is very extensive; the extract of malt and milk, coffee, milk powder, soymilk and various instant drinks etc. as foodstuff; the granulating of the various catalyst of chemical industry class, additive, dyestuff, pigment; granulation before the various electuary medicines of pharmaceutical, the compressing tablet; granulations before the various ceramics of building material are shaped etc., the new method of ceramic tile production especially at present all is to suppress the technology of carrying out moulding again after adopting granulation.This shows that it is the indispensable production technologies of the numerous products of industry such as food, chemical industry, medicine, building materials, metallurgy, agricultural, military project, refractory material that powder is granulated.
The equipment of domestic production loose particles mainly contains following several at present:
(1). wet granulation equipment (three step granulation), promptly production process is divided into many complete equipments multiple working procedures such as batch mixing, granulation, drying, shaping and finishes, and belongs to more original production technology.Though the single complete equipment of this technology is fairly simple, there are problems such as floor space is big, operating process is numerous and diverse, operating condition is poor, dust pollution is serious, material loss is big, production efficiency is low, mainly use at present in industries such as medicine, food, chemical industry;
(2). fluidized granulating equipment (a step granulation), its production method is that a collection of raw material (powder) is packed in the closed container, below container, upwards import hot-air by ventilating board, make powder boiling (fluidization) at this moment above internal tank, spray vaporific binding agent downwards with a nozzle, the liquid material table surface tension that is subjected in the boiling increases, bond mutually, reunite and become big, this process stops hydrojet when all materials all reach granularity requirements, continue the input hot-air material is carried out drying, after reaching moisture requirement, stop air feed, material is taken out in the container carry out shaping.This equipment granulation and dry run just can be finished with a set of equipment, have simplified production technology, have reduced production site, have improved operating condition.It is very long that one step comminutor list is criticized the granulation cycle, needs 2~6 hours or longer, and energy consumption is very big, and actual 70%~80% energy consumption is arranged is to flog a dead horse; Its output size is subjected to the constraint of volume, and at present the domestic maximum type that puts into production is 300 types (are single batch feed intake be 300 liters), and its hourly output is less than 100 kilograms.The particle qualification rate of every batch of product is about about 70%, so the output of qualified products just still less in addition.Because its production capacity is little, production cost is higher again, so do not have substantially to use in industries such as food, chemical industry, only pharmaceuticals industry is used more;
(3). the mist projection granulating tower; the prilling process of this equipment is that the dilution of granulation raw material is sprayed into mist pearl with high pressure nozzle with slurries for slurries (containing 70%~80% water approximately); with high heat, high velocity air the mist pearl is taken away; mist pearl moisture content in the air-flow walking process volatilizees rapidly; become required particle, with reclaimer particle is reclaimed then.This equipment yield is bigger, generally can reach more than 1 ton/hour, thus relatively be fit to the production of big output product, as milk powder, washing powder, ceramic tile etc.But because the energy consumption of this device fabrication particle 90% or more be to be used for making material dewatering, energy consumption is very big, so the granulation cost is very high, this also is to cause one of reason that product price such as ceramic tile remains high.
More than several Granulation Equipments of Jie Shaoing are present main products, just they all exist pollute big, energy consumption is big, it is antipathetic requiring to reduce the aim of polluting, cutting down the consumption of energy with current social, and the scheme that proposed the gravitational method continuous granulator is arranged at present, though can overcome the above problems substantially, still there are problems in it, for example: though save the energy in other respects relatively, do not make its energy saving aspect dry obvious inadequately but its drying efficiency is high, drying effect is not good; Because its vertical design need take big quantity space, so it is little to increase the leeway of dry place, the leeway that increases the classification space is also little, causes grading effect not obvious; It is accurate inadequately that it makes qualified particle.
Summary of the invention
Goal of the invention: the utility model provides a kind of horizontal continuous granulating apparatus of using gravity method and prilling process, its objective is provides a kind of pollution-free, the particle manufacture equipment and the prilling process of low energy consumption, solve that the existing equipment energy consumption is big, cost is high, granulation inadequately accurately, shortcoming that the aspect exists such as drying and grading effect be not obvious.
Technical scheme: the utility model is achieved through the following technical solutions:
A kind of horizontal continuous granulating apparatus of using gravity method, this Granulation Equipments comprises that mainly dust pounces on collection chamber, granulation chamber, blanking chamber, hothouse, continuous feeding, removal device and the spray system that links to each other with this Granulation Equipments, hot-air system and other auxiliary equipment, and it is characterized in that: the hothouse of connection blanking chamber is set to horizontal dry classification chamber; The length of dry classification chamber is 2~6 meters; The outlet of dry classification chamber is connected with material-returning device with removal device respectively; Being arranged on the indoor length of throat of blanking is 50~90mm.
Advantage and effect: by the enforcement of technical solutions of the utility model, can solve well the problem of shortcoming that aspects such as the existing equipment energy consumption is big, cost height exist and thick, the thin and qualified particle that can't directly distinguish formation and the granulation of vertical gravitational method continuous granulator inadequately accurately, the shortcoming of aspect existence such as drying and grading effect be not obvious.
Granulation Equipments of the present utility model and prilling process have fundamentally been broken through existing dry method granulation processes flow process, and the non-slurry pelletizing serialization is achieved.This breakthrough brings a series of positive effects, and is mainly as follows:
1. energy-saving effect is obvious: because the breakthrough on the prilling, useful work obviously improves, and energy consumption is reduced greatly;
2. dust from flying obviously reduces, because totally-enclosed the working continuously of equipment do not have dust to raise substantially outward;
3. production efficiency obviously improves, because the setting of thick, thin material returning device can directly make a distinction the various particles that form, the qualification rate of finished product is improved greatly, the corresponding production efficiency that improved;
4. production site obviously reduces, and owing to granulation, drying are carried out synchronously, equipment volume is reduced greatly, and working area obviously reduces simultaneously.
The utility model is to be called " gravitational method continuous granulator and prilling process " at the original name of the applicant, application number is 200710010095.5 technical scheme, propose after some disadvantage corrects of Cun Zaiing in force, mainly be that vertical drying, classification working method with former gravitational method continuous granulator changes horizontal drying, hierarchical approaches into, the complete machine height is reduced greatly, the increase of length of throat improves blanking efficient greatly, divides the increase of level length that grading effect is obviously improved.This device is provided with a blanking chamber below granulation chamber, the blanking chamber is provided with several trunnions, and the length of trunnion is above than original doubling, and makes the blanking efficient that reaches the particle of release mesh in the granulation chamber obviously improve; Special hot blast is arranged by trunnion, the air quantity size of hot blast can be controlled.The size of the qualified particle of requirement is depended in the control of air quantity size.Because dry classification is changed into the horizontal operation mode, thus greatly reduce the complete machine height, thereby the increase length of throat of having living space, the particle and the wind-force locked time that reach granularity requirements are increased, thereby improved blanking efficient greatly.The mode of horizontal dry classification makes particle enter the classification that will begin in a minute after the dryer section, can bring following positive effect:
1., the grading effect of particle is obviously improved, qualified particle can be controlled in the more accurate scope;
2., qualified particle drying efficient is improved, thereby saved energy consumption;
3., owing to solved the disadvantage that vertical dry place be difficult to strengthen, thereby drying efficiency is improved greatly, this point has great benefit to large-tonnage production equipment, can produce the continuous granulator of output more than 3 tons/hour.
Description of drawings
Fig. 1 is the structural representation of the utility model equipment;
Fig. 2 is that the utility model will be put structural representation;
Fig. 3 is the vertical view of the utility model ventilating board;
Fig. 4 is the side view that the utility model ventilating board is connected with trunnion;
Fig. 5 is the process chart of the utility model prilling process.
The specific embodiment
Below in conjunction with accompanying drawing the utility model Granulation Equipments and prilling process are described in detail as follows, but not because of specific embodiment restriction the utility model.
Among the figure: 1, pulse valve; 2, air-valve one; 3, air-introduced machine; 4, dust is pounced on the collection chamber; 5, nozzle; 6, peristaltic pump; 7, binding agent flow container; 8, granulation chamber; 9, trunnion; 10, blanking chamber; 11, heat exchanger; 12, air-valve two; 13, dry classification chamber; 14, vibrating motor; 15, thin material returning device; 16, thick material returning device; 17, removal device; 18, continuous feeding; 32, ventilating board; 35, particle; 36, hot-wind inlet; 41, air vent; 42, trunnion hole.Other auxiliary equipment refers to the equipment or device, the pipeline etc. that link to each other with this equipment, as air-introduced machine, air compressor, valve etc.
Embodiment 1:
Shown in accompanying drawing 1,2, the utility model is a kind of horizontal continuous granulating apparatus of using gravity method, the dry classification system that this Granulation Equipments comprises spray system that dust pounces on collection chamber 4, granulation chamber 8, is made up of nozzle 5, peristaltic pump 6, binding agent flow container 7, is made up of vibrating motor 14, blanking chamber 10, dry classification chamber 13, hot-air system of forming by air-introduced machine 3 and heat exchanger 11 and continuous feeding 18, removal device 17, material-returning device etc., continuous feeding 18 is connected with granulation chamber 8 by pipeline; Be provided with ventilating board 32 and trunnion 9 in the blanking chamber 10, the hot-blast pipe line of hot-air system is connected with trunnion 9 with ventilating board 32 respectively; Dry classification chamber 13 is arranged on the next door of blanking chamber 10 and is connected with the bottom of blanking chamber 10; The outlet of dry classification chamber 13 is divided into qualified particle outlet and defective particle outlet, and wherein qualified particle outlet is connected with removal device 17; Defective particle outlet is communicated with material-returning device, and material-returning device is connected with granulation chamber 8 by refeed line.
Shown in Fig. 3,4, be evenly distributed with air vent 41 on the ventilating board 32, also evenly be provided with the trunnion hole 42 that several and trunnion 9 sizes adapt on it, trunnion hole 42 corresponding settings on the inlet of trunnion 31 and the ventilating board 32 or trunnion 9 is set directly in the trunnion hole 42, the hot-air system that trunnion 31 and ventilating board 32 are formed with blower fan and heat exchanger 11 respectively by separately independently pipeline be connected, wherein the hot-blast pipe line of trunnion 9 is provided with the air-valve 2 12 of adjusting air quantity.
Material-returning device is two, is divided into the thick material returning device 16 that has broken function and the input port of thin 15, two material returning devices of material returning device 16,15 and all is communicated with the outlet of grading plant by pipeline; Slightly, the delivery outlet of thin material returning device 16,15 is communicated with granulation chamber 8 by refeed line respectively.
Removal device 17 is connected with the qualified particle delivery outlet of dry classification chamber by pipeline, and the output mouth of pipe of removal device 17 can be connected by pipeline with storage bin at a distance, can guarantee to make finished particle to be transported to the place of appointment like this.
Dust is pounced on the top that collection chamber 4 is arranged on granulation chamber 8, and dust is pounced on the pulse valve 1 that collection chamber 4 is provided with the pneumatically pulse dust cleaning.
The trunnion of the lengthening shown in Fig. 1,3 and horizontal dry classification chamber are main points of the present utility model, be to be provided with several length at 50~90mm trunnion 9 in blanking chamber 10, have special hot blast to feed trunnion 9 from hot-wind inlet 36, the air quantity size of hot blast can be controlled.The size of the qualified particle of requirement is depended in the control of air quantity size.When the 35 process trunnions of the agglomerated particle in the granulation chamber 8,9 tops, the gravity of particle is greater than the wind-force that makes progress, so just overcome wind-force and sunk to entering trunnion 9 in the blanking chamber 10, the trunnion 9 of lengthening increases the particle and the wind-force locked time that reach granularity requirements, thereby has improved blanking efficient greatly.The mode of horizontal dry classification makes particle enter the classification that will begin in a minute after the dryer section.If strengthening grading effect, the length of increase grading room can make grading effect obvious, if but vertically increase then the height of whole equipment is significantly increased so that some factories do not have excessive workshop to be suitable for producing, the utmost point is unfavorable for promoting, if and the consideration limitation in height increases the length of grading room then the length of grading room is restricted, therefore horizontal is adopted in the dry classification chamber 13 of this device, make under the prerequisite that the complete machine height reduces greatly, its length also is increased to 2-6 rice (different type of machines length is different), on the basis of saving longitudinal space, because the comparison of dry classification fully obviously improves grading effect.
The process of the utility model granulation as shown in Figure 5, solid line is represented the trend of material and liquid stream among the figure, dotted line is represented the hot blast trend, is summarized as follows: adopt above-mentioned equipment as Granulation Equipments; In the granulation chamber of Granulation Equipments, add a certain amount of former powder earlier, former powder is fluidization under the effect of the hot-air system of air-heater and heat exchanger composition, pass through nozzle, the spray system that peristaltic pump and binding agent flow container are formed sprays into binding agent in granulation chamber, be subjected to the former powder of fluidization of the liquid poly-regimental commander that bonds mutually big, form particle, size according to discharge quantity of fan in the size adjustment trunnion of making grain graininess, the particle that making grows up reaches the requirement granularity enters blanking chamber 10 dryings by the trunnion of Granulation Equipments, particle after coming out from blanking chamber 10 under the vibration processing of vibrating motor, continue on the dry classification chamber 13 dry, classification is discharged qualified particle and is entered removal device as finished product, defective particle turns back to granulation chamber through material-returning device and continues granulation, constantly replenish former powder through continuous feeding in the granulation chamber, make granulation, dry, discharging the particle process carries out continuously.
Above-mentioned former powder by continuous feeding 18 by compressed air to granulation chamber's 8 continuous feedings.
Above-mentioned method middle and upper part granulation and bottom drying, classification are carried out synchronously.
Above-mentioned particle is by trunnion the time, because the trunnion 9 of lengthening increases the particle and the wind-force locked time that reach granularity requirements, the fine grained of crossing that enters the blanking chamber is greatly reduced, thereby the number of times of operation repeatedly that make thin material returning device turn back to 8 continuation granulations in the granulation chamber significantly reduce, and have saved energy consumption.
Above-mentioned particle carries out classification at once after entering the dry classification chamber, cross thick after the classification or cross fine grained and turn back to 8 continuation granulations granulation chamber in through thick, thin material returning device, because what adopted dry classification chamber 13 is the horizontal design, even hierarchy is simplified greatly like this, prolonged the classification approach again, grading effect is obviously improved, the drying efficiency of qualified particle is improved greatly, thereby saved the time and the energy greatly.
Details are as follows to the process of the utility model granulation below in conjunction with the utility model Granulation Equipments shown in Figure 1:
Powder as raw material is reinforced at any time in granulation chamber 8 by a controllable continuous feeding 18, the powder that adds in the granulation chamber 8 is fluidization by the hot blast drive that is provided by hot-air system from bottom to top of ventilative ventilating board 32, when the powder in joining granulation chamber 8 reaches a certain amount of, the nozzle 5 of granulation chamber 8 tops begins to spray the binding agent of atomizing, make granulation chamber's 8 interior fluidised powders evenly be subjected to liquid, the poly-group of bonding forms a particulate to be subjected to powder surface tension behind the liquid to increase mutually, material constantly accepts to spray take liquid-containing binder, small particle is constantly grown up, length reaches constant weight to the particle that requires granularity, when it arrives the utility model key structure, when being the top of trunnion 9 since its gravity greater than hot blast to its active force that makes progress, sink to entering blanking chamber 10, the particle that enters blanking chamber 10 at the uniform velocity moves down under the effect of vibrating motor formation vibration force, under the hot blast effect, dehydrate, the bottom of hothouse 10 is connected with dry classification chamber 13, particle here limit continues dry, the limit classification, crossing coarse granule enters thick material returning device 16 and returns granulation chamber 8 through fragmentation, qualified particle enters removal device 17 and regularly is discharged to the appointed place, and fine grained enters thin material returning device 15 and returns granulation chamber 8 excessively; Continuous feeding 18 constantly replenishes powder material in granulation chamber 8, granulation, drying, qualified particle are discharged continuously carry out, and has realized the continuous of prilling.The hot-air system that hot blast in the utility model equipment is made up of heat exchanger 11 and air-introduced machine 3 provides, and its stroke valve 1 can be controlled total blast volume at any time, air-valve 2 12 control finished product grain graininess sizes, and air-valve three is used for fast cooling.Hot blast is handled the dustless waste gas of discharge through purifier before discharge, the fine powder of holding back enters granulation chamber through pulse valve 1 effect and continues granulation.This device is formed spray system by binding agent flow container 7, peristaltic pump 6, nozzle 5, and the size of the controllable rotation speed system spouting liquid by adjusting peristaltic pump 6 can be controlled the size of hydrojet mist pearl by adjustment nozzle admission pressure.
The utility model Granulation Equipments and prilling process have fundamentally been broken through existing dry method granulation processes flow process, and the non-slurry pelletizing serialization is achieved, and have also solved in the vertical gravitational method continuous granulator simultaneously, and it is excessive to take up room; Because of vertical design makes length of throat limited so that the too short drying effect that influences in dry path is wasted energy simultaneously; Because of vertical design makes hierarchical paths limited so that classification efficiency is not high, influence the precision of particle.This breakthrough brings a series of positive effects, and is mainly as follows:
(1) energy-saving effect is obvious: because the breakthrough on the prilling reduces energy consumption greatly.Table 1 has been listed the relevant data of several Granulation Equipments energy consumptions:
Table 1
Device type One step comminutor Vertical comminutor The utility model equipment
Model PGL-20 LZL-30 LZLW-30
Production capacity kg/h 15~25 25~35 30~40
General power kw 41 15 15
Unit energy consumption kw/kg 2.05 0.5 0.4
Can loss-rate 5.125 1.25 1
As can be seen from the above table, the energy-saving effect of the utility model equipment is obvious especially, and this point also can get across theoretically.With a step comminutor is example; it is high especially that its production technology forces granulation chamber to include material concentration; in granulation process, spouting liquid is restricted, and being subjected to the liquid material is few part; they may just have an opportunity to be subjected to once more liquid after reuniting for a long time; their through colliding the fragmentation that has mutually, treat to be subjected to next time just to understand at inferior growth, granulating so repeatedly behind the liquid under fluidized state before being subjected to liquid next time; broken repeatedly, so need just to make all materials all reach granularity requirements for a long time.In dry run, there is a large amount of particles to collide fragmentation mutually again and diminishes, this shows that a step comminutor most of energy in granulation process is flogging a dead horse.And the utility model equipment granulation chamber include the material concentration very low, as long as spray film can penetrator not expect that reaching ventilating board just can, so the fluidisation landscape is very little, material be subjected to also big many of liquid chance, it is fast many that the speed of granulating is wanted, and the particle that reaches granularity requirements enters hothouse very soon and carries out drying, and dry gas stream is dried particles not only, and arrives granulation chamber and continue work done.In addition, the facilitated fluidization of material in the utility model equipment also plays the effect of saving energy consumption.And the power consumption of mist projection granulating big be because its energy of 90% all be used for the dehydration, dried material.
(2) production efficiency obviously improves: because the energy consumption of inaction reduces greatly, so production efficiency improves greatly, and the utility model equipment has a cover grading plant to make the particle of discharge qualified fully, need not to do once more shaping and handles.
(3) volume obviously reduces: because production efficiency improves greatly; so equipment volume reduces greatly; compare with a step comminutor, the equipment volume of its PGL-20 model is φ 1200 * 3150, and the equipment volume of the utility model equipment LZL-30 model is φ 580 * 2750.Therefore, the utility model equipment can provide large-tonnage non-slurry pelletizing equipment, and it is big to resemble the such output of ceramic tile, if the equipment that the big product of power consumption provides with the utility model equipment goes production, will bring great economic benefit.
(4) the particle quality obviously improves: by analyzing as can be known in (1), one step comminutor material granulating repeatedly in granulation process, broken repeatedly, the particle that has needs through so many times process, and the particle that has only passes through for several times such process, thereby the composition that the former contains in the slurries is many, and the latter is then few; The former is harder, and the latter is pine.Can draw thus, particulate component, difference in hardness that a step comminutor is produced are very big.And the utility model equipment material granulating process basically identical in granulation process, thereby also basically identical of particulate component, also obtained confirmation by experiment.
(5) environmental pollution obviously reduces: the utility model equipment is totally-enclosed operation in granulation process, does not have dust from flying.Charging, discharge process be also without operating personnel contact, so reduced environmental pollution greatly and to the pollution of material.
(6) can be the user and bring obvious economic benefit:
1. since equipment volume little, pollute little, so capital expenditure can significantly reduce;
2. because energy consumption is low, so the equipment operating cost can reduce greatly, product cost also can significantly reduce.
(7) mode of horizontal dry classification makes particle enter the classification that will begin in a minute after the dryer section, can bring following positive effect:
The grading effect of particle is obviously improved, qualified particle can be controlled in the accurate more scope;
Qualified particle drying efficient is improved, thereby saved energy consumption;
3., owing to solved the disadvantage that vertical dry place be difficult to strengthen, thereby drying efficiency is improved greatly, this point has great benefit to large-tonnage production equipment, can produce the continuous granulator of output more than 2 tons/hour.
In sum, adopt horizontal continuous granulating apparatus of using gravity method of the present utility model and prilling process, can carry out granulation continuously and directly distinguish good qualified particle and export, underproof thick excessively, cross fine grained and get back to by material returning device and improve drying effect on the basis of the circulation that enters granulation in the granulation chamber of equipment more significantly and compare with the granulation precision, with vertical gravitational method continuous granulator and showing more superior energy-saving effect aspect raising drying efficiency and the classification efficiency.Especially the size and the yield rate of the particle that will make can be better controlled in the lengthening setting of trunnion and being horizontally disposed with of dry classification chamber, and be more suitable for large-scale promotion.

Claims (1)

1. horizontal continuous granulating apparatus of using gravity method, this Granulation Equipments comprises that mainly dust pounces on collection chamber (4), granulation chamber (8), blanking chamber (10), hothouse, continuous feeding (18), removal device (17) and the spray system that links to each other with this Granulation Equipments, hot-air system and other auxiliary equipment, and it is characterized in that: the hothouse of connection blanking chamber (10) is set to horizontal dry classification chamber (13); The length of dry classification chamber (13) is 2~6 meters; The outlet of dry classification chamber (13) is connected with material-returning device with removal device (17) respectively; Trunnion (9) length that is arranged in the blanking chamber (10) is 50~90mm.
CNU2007200122381U 2007-05-24 2007-05-24 Gravitational method horizontal continuous granulation equipment Expired - Fee Related CN201042661Y (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101721946B (en) * 2008-10-21 2012-05-02 中国石油大学(北京) Novel spray granulation and separation tower with centrifugal separation function

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101721946B (en) * 2008-10-21 2012-05-02 中国石油大学(北京) Novel spray granulation and separation tower with centrifugal separation function

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