CN1820649A - Compound amino acid powder and its preparing method and its compound amino acid drink - Google Patents
Compound amino acid powder and its preparing method and its compound amino acid drink Download PDFInfo
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- CN1820649A CN1820649A CNA200610031424XA CN200610031424A CN1820649A CN 1820649 A CN1820649 A CN 1820649A CN A200610031424X A CNA200610031424X A CN A200610031424XA CN 200610031424 A CN200610031424 A CN 200610031424A CN 1820649 A CN1820649 A CN 1820649A
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Abstract
The present invention relates to compound amino acid powder, compound amino acid drink and their preparation process. The compound amino acid powder is prepared with animal and plant protein powder, and through acid hydrolysis, neutralization with alkali, centrifugal filtering to eliminate dregs, decolorizing the filtrate, vacuum concentrating and final spray drying. The compound amino acid powder is further produced into compound amino acid drink with or without other amino acid, such as lysine, added.
Description
Technical field:
The invention discloses a kind of amino acid powder, beverage and preparation method thereof, particularly disclose a kind of composite aminophenol powder and preparation method thereof and compound amino acid drink thereof.
Background technology:
Along with improving constantly of people's living standard, the beverage consumption idea constantly changes, people are to the beverage requirement, recover from fatigue and nutrition to having simultaneously to quench one's thirst gradually by initially quenching one's thirst merely, and regulate the human physiological functions beverage and pursue, amino acid is as the protein important component part, and the essential material of human body institute, people continually develop amino acid nutrient beverage such as Chinese patent application and number are 03802849.2 " amino acid powder and preparation method thereof) " promptly is open preparation amino acid dry powder and preparation method thereof, it is to add trehalose with the preparation powder of amino acids in amino acid solution, make powder of amino acids easier dissolve and aftertaste better, just with the dry preparation of existing amino acid powder, its powder production cost height, and the various beverages of selling on the existing market mostly only can quench one's thirst, lack nutrition, expectation can obtain to contain the several amino acids powder, the method of beverage and energy large-scale industrial production.
Summary of the invention:
The present invention will provide a kind of nutrition, health, composite aminophenol powder that production cost is low, its preparation method and use this compound amino acid drink.
Technology contents of the present invention is achieved like this:
A kind of compound amino acid powder, preparation method thereof, undertaken by following processing step:
(1) protein acidifying hydrolysis by weight than being that 1～0.96: 0.03 ratio drops in the reactor, adds 100 ℃～130 ℃ of thermal control reaction temperatures with aminosal and acid, and stirring reaction 15～30 hours, hydrolysis solution;
(2) neutralizing hydrolysis is poured the said hydrolyzed reactant liquor into and was added the alkali neutralizing hydrolysis in the neutralization pond 4～10 hours, in and acid solution, filter cleaner gets filtrate then;
(3) decolouring is handled, and with above-mentioned filtrate, adds processings of decolouring of decolorizer active carbon in the suction Decolouring pot, controls 50 ℃～100 ℃ of temperature, 0.5～2.5 hour time; Enter concentration pan more after filtration;
(4) concentrate drying with above-mentioned solution in secondary filter enters concentration pan, is concentrated into liquid volume 20%～40%, the last spray-dried finished product that gets.
The compound amino acid powder, preparation method thereof:
(1) protein acidifying hydrolysis, with the aminosal powder, with concentration be 30% sulfuric acid solution, by weight than being that 0.96～0.03 ratio drops in the reactor, adding the thermal control reaction temperature is 115 ℃～125 ℃, stirs 20～25 hours, and surveying the solution Baume degrees is 8～15Be;
(2) neutralization reaction is poured the said hydrolyzed reactant liquor in the neutralization pond into, add sulfuric acid solution weight portion 30～40% calcium oxide and or calcium hydroxide carry out sulfuric acid in the neutralizing hydrolysis liquid, reacted 5～8 hours, then centrifugal filtration remove the gred filtrate;
(3) decolouring is handled, with the active carbon that adds filtrate weight portion 2%～5% in the above-mentioned filtrate suction Decolouring pot processings of decolouring, and 60 ℃～80 ℃ of control temperature, 1～1.5 hour time, the mensuration light transmittance gets filtrate through secondary filter again greater than 60%.
(4) concentrate drying is concentrated into liquor capacity 30～35% with above-mentioned in secondary filter adds concentration pan, the dry compound amino acid powder that gets of last spray-dried device.
The compound amino acid powder, preparation method thereof: described aminosal is animal protein powder or plant protein powder and or their mixture.
Compound amino acid powder, preparation method thereof: contain 15～20% weight portion milks in described animal and plant protein powder or their mixture, described milk be milk, goat milk, deer milk and or their mixtures, and the bean powder of 30～35% weight portions, corn flour and or their mixture.
The compound amino acid powder, preparation method thereof, the method for described concentrated liquid adopts the vacuum concentration method.
The composite aminophenol powder that described compound amino acid powder, preparation method thereof obtains above a kind of composite aminophenol powder disclosed by the invention.
The invention also discloses the compound amino acid drink that utilizes this composite aminophenol powder to be prepared from.
Compound amino acid drink disclosed in this invention also can be by composite aminophenol powder of the present invention, with or other amino acid, prepare as follows, add amino acid powder in the mineral water in proportion, decolorization filtering gets the achromaticity and clarification transparency liquid through heating up again, be added into an amount of sweetener at last, spices is rich in vitamin substances etc., be cooled to rapidly below 5 degree Celsius, charge into carbon dioxide, and sterilization, compound amino acid drink promptly got.
Described adding sweetener addition is counted 4～5% the white sugar that adds beverage weight by weight.
The composite aminophenol powder production process is as follows:
Raw material acidification hydrolization → add alkali neutralization → centrifugal filtration slagging-off → filtrate decolouring → destainer secondary filter → concentrated → spray-drying → finished product to put in storage;
The compound amino acid drink technological process of production is as follows:
Natural mineral water → filtration → adding compound amino acid powder rising temperature for dissolving → decolouring → interpolation sweetener and spices → secondary filter → cooling → heat exchange → charge into carbon dioxide → virus killing can → finished product to put in storage.
The present invention produces in the process of composite aminophenol powder, the aminosal powder adopts animal and plant protein, animal protein is generally selected milk for use, as milk, goat milk, deer milk powder class, preferentially select milk powder for use, and add an amount of deer milk powder, vegetable protein is selected beans for use, plant protein powders such as corn flour are preferentially selected soy meal for use.
Acid hydrolysis can adopt sulfuric acid and hydrochloric acid preferentially to select sulfuric acid for use in the production process, can use calcium hydroxide in the alkali neutralization reaction and add, caustic soda, calcium oxide.
The present invention adopts aminosal powder or solution to produce compound amino acid powder and preparation method thereof, its raw material is easy to get, be mainly milk such as milk, goat milk, deer milk powder class and liquid milk, and plant protein powder, corn, soy meal etc., production technology is reliable, simply, low cost of manufacture, the compound amino acid powder of producing contains the amino acid of multiple needed by human body, as glycine, serine, valine, leucine, glutamic acid etc., adopts the composite aminophenol powder of the present invention's preparation, and compound amino acid drink, its quality standard is as follows: see attached list 1,2
Subordinate list 1 composite aminophenol powder
| Project | Quality standard | |
| Physical and chemical index | Proterties | Be yellow powder |
| Amino nitrogen＞ | 8.5 | |
| Moisture content＜ | 5％ | |
| PH | 5.0～6.0 | |
| Heavy metal (mp6 meter) | 10ppm | |
| Sanitary index | Total number of bacteria＜ | 10.000 it is individual/g |
| Escherichia coli＜ | 90/100g | |
| Pathogenic bacteria | Must not detect |
Subordinate list 2 compound amino acid drinks
| Project | Quality standard | |
| Physical and chemical index | Amino acid (%) | 2～3 |
| Sodium mg/kg | 200～1000 | |
| Potassium mg/kg | 100～300 | |
| Calcium mg/kg | 40～200 | |
| Iron mg/kg | 5 | |
| Zinc mg/kg | 5 | |
| Aluminium mg/kg | 0.3 | |
| Arsenic mg/kg | 0.2 | |
| Copper mg/kg | 5 | |
| Oxide mg/kg | 0.05 | |
| Sanitary index | Total number of bacteria | 100 |
| Escherichia coli | 6 | |
| Pathogenic bacteria | Must not detect |
The present invention is described in further detail below in conjunction with specific embodiment:
Embodiment 1:
With 12 kilograms milk powders and 2 kilograms of deer milk powder, after 35 kilograms of bean powderes mixing, add 50 kg water again, dissolving also drops in the reactor, 115 ℃ of 3 kilograms of agitating heating control of the sulfuric acid of adding 30% reaction temperatures, reacted 20 hours, enter neutralization reaction when measuring the solution gravity Baume for 13Be, adding 1 kilogram of neutralisation of sulphuric acid of calcium oxide in the above-mentioned acidification hydrolization liquid suction neutralization pond, stirred 5 hours, filter cleaner gets filtrate then, adds 2 kilograms of active carbons in the filtrate suction Decolouring pot that will remove the gred, decolouring is 1.5 hours under 75 ℃ of temperature, the light transmittance of measuring solution then reaches more than 65%, enters concentration pan through secondary filter again, vacuumizes to be concentrated into 30% of decolouring filtrate volume, last spray-dried device drying promptly gets the compound amino acid powder;
Embodiment 2:
With 18 kilograms milk powders and 2 kilograms of goat milk powders, with 30 kilograms of bean powderes, after corn flour mixes, add 50 kg water again, drop in the reactor, 128 ℃ of 3.2 kilograms of agitating heating control of the sulfuric acid of adding 30% reaction temperatures, reacted 28 hours, enter neutralization reaction when measuring the solution gravity Baume for 10Be, adding 1.2 kilograms of neutralisation of sulphuric acid of calcium oxide in the above-mentioned acidification hydrolization liquid suction neutralization pond, stirred 8 hours, filter cleaner gets filtrate then, adds 3 kilograms of active carbons in the filtrate suction Decolouring pot that will remove the gred, decolouring is 1 hour under 80 ℃ of temperature, the light transmittance of measuring solution then reaches more than 70%, enters concentration pan more after filtration, vacuumizes to be concentrated into 35% of decolouring filtrate volume, last spray-dried device drying promptly gets the compound amino acid powder;
Application Example 1:
With 20 kilograms in the above-mentioned compound amino acid powder that is prepared into, add 1000 kilograms of mineral waters, heat temperature raising can also filter by the interior activated carbon decolorizing of suction Decolouring pot the dissolving of compound amino acid powder, get transparency liquid and add 40 kilograms of the good white sugar of dissolving again, 5 kilograms of hawthorn, an amount of anticorrisive agent, spices etc., through secondary filter, cooling charges into carbon dioxide, final pasteurising below 5 ℃ rapidly, can promptly gets compound amino acid drink.
Application Example 2:
With 23 kilograms and 5 kilograms valines of the above-mentioned compound amino acid powder that is prepared into, lysine, threonine etc., it is activated carbon decolorizing and filtration in the suction Decolouring pot that 1000 kilograms of adding mineral waters, heat temperature raising make the dissolving of compound amino acid powder, gets transparency liquid and adds 45 kilograms of the good white sugar of dissolving again, 5 kilograms of hawthorn, an amount of anticorrisive agent, spices etc., after filtration, cooling charges into carbon dioxide, final pasteurising below 5 ℃ rapidly, can promptly gets compound amino acid drink.
Claims (9)
1, a kind of compound amino acid powder, preparation method thereof, undertaken by following processing step:
(1) protein acidifying hydrolysis by weight than being that 1～0.96: 0.03 ratio drops in the reactor, adds 100 ℃～130 ℃ of thermal control reaction temperatures with aminosal and acid, and stirring reaction 15～30 hours, hydrolysis solution;
(2) neutralizing hydrolysis is poured the said hydrolyzed reactant liquor into and was added the alkali neutralizing hydrolysis in the neutralization pond 4～10 hours, in and acid solution, filter cleaner gets filtrate then;
(3) decolouring is handled, and with above-mentioned filtrate, adds processings of decolouring of decolorizer active carbon in the suction Decolouring pot, controls 50 ℃～100 ℃ of temperature, 0.5～2.5 hour time; Enter concentration pan more after filtration;
(4) concentrate drying with above-mentioned solution in secondary filter enters concentration pan, is concentrated into liquid volume 20%～40%, the last spray-dried finished product that gets.
2, according to the described compound amino acid powder, preparation method thereof of claim 1, it is characterized in that:
(1) protein acidifying hydrolysis, with the aminosal powder, with concentration be 30% sulfuric acid solution, by weight than being that 0.96～0.03 ratio drops in the reactor, adding the thermal control reaction temperature is 115 ℃～125 ℃, stirs 20～25 hours, and surveying the solution Baume degrees is 8～15Be;
(2) neutralization reaction is poured the said hydrolyzed reactant liquor in the neutralization pond into, add sulfuric acid solution weight portion 30～40% calcium oxide and or calcium hydroxide carry out sulfuric acid in the neutralizing hydrolysis liquid, reacted 5～8 hours, then centrifugal filtration remove the gred filtrate;
(3) decolouring is handled, with the active carbon that adds filtrate weight portion 2%～5% in the above-mentioned filtrate suction Decolouring pot processings of decolouring, and 60 ℃～80 ℃ of control temperature, 1～1.5 hour time, the mensuration light transmittance gets filtrate through secondary filter again greater than 60%.
(4) concentrate drying is concentrated into liquor capacity 30～35% with above-mentioned in secondary filter adds concentration pan, the dry compound amino acid powder that gets of last spray-dried device.
3, described according to claim 1 or 2, the compound amino acid powder, preparation method thereof is characterized in that: described aminosal is animal protein powder or plant protein powder and or their mixture.
4, according to the described compound amino acid powder, preparation method thereof of claim 3, it is characterized in that: contain 15～20% weight portion milks in described animal and plant protein powder or their mixture, described milk be milk, goat milk, deer milk and or their mixtures, and the bean powder of 30～35% weight portions, corn flour and or their mixture.
According to claim 1 or 2 described compound amino acid powder, preparation method thereofs, it is characterized in that 5, the method for described concentrated liquid adopts the vacuum concentration method.
6, a kind of composite aminophenol powder obtains according to the described method of claim 1～5.
7, a kind of compound amino acid drink is characterized in that: the compound amino acid drink that is prepared from by above-described composite aminophenol powder.
8, according to the described compound amino acid drink of claim 7, it is characterized in that: by described composite aminophenol powder and or other amino acid, prepare as follows, amino acid powder is added in the mineral water in proportion, get the achromaticity and clarification transparency liquid, be added into an amount of sweetener at last through the decolorization filtering that heats up again, spices, be rich in vitamin substances etc., be cooled to rapidly below 5 degree Celsius, charge into carbon dioxide, and sterilization, promptly get compound amino acid drink.
9, according to the described compound amino acid drink of claim 8, it is characterized in that: described adding sweetener is counted 4～5% the white sugar that adds beverage weight by weight.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB200610031424XA CN100490678C (en) | 2006-03-24 | 2006-03-24 | Compound amino acid powder and its preparing method and its compound amino acid drink |
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| CNB200610031424XA CN100490678C (en) | 2006-03-24 | 2006-03-24 | Compound amino acid powder and its preparing method and its compound amino acid drink |
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| CN100490678C CN100490678C (en) | 2009-05-27 |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101708050B (en) * | 2009-11-12 | 2012-08-29 | 南宁市肯扬生物技术有限公司 | Herbaceous amino acids beverage |
| CN102763878A (en) * | 2012-07-25 | 2012-11-07 | 北京中科健宇生物科技有限公司 | Functional health maca drink and production method thereof |
| CN104543390A (en) * | 2014-12-25 | 2015-04-29 | 东莞市双红生物转化技术有限公司 | Preparation method for producing amino acid through livestock blood bioconversion and product |
| CN105725013A (en) * | 2016-03-31 | 2016-07-06 | 广东利泰大健康产业股份有限公司 | Colorless low-sugar type amino acid beverage and preparation process thereof |
| CN106616834A (en) * | 2016-12-07 | 2017-05-10 | 上海爱普食品工业有限公司 | Preparation method of low-salt low-chloropropanol acid hydrolyzed vegetable protein |
| CN107410801A (en) * | 2017-08-02 | 2017-12-01 | 江苏省农业科学院 | A kind of Animal Liver protolysate drink and preparation method thereof |
| CN112108092A (en) * | 2020-09-22 | 2020-12-22 | 江苏鹏翔生物医药有限公司 | Preparation method and equipment of composite amino acid powder |
| CN113100167A (en) * | 2021-04-09 | 2021-07-13 | 湖南祥柏生态环保科技有限公司 | Comprehensive agricultural planting and breeding system |
| CN113439848A (en) * | 2021-06-16 | 2021-09-28 | 安徽安力肽生物科技有限公司 | Preparation method of amino acid powder |
| CN114304465A (en) * | 2022-01-27 | 2022-04-12 | 陇南市祥宇油橄榄开发有限责任公司 | Olive leaf extract effervescent tablet and preparation method thereof |
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2006
- 2006-03-24 CN CNB200610031424XA patent/CN100490678C/en not_active Expired - Fee Related
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101708050B (en) * | 2009-11-12 | 2012-08-29 | 南宁市肯扬生物技术有限公司 | Herbaceous amino acids beverage |
| CN102763878A (en) * | 2012-07-25 | 2012-11-07 | 北京中科健宇生物科技有限公司 | Functional health maca drink and production method thereof |
| CN102763878B (en) * | 2012-07-25 | 2013-08-14 | 北京中科健宇生物科技有限公司 | Functional health maca drink and production method thereof |
| CN104543390A (en) * | 2014-12-25 | 2015-04-29 | 东莞市双红生物转化技术有限公司 | Preparation method for producing amino acid through livestock blood bioconversion and product |
| CN105725013A (en) * | 2016-03-31 | 2016-07-06 | 广东利泰大健康产业股份有限公司 | Colorless low-sugar type amino acid beverage and preparation process thereof |
| CN106616834A (en) * | 2016-12-07 | 2017-05-10 | 上海爱普食品工业有限公司 | Preparation method of low-salt low-chloropropanol acid hydrolyzed vegetable protein |
| CN107410801A (en) * | 2017-08-02 | 2017-12-01 | 江苏省农业科学院 | A kind of Animal Liver protolysate drink and preparation method thereof |
| CN112108092A (en) * | 2020-09-22 | 2020-12-22 | 江苏鹏翔生物医药有限公司 | Preparation method and equipment of composite amino acid powder |
| CN112108092B (en) * | 2020-09-22 | 2022-04-12 | 江苏鹏翔生物医药有限公司 | Preparation method and equipment of composite amino acid powder |
| CN113100167A (en) * | 2021-04-09 | 2021-07-13 | 湖南祥柏生态环保科技有限公司 | Comprehensive agricultural planting and breeding system |
| CN113439848A (en) * | 2021-06-16 | 2021-09-28 | 安徽安力肽生物科技有限公司 | Preparation method of amino acid powder |
| CN114304465A (en) * | 2022-01-27 | 2022-04-12 | 陇南市祥宇油橄榄开发有限责任公司 | Olive leaf extract effervescent tablet and preparation method thereof |
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| CN100490678C (en) | 2009-05-27 |
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