CN1736434A - Throat comforting medicine with licorice and preparation process thereof - Google Patents
Throat comforting medicine with licorice and preparation process thereof Download PDFInfo
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- CN1736434A CN1736434A CN 200410064314 CN200410064314A CN1736434A CN 1736434 A CN1736434 A CN 1736434A CN 200410064314 CN200410064314 CN 200410064314 CN 200410064314 A CN200410064314 A CN 200410064314A CN 1736434 A CN1736434 A CN 1736434A
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Abstract
The invention relates to a throat comforting medicine with licorice and preparation process, wherein the raw material comprises 1000 parts of licorice root, 300 parts of cordate houttuynia, 250 parts of Chinese olive, 80 parts of sterculia seed, 50 parts of Momordica grosvenori, and 30 part of honeysuckle flower. The medicament also contains forming agent 80-90 weight parts, which can be at least two of refined white sugar, glucose plasm and malt sugar, the medicament also refrigerant 0.05-0.08 weight part, which can be at least one of peppermint oil and compound eucalyptus oil.
Description
[technical field]
The present invention relates to a kind of heat-clearing and toxic substances removing, cleaning throat and moistening larynx, the pharmaceutical composition of anti-inflammatory analgetic functional health care food Radix Glycyrrhizae throat comforting, particularly relate to be food be again that the vegetable Chinese herbal medicine of medicine is raw material (" Ministry of Public Health is about the notice of further standard healthy food material management ", defending the method prison sends out [2002] No. 51, adnexa 1) make, because of acute/chronic pharyngitis dry pharynx, pharyngalgia, pharyngeal swelling, the health food medicine of pharyngeal scorching hot disease such as dry and astringent extremely and preparation method thereof, belong to the field of Chinese medicines.
[background technology]
Dry pharynx, pharyngalgia, pharyngeal swelling, pharyngeal scorching hot dry and astringent discomfort are a kind of commonly encountered diseases, the sickness rate height, and number of patients is many, and refractory more brings a lot of worries and inconvenience to the patient.This mainly is because the result that acute/chronic pharyngitis causes.Refrigerant sore-throat relieving confection gets consumer reception very much on the market, yet the simple Herba Menthae essence that utilizes stimulates oral cavity and pharyngeal blood vessel, causes vasoconstriction, to reach the target of temporary transient reducing swelling and alleviating pain, can not solve the sufferings of pharyngeal discomfort at all.But also may cause the stomach illness, pharyngeal illness such as western medical treatment pharyngeal swelling, pharyngalgia, application method that can be different according to different classes of employing.Light disease is generally adopted local treatment, for example Dobell's solution etc. be coated with pharyngeal, also can containing domiphen bromide etc. lozenge, the heavier pharynx of symptom processs the breath, and the person adopts constitutional treatment, takes antibiotic, sulfonamides, medicines such as hormone.But Western medicine is normally alleviated surface symptoms, and side effect is big.If life-time service can cause patient's imbalance between YIN and YANG, immunity degradation, thus resistance against diseases is descended, the state of an illness is shown effect repeatedly, is difficult to cure.The modern chemistry medicine also do not have a kind of specially good effect for the treatment of such disease, can be for the medicine of taking for a long time.And Chinese medicine is with many active ingredients, and many target spots drug effect is a characteristic, on the dry pharynx due to the treatment acute/chronic pharyngitis, pharyngalgia, pharyngeal swelling, pharyngeal disease such as scorching hot special advantages arranged, and can take for a long time.Develop the traditional advantage of Chinese medicine integration of edible and medicinal herbs, the exploitation preparation stabilization, quality controllable, taking convenience, rapid-action, curative effect is reliable, and the dietotherapeutic preparation that bioavailability is high is significant.
The Radix Glycyrrhizae throat comforting that adopts the dietotherapeutic kind is a kind of preparation that is used for the health food of the dry pharynx, pharyngalgia due to the acute/chronic pharyngitis, pharyngeal disease such as scorching hot.The utilization Radix Glycyrrhizae distinctive antibacterial, sore-throat relieving promotes the production of body fluid, the function of relieving spasm to stop pain, relieving cough and resolving phlegm, invigorating the spleen and benefiting QI, utilizes Herba Houttuyniae heat-clearing and toxic substances removing, inhibitory anti-virus effect, assistant is made with the composition of Fructus Canarii, Fructus Momordicae, Semen Sterculiae Lychnophorae pharynx-clearing throat-benefiting.Effect with heat-clearing and toxic substances removing, cleaning throat and moistening larynx, anti-inflammatory analgetic, relieving cough and resolving phlegm.Present commercially available pharynx-clearing throat-benefiting medicine is many, and its deficiency is to enter at once in the stomach, can not soak into the long period pharyngeally, can not give pharyngeal a kind of comfortable, the sense of euphoria of patient.The commercially available confection that wets one's whistle also has, but since used combination without Radix Glycyrrhizae or not based on Radix Glycyrrhizae, mouthfeel is not good enough; It is excessive also to have plenty of Herba Menthae essence consumption, with minty note accurate adjustment mouthfeel, gives pharyngeal stimulation too big, is difficult to stand, and refrigerant thing too much also can cause stomach discomfort or other diseases.
[summary of the invention]
The object of the present invention is to provide a kind of heat-clearing and toxic substances removing that has, cleaning throat and moistening larynx, anti-inflammatory analgetic, relieving cough and resolving phlegm improve pharyngeal the swelling and ache due to the acute/chronic pharyngitis, the Radix Glycyrrhizae throat comforting of diseases such as pharyngeal scorching hot dry and astringent discomfort.
Another object of the present invention provides the preparation method of Radix Glycyrrhizae throat comforting.
Solution of the present invention is based on motherland's medical science to pharyngitis and pathogenetic understanding of complication and Therapeutic Principle, achieve with reference to modern pharmacological research, from motherland's medical treasure-house, filter out heat clearing away, detoxifcation, sore-throat relieving, promote the production of body fluid, lung moistening, antiviral, expelling phlegm for arresting cough, relieving spasm to stop pain, invigorating the spleen and replenishing QI, the body resistance strengthening and constitution consolidating, the natural plant of dietotherapeutic by the theory of Chinese medical science prescription, is alleviated because the effect of the pharyngeal pathological changes that acute/chronic pharyngitis causes.
Radix Glycyrrhizae throat comforting of the present invention is that raw material is made by 1000 weight portion Radix Glycyrrhizaes, 300 weight portion Herba Houttuyniae, 250 weight portion Fructus Canariis, 80 weight portion Semen Sterculiae Lychnophoraes, 50 weight portion Fructus Momordicaes, 30 weight portion Flos Loniceraes.Medicament also contains forming agent 80-90 weight portion, and this forming agent is in white sugar, glucose syrup, the maltose at least two kinds, contains freshener 0.05-0.08 weight portion, and this freshener is at least a in Oleum menthae and the compound recipe eucalyptus oil.
The preparation method of Radix Glycyrrhizae throat comforting of the present invention is:
(1) take by weighing Radix Glycyrrhizae, Herba Houttuyniae, Fructus Canarii, Fructus Momordicae, water flushing 1-2 time is with 1: 10-1: 15 (W: V) be soaked in water and spend the night, 100 ℃ of water temperature heat were extracted 1-2 hour, filtered, and medicinal residues add water (flood and get final product), 100 ℃ of water temperature heat of secondary were extracted 0.5 hour, filtered, and merged medicinal liquid.
(2) get Semen Sterculiae Lychnophorae, Flos Lonicerae, water flushing back water logging is spent the night (water does not have medicine to get final product), and 100 ℃ of water temperature heat were extracted 0.5 hour, filtered.
(3) get (1) (2) two kinds of medicinal liquids, merging concentrates, and (70 ℃) get Radix Glycyrrhizae throat comforting medicine slurry to be concentrated into relative density 1: 10.
Add forming agent 80-90 weight portion, this forming agent is in white sugar, glucose syrup, the maltose at least two kinds, contain freshener 0.05-0.08 weight portion, this freshener is at least a in Oleum menthae and the compound recipe eucalyptus oil, and Steam Heating is dissolved, and stirs, filter, pour in the molding sugar mould, treat natural cooling after, the demoulding, packing.
[Radix Glycyrrhizae throat comforting chmice acute test-maximum tolerance determination (margin of safety test)]
The Radix Glycyrrhizae throat comforting be up-to-date development by be food be again that the medicine natural plant is the novel throat lozenge that raw material is made, for the purpose of edible safety, the spy makes the chmice acute toxicity test, i.e. human body margin of safety test.
This law is got the healthy mice of body weight 18-22g, male and female half and half are divided into several groups at random, and what every treated animal gavaged variable concentrations is subjected to the reagent thing 1-3 time, every 0.5ml, observe the various life Signs of mice in 7 days, determine that mice has or not toxic reaction, be not as the criterion dead group just not occur, the dosage of this moment is the maximum tolerated dose of mice, calculate the dosis tolerata multiple then as follows, oral with tolerance people consumption is safety more than 100 times, and computing formula is as follows:
(1) reagent: 1, main component Radix Glycyrrhizae 70% Herba Houttuyniae, Fructus Canarii, Semen Sterculiae Lychnophorae etc. 30%
2, the aqueous extract of mentioned component is got in preparation, merges to be concentrated into 2g/ml
Concentration, with syrup (40 °),, standby by 1: 1 mixing.
(2) animal subject: 1, the healthy Kunming of kind kind white mice is 80, male and female half and half
2, grouping is divided into mice 4 groups at random, and 1. contrast gavages Fructus Vitis viniferae
Slurry (40 °); 2. 1g/ only/the d test group; 3. 2g/ only
/ d test group is 3g//d test group 4.
(3) method: 1, the route of administration per os is irritated stomach, requires to irritate the preceding mice fasting of stomach, taboo
Water 4 hours.
2,1. matched group 3 times/day of dosage, 0.5ml/ time/only
2. test group is 1 time/day, 0.5ml/ time/only
3. test group is 2 times/day, 0.5ml/ time/only
4. test group is 3 times/day, 0.5ml/ time/only
3, observe: each organizes mice after irritating stomach continuous 7 days, observes each group
Situations such as the feed of mice, water inlet, activity are differentiated
Its hair color, state, action have no change, thereby declare
Whether do not poison, dead be the most serious poisoning.
Table one: Radix Glycyrrhizae throat comforting effective ingredient acute toxicity test in mice result
| Feed | Water inlet | Movable | Signs | Toxic reaction | Mortality rate | |
| Contrast | - | - | - | - | - | 0 |
| Lg//day | - | - | - | - | - | 0 |
| 2g//day | - | - | - | - | - | 0 |
| 3g//day | 5-，2× | - | 5-，2× | 5-，2× | 5-，2+ | 0 |
Annotate;-normal, * unusual ,+toxic reaction arranged
(4) every mice maximum tolerated dose of result is 3g/d, adult consumption 50g every day,
Maximum tolerated dose multiple=3/20*5000/50=150 of mice doubly
Result of calculation shows that the maximum tolerated dose of mice＞tolerance people consumption is more than 100 times, and this Radix Glycyrrhizae throat comforting is taken safety.
[the Radix Glycyrrhizae throat comforting is to the main pharmacodynamics research of acute pharyngitis]
(1), relieving sore-throat by clearing away heat effect:
1, antiinflammatory test---suppress the capillary permeability test
[principle] drips dimethylbenzene in the mouse web portion skin of unhairing, because of its local irritant effect causes capillary permeability hyperfunction, when go into blue dye (ivens orchid) in intravenous injection after, the ivens orchid can go out to vascular exosmosis in hyperfunction blood capillary, form blue mottle piece in the position of melted paraxylene, with the dyestuff seepage discharge what, as judging whether medicine can the hyperfunction index of the early stage capillary permeability of inflammation-inhibiting.
Glycyrrhizin, enoxolone and licoflavone etc. are the main effective ingredient of Radix Glycyrrhizae, treat the actute infection inflammation clinically curative effect is preferably arranged, its therapeutic mechanism with strengthen anti-infectious immunity, antiallergic, analgesic and antiinflammatory action is relevant, in the experimentation due to the Radix Glycyrrhizae extract xylol early stage inflammation obvious inhibitory action is arranged.
[material] animal: mice, male and female half and half, body weight 18-22g, equipment: 0.25ml white inner core syringe, No. 4 syringe needles, spectrophotometer, medicine and reagent: Radix Glycyrrhizae extract, injection (40/mg/2ul/ props up), the blue normal saline solution (0.5%) of ivens, dimethylbenzene, acetone, sodium sulfate etc.
[method] 1, the blue normal saline preparation of 0.5% ivens: precision takes by weighing the blue 0.5g of ivens, is dissolved in normal saline and becomes 100ml.
2, acetone sodium sulfate liquid configuration: precision takes by weighing anhydrous sodium sulfate 1.5g, is dissolved in becoming 150ml slowly to add acetone 350ml again in the distilled water in metabisulfite solution, and this liquid is used to extract the skin inner dye.
3, experiment: 30 mices, male and female half and half are divided into 3 groups at random: 1. 2. 3. 200mg/kg group (0.2ul/ time /) of 100mg/kg group (0.1ul/ time/only) of matched group.Respectively at back subcutaneous injection Radix Glycyrrhizae extract, injection and normal saline.Inject the blue normal saline of 0.5% ivens in the tail vein after 1 hour, 0.1ml/10g body weight, melted paraxylene 0.03ml/ is only on the skin of unhairing of the positive middle part of mouse web portion immediately, mice takes off cervical vertebra and causes death after 20 minutes, peel skin of abdomen, be affixed on after the upset on the white enamel tray, according to each blue speckle color and luster depth it is divided into the 7-10 rank, 1 rank is remembered 1 fen, behind the blue mottle piece of evaluation skin, the every blue speckle of skin shreds to drop into operating scissors to be had in the plug teat glass, to going into acetone-sodium sulfate extracting solution 10ml, puts the dark place and places, shake test tube 2-3 time every day gently, 2000rpm is centrifugal 10 minutes after 3 days, gets supernatant in 590nm place colorimetric determination density, with the acetone acid-sodium sulfate school zero of not steeping skin.
[result] finds by the measurement result of above-mentioned experiment, no matter relatively with the scoring of the blue speckle color and luster of the skin depth, or compare to extract dyestuff spectrophotometer result, the numerical value of Radix Glycyrrhizae extract group all is starkly lower than the normal saline matched group, and it is hyperfunction to show that Radix Glycyrrhizae extract can obviously suppress dimethylbenzene induced mice skin of abdomen capillary permeability.The results are shown in Table 1:
The hyperfunction influence of table 1 Radix Glycyrrhizae 1 extract xylol induced mice capillary of skin permeability
| Medicine | Dosage (mg/ml) | Mus number (only) | The blue speckle depth (level) | Blue speckle amount of dye (ug) |
| Normal saline Radix Glycyrrhizae extract Radix Glycyrrhizae extract | - 100 200 | 10 10 10 | 5.9±1.8 3.1±2.0* 2.3±1.4** | 2.01±0.35 1.28±0.31* 1.12±0.29** |
It is one of the most frequently used model of antiinflammatory action research that [evaluation] capillary of skin permeability increases, favorable reproducibility as a result easy and simple to handle, the capillary of skin permeability changes also is the early stage important behaviour of inflammation simultaneously, red (telangiectasis), heat (blood flow acceleration), swollen performances such as (oozing out) are arranged under the local action of stimulus object, to " heat syndrome " see that disease is similar, so also be usually used in the pharmaceutically-active research of heat clearing away.
(2) antibacterial tests of Radix Glycyrrhizae throat comforting---punching perfusion method
[principle] digs out agar block on the meat extract agar flat board with aseptic card punch, the medicinal liquid that in each hole, adds variable concentrations then respectively, and test organisms liquid is coated on the agar around the hole wall equably, after the cultivation, judge medicine bacteriostatic ability with the diameter (mm) that the bacterium circle occurs suppressing.
[method] is that the aseptic card punch of 6mm punches 5-6 with the diameter on the meat extract agar flat board, choose agar in the hole with aseptic syringe needle, add variable concentrations medicinal liquid 0.2ml in each hole respectively, then test organisms liquid evenly is inoculated on the meat extract agar all around of hole, hatch, with the bacteriostasis of antibacterial circle diameter mm evaluation medicine.Result's proof has tangible bacteriostasis.
[investigation of volunteer crowd's effect test]
Be the function of detection Radix Glycyrrhizae throat comforting and crowd's welcome degree, the further corresponding market demand, we the special volunteer of tissue part tastes the Radix Glycyrrhizae throat comforting, and makes following investigation statistics:
Function: heat-clearing and toxic substances removing, cleaning throat and moistening larynx, anti-inflammatory analgetic, relieving cough and resolving phlegm;
The aspiration object: 1, the various places teacher is 50; 2, the retailer is 10; 3, sing 10 of fans; 4, flu is followed 10 of disease persons; 5, the heavy smoker is 10; Contrast 10.Amount to 100.
Investigation method: edible for each person every day 10 Radix Glycyrrhizae throat comfortings, 0.5-1 hour at interval, an edible continuously week; Matched group eats common larynx moistening candy, the same test group of method.Adopt inquiry that the method for the impression of above-mentioned functions is carried out example table statistics.
The supply and marketing judgment criteria: the main suit is a produce effects to the symptom person of having clear improvement; It is effective that symptom is had the improver; Symptom there is not obvious improver for invalid.
Table two: Radix Glycyrrhizae throat comforting crowd result of the test.
| Heat-clearing and toxic substances removing | Cleaning throat and moistening larynx | Anti-inflammatory analgetic | Relieving cough and resolving phlegm | |||||
| Test | Contrast | Test | Contrast | Test | Contrast | Test | Contrast | |
| Produce effects | 68 | 0 | 81 | 18 | 66 | 1 | 48 | 0 |
| Effectively | 27 | 5 | 19 | 2 | 30 | 2 | 37 | 1 |
| Invalid | 5 | 15 | 0 | 0 | 4 | 17 | 15 | 0 |
| Total effective rate | 95％ | 25％ | 100％ | 100％ | 96％ | 15％ | 75％ | 5％ |
Above-mentioned the survey showed that: edible Radix Glycyrrhizae throat comforting has obvious effect to general larynx disease, but often edible mitigation symptoms reaches the purpose of protecting the strong larynx of throat.
The selected medicine of the present invention all be food be again medicine natural plant kind, the nature and flavor sweetness has no side effect, manufactured goods are sweet and oiliness, and are refrigerant tasty and refreshing, are a kind of new-type traditional Chinese health foods.
Chinese medicine of the present invention adopts water extraction, and active ingredient is kept fully, and forming process adopts the hard sugar processing technology, and operating process is simple, and the flow process time is short, is suitable for the large-scale production of scale.
Claims (2)
1, a kind of pharmaceutical composition of health food Radix Glycyrrhizae throat comforting, it is characterized in that by 1000 portions of Radix Glycyrrhizaes, 300 parts of Herba Houttuyniae, 250 portions of Fructus Canariis, 80 parts of Semen Sterculiae Lychnophoraes, 50 portions of Fructus Momordicaes, 30 portions of Flos Loniceraes be that raw material is made, medicament also contains forming agent 80-90 weight portion, this forming agent is in white sugar, glucose syrup, the maltose at least two kinds, contain freshener 0.05-0.08 weight portion, this freshener is at least a in Oleum menthae and the compound recipe eucalyptus oil;
2, the preparation method of the Radix Glycyrrhizae throat comforting of claim 1 is as follows by concrete steps:
A, take by weighing Radix Glycyrrhizae, Herba Houttuyniae, Fructus Canarii, Fructus Momordicae, water flushing 1-2 time is with 1: 10-1: 15 (W: V) be soaked in water and spend the night, 100 ℃ of water temperature heat were extracted 1-2 hour, filtered, and medicinal residues add 100 ℃ of water temperature heat of water (flood and get final product) secondary and extracted 0.5 hour, filter, merge medicinal liquid;
B, get Semen Sterculiae Lychnophorae, Flos Lonicerae, water flushing back water logging is spent the night (water does not have medicine get final product), and 100 ℃ of water temperature heat were extracted filtration 0.5 hour;
C, get two kinds of medicinal liquids of a, b, merge and concentrate, be concentrated into relative density 1.10 (70 ℃) Radix Glycyrrhizae throat comforting medicine slurry;
It is characterized in that adding forming agent 80-90 weight portion, this forming agent is in white sugar, glucose syrup, the maltose at least two kinds, contain freshener 0.05-0.08 weight portion, this freshener is at least a in Oleum menthae and the compound recipe eucalyptus oil, and Steam Heating is dissolved, stir, filter, pour in the molding sugar mould, treat natural cooling after, the demoulding, packing.
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| CN 200410064314 CN1736434A (en) | 2004-08-19 | 2004-08-19 | Throat comforting medicine with licorice and preparation process thereof |
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|---|---|---|---|
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101803663A (en) * | 2010-04-23 | 2010-08-18 | 山东蜜福堂食品有限公司 | Sugar alcohol crystal cool sugar-free candy and preparation method thereof |
| CN103070439A (en) * | 2013-02-01 | 2013-05-01 | 重庆百花生物医药股份有限公司 | Health care beverage with functions of clearing heat, moistening lung and promoting production of body fluid as well as preparation method and application of health care beverage |
| CN103584076A (en) * | 2012-08-14 | 2014-02-19 | 广西玉林制药集团巨安保健品有限公司 | Health food composition |
| CN105079230A (en) * | 2015-09-24 | 2015-11-25 | 高其品 | Buccal tablet for treating chronic pharyngitis |
| CN105767827A (en) * | 2016-04-11 | 2016-07-20 | 广州市东鹏食品饮料有限公司 | Method for preparing dried orange peel and boat-fruited scaphium seed beverage capable of producing saliva, moistening throat and stimulating appetite |
| CN105848664A (en) * | 2013-12-23 | 2016-08-10 | 阿波卡-阿格里科拉共同股份公司 | Composition for use in the treatment of persistent cough |
| CN105851749A (en) * | 2016-04-11 | 2016-08-17 | 广州市东鹏食品饮料有限公司 | Dried orange peel and scaphium scaphigerum beverage capable of promoting production of body fluid, wetting throat and stimulating appetite |
-
2004
- 2004-08-19 CN CN 200410064314 patent/CN1736434A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101803663A (en) * | 2010-04-23 | 2010-08-18 | 山东蜜福堂食品有限公司 | Sugar alcohol crystal cool sugar-free candy and preparation method thereof |
| CN101803663B (en) * | 2010-04-23 | 2014-10-15 | 山东蜜福堂食品有限公司 | Sugar alcohol crystal cool sugar-free candy and preparation method thereof |
| CN103584076A (en) * | 2012-08-14 | 2014-02-19 | 广西玉林制药集团巨安保健品有限公司 | Health food composition |
| CN103584076B (en) * | 2012-08-14 | 2016-06-22 | 广西玉林制药集团巨安保健品有限公司 | A kind of compositions of health food |
| CN103070439A (en) * | 2013-02-01 | 2013-05-01 | 重庆百花生物医药股份有限公司 | Health care beverage with functions of clearing heat, moistening lung and promoting production of body fluid as well as preparation method and application of health care beverage |
| CN103070439B (en) * | 2013-02-01 | 2014-03-05 | 重庆百花生物医药股份有限公司 | Health care beverage with functions of clearing heat, moistening lung and promoting production of body fluid as well as preparation method and application of health care beverage |
| CN105848664A (en) * | 2013-12-23 | 2016-08-10 | 阿波卡-阿格里科拉共同股份公司 | Composition for use in the treatment of persistent cough |
| CN105079230A (en) * | 2015-09-24 | 2015-11-25 | 高其品 | Buccal tablet for treating chronic pharyngitis |
| CN105079230B (en) * | 2015-09-24 | 2018-07-06 | 高其品 | A kind of buccal tablet for treating chronic pharyngitis |
| CN105767827A (en) * | 2016-04-11 | 2016-07-20 | 广州市东鹏食品饮料有限公司 | Method for preparing dried orange peel and boat-fruited scaphium seed beverage capable of producing saliva, moistening throat and stimulating appetite |
| CN105851749A (en) * | 2016-04-11 | 2016-08-17 | 广州市东鹏食品饮料有限公司 | Dried orange peel and scaphium scaphigerum beverage capable of promoting production of body fluid, wetting throat and stimulating appetite |
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