CN1721589A - Silk reeling technology for hollow cocoon, dry solid cocoon and live pupa cocoon - Google Patents

Silk reeling technology for hollow cocoon, dry solid cocoon and live pupa cocoon Download PDF

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Publication number
CN1721589A
CN1721589A CN 200510075748 CN200510075748A CN1721589A CN 1721589 A CN1721589 A CN 1721589A CN 200510075748 CN200510075748 CN 200510075748 CN 200510075748 A CN200510075748 A CN 200510075748A CN 1721589 A CN1721589 A CN 1721589A
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cocoon
silk
hollow
separate
relaxes
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CN 200510075748
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CN100359049C (en
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韩翠英
韩仁君
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Zheng Liwei
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Priority claimed from CN 200410049419 external-priority patent/CN1584134A/en
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Abstract

This invention relates to hollow pulp cocoon, dried cocoon and live cocoon filature process, which vacuums the waste hollow pulp cocoon or dried cocoon discarded in traditional process and dips the cocoon under room temperature after being boiled and goes through dispel liquid composed of sodium silicate, sodium carbonate, red oil, borax, hydrogen dioxide solution, surface activity agent and water and finally through filature and shading and processing into silk.

Description

Hollow cocoon, dry cocoon and living cocoon silk reeling technology
Technical field
The present invention relates to a kind of silk cocoon silk reeling technology, the silk reeling technology of particularly a kind of hollow cocoon, dry cocoon and living cocoon.
Background technology
Tussah cocoon belongs to pretty young woman section, and its whole body all is precious, and the silk of extraction belongs to green-fabrics, can be used as the raw material of high-grade ornament and various textiless, and the tussah filature has long civilized history from ancient times to the present.Though traditional silk reeling method is with a long history, technical maturity, but only be applicable to maturation, full bright silk cocoon, generally as leftover bits and pieces, can not fully be used for some hollow cocoons and dry cocoon, even perhaps be used for filature reluctantly, but separate in the process of relaxing, separate and relax not exclusively, occur the wooden dipper cocoon easily, the difficult quality of filature reaches quality standards, or can not carry out filature fully.Traditional in addition silk reeling technology be bright silk cocoon is separated through boiling easypro, filature and must become silk, in these processes, the pupa of living becomes dead pupa, economic benefit reduces greatly.
Summary of the invention
The object of the present invention is to provide the silk reeling technology of a kind of hollow cocoon, dry cocoon and living cocoon, with hollow cocoon, dry cocoon and the living cocoon that utilizes traditional silk reeling technology not make full use of, be processed into finished silk, to reach the purpose that makes full use of resource, energy savings and increase economic efficiency.
The technical solution adopted for the present invention to solve the technical problems is: a kind of hollow cocoon, dry cocoon and living cocoon silk reeling technology are provided, it is characterized in that hollow cocoon discarded and that store under lucifuge, ventilation and drying condition in the conventional machining process process, dry cocoon are separated easypro, filature, whirlwind and arranging process and finished by boiling bubble, medicine; Or the fresh living cocoon that will under lucifuge, ventilation and drying condition, store, separate easypro, filature, whirlwind and arrangement and the pupa manufacturing procedure of living is finished by water logging, medicine.
The concrete silk reeling technology of A, hollow cocoon and dry cocoon is:
A. boil bubble: the hollow cocoon or the dry cocoon of storage are poured vacuum tank into down with lucifuge, ventilation and drying condition, start vavuum pump, after being evacuated to 0.02-0.06Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into 80-100 ℃ hot water, the pH value of hot water is 7.0-8.0, inflow was advisable to soak silk cocoon 2-3 centimetre, soaked draining after 15 minutes, during control the hot water temperature between 80-95 ℃; According to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, repeat to vacuumize, water inlet and immersion process 1-5 time, until the silk cocoon state that reaches capacity that absorbs water;
B. medicine is separated easypro: according to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, adjust the composition and the control of separating the liquid that relaxes and separate easypro condition; Separating the liquid that relaxes consists of: the surfactant that adds 9-15kg sodium metasilicate, 6-14kg sodium carbonate, 0.6-1.5kg chilli oil, 0.6-1.5kg borax, 30-60kg hydrogen peroxide and 0.15-0.5kg in every 1000kg water respectively, form through mixed dissolution, separating the lyolysis of relaxing by every 100kg silk cocoon adding 200-250kg relaxes, hollow cocoon or dry cocoon are after 30-60 ℃ of following medicine separated easypro 20-70 minute, add the 6-7kg hydrogen peroxide by every 100kg silk cocoon, separate at 30-60 ℃ of following secondary and relaxed 20-30 minute;
C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature;
D. through rereeling and arrangement, be processed into silk.
B, the concrete silk reeling technology of living cocoon are:
A. water logging: the living cocoon that will store under lucifuge, ventilation and drying condition is poured vacuum tank into, start vavuum pump, after being evacuated to 0.02-0.06Mpa, close evacuating valve, open inlet valve, be drawn into 20-30 ℃ hot water in vacuum tank, the pH value of hot water is 7.0-8.0, and inflow was advisable to soak silk cocoon 2-3 centimetre; Water fully soaks draining after 0-4 hour under the room temperature; Perhaps utilize vacuum to be drawn into to separate the liquid that relaxes directly to carry out medicine and separate easypro;
B. medicine is separated easypro: according to living cocoon fibre weight size and silk gum convergence coagulation grade, adjust the composition and the control of separating the liquid that relaxes and separate easypro condition; Separating the liquid that relaxes consists of: the surfactant that adds 9-18kg sodium metasilicate, 6-15kg sodium carbonate, 0.6-2.0kg chilli oil, 0.6-2.5kg borax, 30-70kg hydrogen peroxide and 0.15-0.5kg in every 1000kg water respectively, form through mixed dissolution, add 200-250kg by every 100kg silk cocoon and separate easypro liquid, at room temperature medicine is separated and was relaxed 2-4 hour; Perhaps at room temperature medicine is separated and is relaxed after 2-4 hour, adds the 6-7kg hydrogen peroxide by every 100kg silk cocoon, and at room temperature secondary is separated and relaxed 20-30 minute;
C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature;
D. through rereeling and arrangement, be processed into silk;
E. the pupa of living is processed: pupa alive wherein is finished product through washing, low temperature drying.
Hollow cocoon provided by the present invention, dry cocoon and living cocoon silk reeling technology, hollow cocoon, the dry cocoon that traditional silk reeling technology can not be able to be made full use of are processed into the finished silk that meets QUALITY STANDARD, also can utilize living cocoon without hot digestion, carry out filature, not only play the effect of turning waste into wealth, and save time, laborsaving, energy savings, the pupa that can also obtain living is as commodity, economic benefit improves greatly, has remarkable economic efficiency and positive social benefit.
The invention will be further described below in conjunction with embodiment.
The specific embodiment
Embodiment 1. gets the hollow cocoon or the dry cocoon 100kg of storage under lucifuge, ventilation and the drying condition, by following working procedure processing: a. boils bubble: the hollow cocoon or the dry cocoon of storage are poured vacuum tank into down with lucifuge, ventilation and drying condition, start vavuum pump, after being evacuated to 0.04-0.06Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into 90-100 ℃ hot water, the pH value of hot water is 7.0-8.0, inflow was advisable to soak silk cocoon 2-3 centimetre, soak draining after 15 minutes, during control the hot water temperature between 80-95 ℃; According to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, repeat to vacuumize, water inlet and immersion process 1-5 time, until the silk cocoon state that reaches capacity that absorbs water; B. medicine is separated easypro: separate the liquid that relaxes and consist of: the alkyl sulfonic acid natrium surfactant that adds 9kg sodium metasilicate, 14kg sodium carbonate, 1.0kg chilli oil, 0.6kg borax, 45kg hydrogen peroxide and 0.3kg in every 1000kg water respectively, form through mixed dissolution, separating the lyolysis of relaxing by every 100kg silk cocoon adding 200kg relaxes, hollow cocoon or dry cocoon are after 60 ℃ of following medicines are separated easypro 20-40 minute, add the 6kg hydrogen peroxide by every 100kg silk cocoon, separate at 45 ℃ of following secondaries and relaxed 20-30 minute;
C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature;
D. through rereeling and arrangement, be processed into silk.
Finished silk detects through authoritative institution, and indexs such as silk intensity, obvolvent degree, fiber number, outward appearance and rough class reach more than the A level, meet national standard fully.
Embodiment 2. gets the living cocoon 100kg of storage under lucifuge, ventilation and the drying condition, by following working procedure processing: a. water logging: the living cocoon that will store under lucifuge, ventilation and drying condition is poured vacuum tank into, start vavuum pump, after being evacuated to 0.04-0.06Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into 20-30 ℃ hot water, the pH value of hot water is 7.0-8.0, and inflow was advisable to soak silk cocoon 2-3 centimetre; Water fully soaks draining after 0-4 hour under the room temperature; According to living cocoon fibre weight size and silk gum convergence coagulation grade, at room temperature water fully soaks draining after 4 hours; B. medicine is separated easypro: according to living cocoon fibre weight size and silk gum convergence coagulation grade, adjust the composition and the control of separating the liquid that relaxes and separate easypro condition; Separating the liquid that relaxes consists of: the pure ethers non-ionic surface active agent that adds 14kg sodium metasilicate, 6kg sodium carbonate, 1.3kg chilli oil, 1.5kg borax, 50kg hydrogen peroxide and 0.15kg in every 1000kg water respectively, form through mixed dissolution, separate the lyolysis of relaxing by every 100kg silk cocoon adding 250kg and relax, living cocoon at room temperature medicine was separated easypro 2-4 hour; C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature; D. through rereeling and arrangement, be processed into silk; E. the pupa of living is processed: pupa alive wherein is finished product through washing, low temperature drying.
Finished silk detects through authoritative institution, and indexs such as silk intensity, obvolvent degree, fiber number, outward appearance and rough class reach more than the A level, meet national standard fully.
Embodiment 3. gets the hollow cocoon or the dry cocoon 100kg of storage under lucifuge, ventilation and the drying condition, by following working procedure processing: a. boils bubble: the hollow cocoon or the dry cocoon of storage are poured vacuum tank into down with lucifuge, ventilation and drying condition, start vavuum pump, after being evacuated to 0.02-0.04Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into 80-90 ℃ hot water, the pH value of hot water is 7.0-8.0, inflow was advisable to soak silk cocoon 2-3 centimetre, soak draining after 15 minutes, during control the hot water temperature between 80-95 ℃; According to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, repeat to vacuumize, water inlet and immersion process 1-5 time, until the silk cocoon state that reaches capacity that absorbs water; B. medicine is separated easypro: separate the liquid that relaxes and consist of: the pure ethers non-ionic surface active agent that adds 15kg sodium metasilicate, 6kg sodium carbonate, 0.6kg chilli oil, 1.5kg borax, 30kg hydrogen peroxide and 0.15kg in every 1000kg water respectively, form through mixed dissolution, separating the lyolysis of relaxing by every 100kg silk cocoon adding 200kg relaxes, hollow cocoon or dry cocoon are after 45 ℃ of following medicines are separated easypro 40-50 minute, add the 7kg hydrogen peroxide by every 100kg silk cocoon, separate at 30 ℃ of following secondaries and relaxed 20-30 minute;
Finished silk detects through authoritative institution, and indexs such as silk intensity, obvolvent degree, fiber number, outward appearance and rough class reach more than the A level, meet national standard fully.
Embodiment 4. gets under lucifuge, ventilation and the drying condition hollow cocoon or the dry cocoon 100kg of storage, and by following working procedure processing: a. boils bubble: as embodiment 1; B. medicine is separated easypro: separate the liquid that relaxes and consist of: the alcohol ether sulfonate surfactant that adds 15kg sodium metasilicate, 13kg sodium carbonate, 1.5kg chilli oil, 1.5kg borax, 60kg hydrogen peroxide and 0.3kg in every 1000kg water respectively, form through mixed dissolution, separating the lyolysis of relaxing by every 00kg silk cocoon adding 220kg relaxes, hollow cocoon or dry cocoon are after 40-60 ℃ of following medicine separated easypro 20-30 minute, add the 6kg hydrogen peroxide by every 100kg silk cocoon, separate at 60 ℃ of following secondaries and relaxed 20-30 minute; C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature; D. through rereeling and arrangement, be processed into silk.Finished silk detects through authoritative institution, and indexs such as silk intensity, obvolvent degree, fiber number, outward appearance and rough class reach more than the A level, meet national standard fully.
Embodiment 5. gets the hollow cocoon or the dry cocoon 100kg of storage under lucifuge, ventilation and the drying condition, by following working procedure processing: a. boils bubble: the hollow cocoon or the dry cocoon of storage are poured vacuum tank into down with lucifuge, ventilation and drying condition, start vavuum pump, after being evacuated to 0.04-0.05Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into 85-95 ℃ hot water, the pH value of hot water is 7.0-8.0, inflow was advisable to soak silk cocoon 2-3 centimetre, soak draining after 15 minutes, during control the hot water temperature between 80-95 ℃; According to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, repeat to vacuumize, water inlet and immersion process 1-5 time, until the silk cocoon state that reaches capacity that absorbs water; B. medicine is separated easypro: separate the liquid that relaxes and consist of: the alcohol ether sulfonate surfactant that adds 12kg sodium metasilicate, 10kg sodium carbonate, 1.5kg chilli oil, 1.0kg borax, 60kg hydrogen peroxide and 0.5kg in every 1000kg water respectively, form through mixed dissolution, separate the lyolysis of relaxing by every 00kg silk cocoon adding 225kg and relax, hollow cocoon or dry cocoon are separated at 60 ℃ of following medicines and were relaxed 50-70 minute; C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature; D. through rereeling and arrangement, be processed into silk.
6. pairs of direct medicines of living cocoon of embodiment are separated easypro.Get the living cocoon 100kg of storage under lucifuge, ventilation and the drying condition, pour vacuum tank into by the living cocoon that following working procedure processing: a. will store under lucifuge, ventilation and drying condition, start vavuum pump, after being evacuated to 0.02-0.04Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into and separate easypro liquid; B. medicine is separated easypro: according to living cocoon fibre weight size and silk gum convergence coagulation grade, adjust the composition and the control of separating the liquid that relaxes and separate easypro condition; Separating the liquid that relaxes consists of: the pure ethers non-ionic surface active agent that adds 9kg sodium metasilicate, 15kg sodium carbonate, 2.0kg chilli oil, 2.5kg borax, 70kg hydrogen peroxide and 0.15kg in every 1000kg water respectively, form through mixed dissolution, add 200-250kg by every 100kg silk cocoon and separate easypro liquid, at room temperature medicine is separated and is relaxed after 2-4 hour, add the 6-7kg hydrogen peroxide by every 100kg silk cocoon, at room temperature secondary is separated and was relaxed 20-30 minute; C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature; D. through rereeling and arrangement, be processed into silk; E. the pupa of living is processed: pupa alive wherein is finished product through washing, low temperature drying.
Finished silk detects through authoritative institution, and indexs such as silk intensity, obvolvent degree, fiber number, outward appearance and rough class reach more than the A level, meet national standard fully.

Claims (1)

1. a hollow cocoon, dry cocoon and living cocoon silk reeling technology is characterized in that hollow cocoon discarded and that store under lucifuge, ventilation and drying condition in the conventional machining process process, dry cocoon are separated easypro, filature, whirlwind and arranging process and finished by boiling bubble, medicine; Or the fresh living cocoon that will under lucifuge, ventilation and drying condition, store, separate easypro, filature, whirlwind and arrangement and the pupa manufacturing procedure of living is finished by water logging, medicine;
The concrete silk reeling technology of A, hollow cocoon and dry cocoon is:
A. boil bubble: the hollow cocoon or the dry cocoon of storage are poured vacuum tank into down with lucifuge, ventilation and drying condition, start vavuum pump, after being evacuated to 0.02-0.06Mpa, close evacuating valve, open inlet valve, in vacuum tank, be drawn into 80-100 ℃ hot water, the pH value of hot water is 7.0-8.0, inflow was advisable to soak silk cocoon 2-3 centimetre, soaked draining after 15 minutes, during control the hot water temperature between 80-95 ℃; According to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, repeat to vacuumize, water inlet and immersion process 1-5 time, until the silk cocoon state that reaches capacity that absorbs water;
B. medicine is separated easypro: according to hollow cocoon or dry cocoon fibre weight size and silk gum convergence coagulation grade, adjust the composition and the control of separating the liquid that relaxes and separate easypro condition; Separating the liquid that relaxes consists of: the surfactant that adds 9-15kg sodium metasilicate, 6-14kg sodium carbonate, 0.6-1.5kg chilli oil, 0.6-1.5kg borax, 30-60kg hydrogen peroxide and 0.15-0.5kg in every 1000kg water respectively, form through mixed dissolution, separating the lyolysis of relaxing by every 100kg silk cocoon adding 200-250kg relaxes, hollow cocoon or dry cocoon are after 30-60 ℃ of following medicine separated easypro 20-70 minute, add the 6-7kg hydrogen peroxide by every 100kg silk cocoon, separate at 30-60 ℃ of following secondary and relaxed 20-30 minute;
C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature;
D. through rereeling and arrangement, be processed into silk;
B, the concrete silk reeling technology of living cocoon are:
A. water logging: the living cocoon that will store under lucifuge, ventilation and drying condition is poured vacuum tank into, start vavuum pump, after being evacuated to 0.02-0.06Mpa, close evacuating valve, open inlet valve, be drawn into 20-30 ℃ hot water in vacuum tank, the pH value of hot water is 7.0-8.0, and inflow was advisable to soak silk cocoon 2-3 centimetre; Water fully soaks draining after 0-4 hour under the room temperature; Perhaps utilize vacuum to be drawn into to separate the liquid that relaxes directly to carry out medicine and separate easypro;
B. medicine is separated easypro: according to living cocoon fibre weight size and silk gum convergence coagulation grade, adjust the composition and the control of separating the liquid that relaxes and separate easypro condition; Separating the liquid that relaxes consists of: the surfactant that adds 9-18kg sodium metasilicate, 6-15kg sodium carbonate, 0.6-2.0kg chilli oil, 0.6-2.5kg borax, 30-70kg hydrogen peroxide and 0.15-0.5kg in every 1000kg water respectively, form through mixed dissolution, add 200-250kg by every 100kg silk cocoon and separate easypro liquid, at room temperature medicine is separated and was relaxed 2-4 hour; Perhaps at room temperature medicine is separated and is relaxed after 2-4 hour, adds the 6-7kg hydrogen peroxide by every 100kg silk cocoon, and at room temperature secondary is separated and relaxed 20-30 minute;
C. take out and separate the silk cocoon that relaxes and finish, carry out artificial or mechanical filature;
D. through rereeling and arrangement, be processed into silk;
E. the pupa of living is processed: pupa alive wherein is finished product through washing, low temperature drying.
CNB2005100757489A 2004-06-07 2005-06-01 Silk reeling technology for hollow cocoon, dry solid cocoon and live pupa cocoon Expired - Fee Related CN100359049C (en)

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CNB2005100757489A CN100359049C (en) 2004-06-07 2005-06-01 Silk reeling technology for hollow cocoon, dry solid cocoon and live pupa cocoon

Applications Claiming Priority (3)

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CN 200410049419 CN1584134A (en) 2004-06-07 2004-06-07 Process for reeling hollow cocoons, dry cocoons or living cocoons
CN200410049419.2 2004-06-07
CNB2005100757489A CN100359049C (en) 2004-06-07 2005-06-01 Silk reeling technology for hollow cocoon, dry solid cocoon and live pupa cocoon

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CN1721589A true CN1721589A (en) 2006-01-18
CN100359049C CN100359049C (en) 2008-01-02

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102586896A (en) * 2012-01-11 2012-07-18 广西工学院 Novel cocoon cooking aid and its application
CN103132155A (en) * 2013-02-22 2013-06-05 广西立盛茧丝绸有限公司 Formula of soaking liquid improving cocoon reelability
CN103938278A (en) * 2014-04-23 2014-07-23 辽宁柞蚕丝绸科学研究院有限责任公司 Silk-reeling technology by utilization of tussah fresh cocoon live pupae
CN104480536A (en) * 2014-11-14 2015-04-01 安徽省广德新丰丝绸有限公司 Reeling agent for automatic silk reeling production
CN113265708A (en) * 2021-06-28 2021-08-17 四川依格尔纺织品有限公司 Tussah living cocoon reelability silk reeling process

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0735602B2 (en) * 1991-07-26 1995-04-19 佳男 新田 Prevention of abnormal fineness
JP2691499B2 (en) * 1993-04-14 1997-12-17 大日精化工業株式会社 Colored silk thread manufacturing method
CN1461828A (en) * 2002-05-30 2003-12-17 汤池 Method of rejecting secondary cocoon during silk reeling and using secondary cocoon produce silk floss
CN1280458C (en) * 2003-03-27 2006-10-18 成都天友发展有限公司 Method for refrigerating filature with no need of boiling cocoons
CN1272477C (en) * 2003-03-27 2006-08-30 成都天友发展有限公司 One step filature method for fresh cocoons of silkworms

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102586896A (en) * 2012-01-11 2012-07-18 广西工学院 Novel cocoon cooking aid and its application
CN102586896B (en) * 2012-01-11 2014-11-05 广西工学院 Novel cocoon cooking aid and its application
CN103132155A (en) * 2013-02-22 2013-06-05 广西立盛茧丝绸有限公司 Formula of soaking liquid improving cocoon reelability
CN103938278A (en) * 2014-04-23 2014-07-23 辽宁柞蚕丝绸科学研究院有限责任公司 Silk-reeling technology by utilization of tussah fresh cocoon live pupae
CN104480536A (en) * 2014-11-14 2015-04-01 安徽省广德新丰丝绸有限公司 Reeling agent for automatic silk reeling production
CN113265708A (en) * 2021-06-28 2021-08-17 四川依格尔纺织品有限公司 Tussah living cocoon reelability silk reeling process

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