CN1614409A - Simulating device for geophyscical gas hydrate - Google Patents

Simulating device for geophyscical gas hydrate Download PDF

Info

Publication number
CN1614409A
CN1614409A CN 200410036544 CN200410036544A CN1614409A CN 1614409 A CN1614409 A CN 1614409A CN 200410036544 CN200410036544 CN 200410036544 CN 200410036544 A CN200410036544 A CN 200410036544A CN 1614409 A CN1614409 A CN 1614409A
Authority
CN
China
Prior art keywords
autoclave
saturation water
gas hydrate
analogue means
geophysical exploration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 200410036544
Other languages
Chinese (zh)
Other versions
CN1317557C (en
Inventor
业渝光
张剑
刁少波
刘昌岭
林维正
程军
潘红良
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Institute of Marine Geology
Original Assignee
Qingdao Institute of Marine Geology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Institute of Marine Geology filed Critical Qingdao Institute of Marine Geology
Priority to CNB200410036544XA priority Critical patent/CN1317557C/en
Publication of CN1614409A publication Critical patent/CN1614409A/en
Application granted granted Critical
Publication of CN1317557C publication Critical patent/CN1317557C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Geophysics And Detection Of Objects (AREA)

Abstract

An analog device consists of high pressure reactor for placing core, ultrasonic detector, cooling device, time domain reflection detecting device set in the reactor, time domain reflection detector and TDR probe set in the detecting device of time domain reflection. In the same analog device, both saturation level and coustic parameter of air hydrate in the core can be detected.

Description

Gas hydrate geophysical exploration analogue means
Technical field
The present invention relates to the geophysical exploration analogue means, relate in particular to a kind of geophysical exploration analogue means of surveying the core gas hydrate.
Background technology
In geophysical probing technique, the estimation saturation degree of hydrate in the sediment hole with and and acoustic characteristic between relation be the important research content of gas hydrate geophysical exploration.03268815 utility model patent that on September 1st, 2004 was announced, a kind of landwaste acoustic velocity measurement mechanism is disclosed, it comprises supersonic reflectoscope, and it transmitting and receiving the upper and lower surface that probe is connected to core by the probe that transmits and receives of lead connection sound wave.In order to survey the saturation degree of hydrate in the sediment hole, the someone had proposed the Time Domain Reflectometry detection technique in recent years, and it comprises the Time Domain Reflectometry pick-up unit, and the TDR probe of this device is connected with core by metal.Existing sniffer or have only the supersonic sounding technology, has only the Time Domain Reflectometry detection technique, the result that single Detection Techniques detect produces deviation probably, can't accurately understand the correlativity between gas hydrate saturation degree and its acoustics parameters, and the result is difficult to mutual evidence.In addition, in sniffer, adopt the form of gaseous diffusion to make the gas in the core pore water saturated gradually, the time of being consumed is several weeks, even more than one month, has oversize problem experimental period.
Summary of the invention
The present invention designs in order to overcome above-mentioned defective, and one of its purpose provides a kind of geophysical exploration analogue means that can survey hydrate saturation degree and acoustic characteristic in the sediment, reduction experimental error simultaneously.
Two of purpose of the present invention is that a kind of geophysical exploration analogue means that shortens experimental period is provided simultaneously.
In order to reach the foregoing invention purpose, the present invention includes the autoclave, supersonic reflectoscope and the cooling device that are used to place core, wherein supersonic reflectoscope comprises ultrasonic emitting and the receiving transducer that lead connects, this probe is positioned at autoclave, autoclave is positioned at the temperature control bath of cooling device, and wherein supersonic reflectoscope connects computer processor unit; The Time Domain Reflectometry pick-up unit is set in autoclave, this device connects computer processor unit, and this Time Domain Reflectometry pick-up unit comprises Time Domain Reflectometry detector and TDR probe, and this TDR probe has two, central authorities that insert autoclave, another is a becket.
The inner core of being made by nonmetallic materials is set in the autoclave, and these nonmetallic materials can be teflon.At inner core inwall middle part draw-in groove is set, the corresponding embedding in this draw-in groove of described metal ring type TDR probe.
The described ultrasonic probe of this gas hydrate geophysical exploration analogue means is ripple integrated probe in length and breadth, and upper shed place that is positioned at inner core is in another embeds in the preformed hole of tube bottom.Thermocouple temperature sensor and the pressure transducer that links to each other with computer processor unit is set in autoclave; The thermopair of temperature sensor is arranged on the sidewall of inner core.
To achieve the above object of the invention, the present invention also comprises saturation water preparation facilities and gas pressue device, wherein between gas boosting device and saturation water preparation facilities and the autoclave, be connected by pipeline respectively between saturation water preparation facilities and the autoclave.
Described saturation water preparation facilities comprises that saturation water prepares still, magnetic stirring apparatus, thermocouple temperature sensor and pressure transducer, wherein saturation water prepares still and is communicated with autoclave by pipeline, valve is set on the pipeline, and the position that saturation water prepares still is higher than autoclave; The top that saturation water prepares still is provided with water inlet pipe and valve, and the bottom that saturation water prepares still is magnetic stirring apparatus fixedly; The thermocouple temperature sensor links to each other with computer processor unit with pressure transducer.The gas boosting device is communicated with saturation water respectively by three-way pipe and prepares still and autoclave, and three-way pipe and saturation water prepare valve is set respectively between still and the autoclave.
Adopt the gas hydrate geophysical exploration analogue means of this structure, can in same device, survey gas hydrate saturation degree and acoustics parameters in the core simultaneously, adopt gas saturation water technology of preparing simultaneously, it is few that whole experiment consumes the time, can shorten experimental period greatly.
Description of drawings
Fig. 1 is a structural representation of the present invention;
Fig. 2 is the partial enlarged drawing of Fig. 1;
1. gas boosting device; 2. cooling device; 3. computer processor unit; 4. temperature control bath; 5. saturation water prepares still; 6. autoclave; 7. inner core; 8. supersonic reflectoscope; 9. Time Domain Reflectometry detector; 10. pressure transducer; 11. temperature sensor; 12. ripple integrative ultrasonic ripple transmitting probe in length and breadth; 13. ripple integrative ultrasonic ripple receiving transducer in length and breadth; 14. thermopair; 15. thermopair; 16. core sample; 17. magnetic stirring apparatus; 18. metal ring type TDR probe; 19.TDR probe; 21. valve; 22. valve; 23. valve; 24. valve; 25. valve;
Embodiment
See Fig. 1,2, the present invention includes the autoclave 6, ultrasonic detection device, Time Domain Reflectometry pick-up unit, pressure transducer 10, temperature sensor 11, computer processor unit 3, cooling device 2, saturation water preparation facilities and the gas pressue device 1 that are used to place core, wherein the Time Domain Reflectometry pick-up unit comprises Time Domain Reflectometry detector 9 and two TDR probe 18,19, and ultrasonic detection device comprises supersonic reflectoscope 8 and ripple integrative ultrasonic ripple transmitting probe 12, receiving transducer 13 in length and breadth.Supersonic reflectoscope 8 all is connected with computer processor unit 3 with Time Domain Reflectometry detector 9, and autoclave is positioned at the temperature control bath 4 of cooling device, and the saturation water preparation facilities is connected with autoclave by pipeline with gas pressue device 1.Supersonic reflectoscope 8 and Time Domain Reflectometry detector 9 both can a shared cover computer processor unit, also can connect computer processor unit separately respectively.
The inner core of being made by teflon 7 is set in autoclave, it can realize contacting with the tight of sediment core, inner core inwall middle part is provided with draw-in groove, and described metal ring type TDR probe embeds in this draw-in groove, the core central authorities that another probe 19 inserts inner core; The described integrative ultrasonic of ripple in length and breadth ripple transmitting probe 12 is positioned at upper shed place of inner core, and ripple integrative ultrasonic ripple receiving transducer 13 embeds in the preformed hole of interior tube bottom in length and breadth.Thermocouple temperature sensor 11 and the pressure transducer 10 that links to each other with computer processor unit is set in autoclave; The thermopair 14,15 of temperature sensor is arranged on the routine wall of inner core.
Said structure can be implemented in the purpose of surveying gas hydrate saturation degree and acoustics parameters in the core in the same device simultaneously, thereby has effectively avoided the experimental error under the different experiments environment.
Saturation water preparation facilities of the present invention comprises that saturation water prepares still 5, magnetic stirring apparatus 17, thermocouple temperature sensor 11 and pressure transducer 10, wherein saturation water prepares still 5 and is communicated with autoclave 6 by pipeline, valve 24,25 is set on the pipeline, and the position that saturation water prepares still is higher than autoclave; Open valve 25, saturated aqueous solution injects in the autoclave by gravity.The top that saturation water prepares still is provided with water inlet pipe and valve 21, and magnetic stirring apparatus 17 is fixed on the bottom that saturation water prepares still; Thermocouple temperature sensor 11 links to each other with computer processor unit 3 with pressure transducer 10.The gas boosting device is communicated with saturation water respectively by three-way pipe and prepares still 5 and autoclave 6, and three-way pipe and saturation water prepare valve 22,23 is set respectively between still and the autoclave.Adopt this gas saturation water technology of preparing, can shorten experimental period greatly.
The course of work of the present invention is such, at first open autoclave 6 top covers, the core sample of being surveyed 16 is placed in the inner core 7 of autoclave, make it to closely cooperate with inner core, central authorities at core sample punching, then one of TDR probe that is connected with the Time Domain Reflectometry detector 19 is put into the medium pore of core sample 16, another lead fixed that will be connected with the Time Domain Reflectometry detector closes the autoclave top cover then on metal ring type TDR probe 18.Open valve 21, valve-off 25 injects valve-off 21 behind an amount of water.Open valve 22 and 24 prepares still 5 with saturation water and autoclave 6 is evacuated.Open valve 23 again, feed gas to certain pressure, and valve-off 22,23,24 starts magnetic stirring apparatus 17, and air water is fully contacted.Because gas dissolving is in aqueous solution, cause pressure to descend, said process no longer descends until pressure and makes saturated aqueous solution repeatedly.Open valve 25, saturated aqueous solution injects inner core 7 by gravity, soaks into valve-off 25 fully until core sample 16.Start cooling device 2 liquid are lowered the temperature gradually, start supersonic reflectoscope and Time Domain Reflectometry pick-up unit simultaneously, gather the data of the parameter of surveying in real time and handle by computer processing unit.According to requirement of experiment, the temperature and time that heats up and lower the temperature in the control temperature control bath 4.

Claims (10)

1. gas hydrate geophysical exploration analogue means, it comprises autoclave, supersonic reflectoscope and the cooling device that is used to place core, wherein supersonic reflectoscope comprises sound wave emissions and the receiving transducer that lead connects, this probe is positioned at autoclave, autoclave is positioned at the temperature control bath of cooling device, it is characterized in that, supersonic reflectoscope connects computer processor unit, the Time Domain Reflectometry pick-up unit is set in autoclave, and this device connects computer processor unit.
2. gas hydrate geophysical exploration analogue means according to claim 1 is characterized in that, the Time Domain Reflectometry pick-up unit comprises Time Domain Reflectometry detector and TDR probe, and this TDR probe is positioned at autoclave.
3. gas hydrate geophysical exploration analogue means according to claim 2 is characterized in that, the TDR probe of Time Domain Reflectometry pick-up unit has two, central authorities that insert autoclave, and another is a becket.
4. gas hydrate geophysical exploration analogue means according to claim 3 is characterized in that be provided for placing the inner core of core in the autoclave, it is made by nonmetallic materials, and the metal ring type probe of TDR is positioned on the inner core inwall.
5. gas hydrate geophysical exploration analogue means according to claim 4 is characterized in that inner core made by teflon, at the inwall middle part of inner core annular slot is set, and becket embeds in this draw-in groove.
6. gas hydrate geophysical exploration analogue means according to claim 1 is characterized in that, ultrasonic probe is ripple integrated probe in length and breadth, and upper shed place that is positioned at inner core is in another embeds in the preformed hole of tube bottom.
7. gas hydrate geophysical exploration analogue means according to claim 1 is characterized in that, thermocouple temperature sensor and the pressure transducer that links to each other with computer processor unit is set in autoclave; The thermopair of temperature sensor is arranged on the sidewall of inner core.
8. gas hydrate geophysical exploration analogue means according to claim 1, it is characterized in that, it also comprises saturation water preparation facilities and gas pressue device, wherein between gas boosting device and saturation water preparation facilities and the autoclave, be connected by pipeline respectively between saturation water preparation facilities and the autoclave.
9. gas hydrate geophysical exploration analogue means according to claim 8, it is characterized in that, the saturation water preparation facilities comprises that saturation water prepares still, magnetic stirring apparatus, thermocouple temperature sensor and pressure transducer, wherein saturation water prepares still and is communicated with autoclave by pipeline, valve is set on the pipeline, and the position that saturation water prepares still is higher than autoclave; The top that saturation water prepares still is provided with water inlet pipe and valve, and the bottom that saturation water prepares still is magnetic stirring apparatus fixedly; The thermocouple temperature sensor links to each other with computer processor unit with pressure transducer.
10. gas hydrate geophysical exploration analogue means according to claim 8, it is characterized in that, the gas boosting device is communicated with saturation water respectively by three-way pipe and prepares still and autoclave, and three-way pipe and saturation water prepare valve is set respectively between still and the autoclave.
CNB200410036544XA 2004-11-30 2004-11-30 Simulating device for geophyscical gas hydrate Expired - Fee Related CN1317557C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB200410036544XA CN1317557C (en) 2004-11-30 2004-11-30 Simulating device for geophyscical gas hydrate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB200410036544XA CN1317557C (en) 2004-11-30 2004-11-30 Simulating device for geophyscical gas hydrate

Publications (2)

Publication Number Publication Date
CN1614409A true CN1614409A (en) 2005-05-11
CN1317557C CN1317557C (en) 2007-05-23

Family

ID=34763576

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB200410036544XA Expired - Fee Related CN1317557C (en) 2004-11-30 2004-11-30 Simulating device for geophyscical gas hydrate

Country Status (1)

Country Link
CN (1) CN1317557C (en)

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101936833A (en) * 2010-07-21 2011-01-05 中国海洋石油总公司 Device and method for simulating generation of gas hydrate and measuring physical property parameters thereof
CN102042995A (en) * 2010-07-01 2011-05-04 青岛海洋地质研究所 Gas hydrate thermophysical property simulation experiment device
CN102052065A (en) * 2010-07-01 2011-05-11 青岛海洋地质研究所 Simulation exploiting experiment device for natural gas hydrate
CN102539521A (en) * 2010-12-08 2012-07-04 中国海洋石油总公司 Natural gas hydrate and drilling fluid interaction simulation test device
CN101071177B (en) * 2006-05-11 2012-08-22 普拉德研究及开发股份有限公司 Method and apparatus for locating gas hydrate
CN103424532A (en) * 2012-05-22 2013-12-04 青岛海洋地质研究所 Experiment device for researching structural characteristics of hydrate-containing deposit velocity profile
CN103424182A (en) * 2012-05-22 2013-12-04 青岛海洋地质研究所 Acoustic response characteristic simulation experiment set for seabed gas transfer and aquo-complex generation
CN103470220A (en) * 2013-08-20 2013-12-25 中国石油天然气股份有限公司 Natural gas hydrate simulation experiment apparatus
CN103698397A (en) * 2012-09-27 2014-04-02 中国石油化工股份有限公司 Ultrasonic detection system of quantitative contact pressure, and detection method thereof
CN105334547A (en) * 2015-09-23 2016-02-17 中国石油大学(华东) Simulated experiment testing system of gas hydrate in porous medium
WO2017050142A1 (en) * 2015-09-23 2017-03-30 中国石油大学(华东) Simulation experiment test system and test method for gas hydrates in porous medium
CN108776174A (en) * 2018-05-24 2018-11-09 大连理工大学 A kind of screw type acoustic measurement barge unit of core
CN109270577A (en) * 2018-11-12 2019-01-25 广州冷聚变电力科技有限公司 A kind of combustible ice diving detection device
CN110361420A (en) * 2018-12-10 2019-10-22 青岛海洋地质研究所 The test method of hydrate core sample

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102042947A (en) * 2010-07-01 2011-05-04 青岛海洋地质研究所 Natural gas hydrate permeability simulation experimental device
CN102042948A (en) * 2010-07-01 2011-05-04 青岛海洋地质研究所 Device for testing hydrate acoustic properties

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4243320A (en) * 1979-03-20 1981-01-06 Northern Telecom Limited Methods for testing optical fibres
CN2638064Y (en) * 2003-07-09 2004-09-01 石油大学(华东) Rock scraps sonic wave wave speed measuring device
CN2635201Y (en) * 2003-08-20 2004-08-25 青岛海洋地质研究所 Air hydrate preparation device

Cited By (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102789002B (en) * 2006-05-11 2017-04-19 普拉德研究及开发股份有限公司 Method and apparatus for locating gas hydrate
CN101071177B (en) * 2006-05-11 2012-08-22 普拉德研究及开发股份有限公司 Method and apparatus for locating gas hydrate
CN102789002A (en) * 2006-05-11 2012-11-21 普拉德研究及开发股份有限公司 Method and apparatus for locating gas hydrate
US9519072B2 (en) 2006-05-11 2016-12-13 Schlumberger Technology Corporation Method and apparatus for locating gas hydrate
CN102042995A (en) * 2010-07-01 2011-05-04 青岛海洋地质研究所 Gas hydrate thermophysical property simulation experiment device
CN102052065A (en) * 2010-07-01 2011-05-11 青岛海洋地质研究所 Simulation exploiting experiment device for natural gas hydrate
CN101936833A (en) * 2010-07-21 2011-01-05 中国海洋石油总公司 Device and method for simulating generation of gas hydrate and measuring physical property parameters thereof
CN101936833B (en) * 2010-07-21 2012-07-18 中国海洋石油总公司 Device and method for simulating generation of gas hydrate and measuring physical property parameters thereof
CN102539521B (en) * 2010-12-08 2014-03-12 中国海洋石油总公司 Natural gas hydrate and drilling fluid interaction simulation test device
CN102539521A (en) * 2010-12-08 2012-07-04 中国海洋石油总公司 Natural gas hydrate and drilling fluid interaction simulation test device
CN103424182B (en) * 2012-05-22 2015-10-28 青岛海洋地质研究所 The acoustic response characteristics analogue experiment installation of receive gas migration and gas hydrate synthesis
CN103424532A (en) * 2012-05-22 2013-12-04 青岛海洋地质研究所 Experiment device for researching structural characteristics of hydrate-containing deposit velocity profile
CN103424182A (en) * 2012-05-22 2013-12-04 青岛海洋地质研究所 Acoustic response characteristic simulation experiment set for seabed gas transfer and aquo-complex generation
CN103698397A (en) * 2012-09-27 2014-04-02 中国石油化工股份有限公司 Ultrasonic detection system of quantitative contact pressure, and detection method thereof
CN103698397B (en) * 2012-09-27 2015-11-18 中国石油化工股份有限公司 A kind of quantitatively contact ultrasonic wave detecting system and detection method thereof
CN103470220A (en) * 2013-08-20 2013-12-25 中国石油天然气股份有限公司 Natural gas hydrate simulation experiment apparatus
CN103470220B (en) * 2013-08-20 2015-12-02 中国石油天然气股份有限公司 Gas hydrates analogue experiment installation
CN105334547A (en) * 2015-09-23 2016-02-17 中国石油大学(华东) Simulated experiment testing system of gas hydrate in porous medium
WO2017050142A1 (en) * 2015-09-23 2017-03-30 中国石油大学(华东) Simulation experiment test system and test method for gas hydrates in porous medium
US9897529B2 (en) 2015-09-23 2018-02-20 China University Of Petroleum (East China) Test system and test method for a simulation experiment of gas hydrate in a porous medium
CN108776174A (en) * 2018-05-24 2018-11-09 大连理工大学 A kind of screw type acoustic measurement barge unit of core
CN109270577A (en) * 2018-11-12 2019-01-25 广州冷聚变电力科技有限公司 A kind of combustible ice diving detection device
CN110361420A (en) * 2018-12-10 2019-10-22 青岛海洋地质研究所 The test method of hydrate core sample

Also Published As

Publication number Publication date
CN1317557C (en) 2007-05-23

Similar Documents

Publication Publication Date Title
CN1317557C (en) Simulating device for geophyscical gas hydrate
CN101936833B (en) Device and method for simulating generation of gas hydrate and measuring physical property parameters thereof
CN108106965A (en) A kind of seabed sediment acoustics and physical parameter in-situ synchronization measuring device and method
CN106556687B (en) Weak cementing non-diagenesis hydrate acoustics and saturation degree synchronous testing device and method
WO2017050142A1 (en) Simulation experiment test system and test method for gas hydrates in porous medium
JP6758585B2 (en) In-situ test equipment and methods for detecting the amount of internal contaminants released in seafloor sediments by simulating wave action.
CN111812711B (en) Hydrate stratum seismic physical simulation test equipment based on reflection wave field
CN105589111B (en) Measure the wave speed of the earthquake of deposition medium containing hydrate and the device and method of electromagnetic attenuation
EP1733178A2 (en) System and method for generating three-dimensional density-based defect map
CN101376854A (en) Method and apparatus for simulating gas hydrate accumulation process under three-dimensional condition
CN103470220B (en) Gas hydrates analogue experiment installation
CN103424182B (en) The acoustic response characteristics analogue experiment installation of receive gas migration and gas hydrate synthesis
CN210834784U (en) Hydrate core sample preparation and resistance imaging and acoustic wave combined detection device thereof
CN106645421A (en) Bottom sediment acoustics in-situ measurement and synchronous sampling device and method
CN207586187U (en) The storage tank bottom plate universe detecting system of main passive sound fusion
CN207675586U (en) A kind of seabed sediment acoustics and physical parameter in-situ synchronization measuring device
CN201749073U (en) Hydrate acoustical characteristic testing device
CN117214294A (en) Ultrasonic guided wave detection device for pipeline damage and three-dimensional reconstruction method for damage signal of ultrasonic guided wave detection device
CN102042948A (en) Device for testing hydrate acoustic properties
CN202676668U (en) Self-adaptive device for sound response simulation experiment of hydrates in samples of different sizes
CN112198232A (en) Drainage pipeline working condition detection and identification method
CN103424532B (en) Containing the experimental provision of hydrate sediment velocities cross-section structure characteristic research
CN115980758A (en) Mud line position tester integrated in seabed in-situ equipment and identification method
CN114216961A (en) Hydrate-containing sediment low-frequency acoustic detection device and test method
CN202661164U (en) Device for performing simulation experiment of acoustic response characteristic in seabed gas movement and hydrate formation

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20070523

Termination date: 20111130