CN1563236A - Brightening agent for vehicle without water washing, and preparation method - Google Patents
Brightening agent for vehicle without water washing, and preparation method Download PDFInfo
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- CN1563236A CN1563236A CN 200410033974 CN200410033974A CN1563236A CN 1563236 A CN1563236 A CN 1563236A CN 200410033974 CN200410033974 CN 200410033974 CN 200410033974 A CN200410033974 A CN 200410033974A CN 1563236 A CN1563236 A CN 1563236A
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Abstract
A type of anhydrous car washing polish agent is prepared from wax polish, emulsifier, solvent naphtha, oleic acid, additive and distilled water of which emulsified is made of nonylphenol polyethenoxy ether dehydrosorbito oleate polyethenoxy ether -80 or -60 and TA-20 emulsifier. The preparation method is included in operation manual.
Description
Technical field
The present invention relates to a kind of novel waterless carwash special product, specifically, relate to a kind of waterless carwash brightening agent, also relate to the preparation method of this waterless carwash brightening agent.
Background technology
Show according to pertinent data, automobile quantity increases substantially rapidly at present, having driven with automobile cleaning, beauty services is the emergence of the industry of content, and we are astronomical figures because of cleaning the used up water resources of automobile every year, and China is the country of the serious scarcity of a water resources.Be the restriction car washing water, country puts into effect multinomial rules such as Water Law in succession.For meeting China's present situation, must once reform and innovate up hill and dale in the carwash field---and developing a kind of not water can clean up car, and finishes the waterless carwash special product of waxing, glazing function simultaneously.
At present, commercial automobile polish, based on solid wax, only several liquid waxs, as brightening agent, liquid wax, the cleaning and polishing performance of corresponding product is bad, and easily layering, easy caking, volatile, and the stability of product is also relatively poor.Therefore, need a kind of cleaning and polishing of exploitation effective, the waterless carwash brightening agent that emulsifying property and stability are good.
Summary of the invention
An object of the present invention is to provide a kind of have high emulsibility more can and the waterless carwash brightening agent of stability.
Another object of the present invention provides a kind of preparation method of waterless carwash brightening agent.
For achieving the above object, a technical scheme of the present invention provides a kind of waterless carwash brightening agent, this waterless carwash brightening agent comprises that concentration is the polishing wax of 2～5.5wt%, the emulsifying agent of 1～3.5wt%, 4.5 the solvent oil of～12.5wt%, 0.8 the oleic acid of～2.5wt%, all the other components are additive and distilled water, described emulsifying agent comprises that concentration is the polyoxyethylene nonylphenol ether of 0.1～1.2wt%, the sorbitan monooleate Soxylat A 25-7-80 of 0～2wt% or sorbitan monooleate Soxylat A 25-7-60 comprise that also concentration is the TA-20 emulsifying agent (Henkel KGaA grease chemical article company product) of 0.3～1.5wt%.
Adopting concentration at polishing wax described in the technique scheme of the present invention is three kinds of any two kinds or they in the beeswax of river wax, 0～2.5wt% of carnauba wax, the 0～3.5wt% of 0～2wt%, described solvent oil is the petroleum fractions of boiling range in the kerosene scope, and the boiling range scope of described kerosene is 110～350 ℃.
At additive described in the technique scheme of the present invention is that the trolamine of 0～2wt%, the macromolecule resin of 0～4wt% and the sanitas of 0～0.2wt% are formed by concentration mainly, described macromolecule resin adopts methyl-silicone oil or RHODORSILEIP emulsion (NCM's product), and described sanitas adopts Tegosept M, ethyl p-hydroxybenzoate or Kai Feng-88 (mixture of 2-methyl-4 isothiazoline-3 ketone and 5-chlorine 2-methyl-4 isothiazoline-3 ketone).
Also comprise an amount of spices at waterless carwash brightening agent described in the technical scheme of the present invention, described spices odor type is as requested chosen, such as lemon flavour, apple flavour etc.
Waterless carwash brightening agent provided by the invention has the following advantages:
1. in the waterless carwash brightening agent, added the TA-20 emulsifying agent, the waterless carwash brightening agent of production can be existed with the form of a stable emulsion, improve the emulsifying property and the stability of waterless carwash brightening agent, thereby overcome the poor stability of currently available products emulsion, easy stratified shortcoming;
2. additive---macromolecule resin can be described as the cere protective material, and its existence has increased the hardness and the wear resistance of the wax protective membrane of brightening agent formation; The existence of additive---trolamine makes the dissolving of each component and dissolves each other and becomes easier.
For achieving the above object, another technical scheme of the present invention provides a kind of preparation method of waterless carwash brightening agent, and this method may further comprise the steps:
1. distilled water is added in the reactor 1, open to stir, with steam or oil bath indirect heating distilled water to 30～60 ℃, then emulsifying agent is added in the reactor 1 under constantly stirring it is dissolved fully, and uniform mixing liquid is warming up to 75～95 ℃;
2. solvent oil is added in the reactor 2, open and stir, with steam, oil bath or water-bath indirect heating to 20～40 ℃, then polishing wax being added in the reactor 2 under constantly stirring dissolves it fully, in the adding reactor 2 it is dissolved fully under constantly stirring oleic acid again, temperature remains on 40～60 ℃ during the reinforced stirring and dissolving;
3. the 2. prepared uniform mixing liquid of above-mentioned steps being added above-mentioned steps 1. is equipped with in the reaction ax 1 of obtained uniform mixing liquid, constantly stir and make mixeding liquid temperature be increased to 80～90 ℃, with colloidal mill polishing mixed solution 10～20min with steam or oil bath indirect heating;
4. discharging, standard pack finished product according to the rules.
Step described in the technique scheme of the present invention 1. in, it is dissolved fully under constantly stirring, adding the additive trolamine behind the dissolved emulsifier; Described step 2. in, it is dissolved fully under constantly stirring, adding the additive macromolecule resin behind the dissolving polishing wax; Described step 3. in, after colloidal mill polishing mixed solution, add the sanitas 5～10min that polishes again, add spices again.
The preparation method of waterless carwash brightening agent provided by the invention has the following advantages:
Oleic acid is joined in the solvent oil in 2. in preparation method's step of the present invention, make its easier dissolving, also make it easily miscible, thereby overcome in the prior art the first defective that oleic acid and trolamine is joined the easy chromatography of oleic acid in the aqueous solution in the preparation waterless carwash brightening agent with other compositions.
Embodiment
The preferred waterless carwash brightening agent of the present invention mainly is made up of polishing wax, emulsifying agent, solvent oil, oleic acid, additive, sanitas and spices, all the other components are distilled water, and described polishing wax is that any two kinds or they in the beeswax of river wax, 0.3～1wt% of carnauba wax, the 1～2wt% of 0.5～1.5wt% are formed for three kinds by preferred concentration; Comprise in the described emulsifying agent that preferred concentration is the polyoxyethylene nonylphenol ether (hereinafter to be referred as TX-10) of 0.2～0.8wt%, sorbitan monooleate Soxylat A 25-7-80 (hereinafter to be referred as tween-80) or the sorbitan monooleate Soxylat A 25-7-60 (hereinafter to be referred as Tween-60) of 0.2～1.5wt%, comprise that also preferred concentration is the TA-20 emulsifying agent (hereinafter to be referred as TA-20) of 0.5～1wt%; Described solvent oil is the petroleum fractions of boiling range in kerosene scope (110～350 ℃), and preferred concentration is 6～8wt%; Described oleic preferred concentration is 1～2wt%; Described additive is that the trolamine of 0.25～1.5wt%, the macromolecule resin of 0.9～1.5wt% are formed by preferred concentration, adopts methyl-silicone oil or RHODORSIL EIP emulsion; The preferred concentration of described sanitas is 0.07～0.15wt%, adopts Tegosept M, ethyl p-hydroxybenzoate or Kai Feng-88 (mixture of 2-methyl-4 isothiazoline-3 ketone and 5-chlorine 2-methyl-4 isothiazoline-3 ketone); Described spices odor type is as requested chosen, such as lemon flavour, apple flavour etc.
The preparation method of above-mentioned preferred waterless carwash brightening agent is elaborated as follows:
1. distilled water is added in the reactor 1, open and stir, with steam or oil bath indirect heating distilled water to 30～60 ℃, successively TA-20, tween-80 (or Tween-60), TX-10 being added in the reactor 1 under constantly stirring then dissolves it fully, under constantly stirring, in the adding reactor 1 it is dissolved fully the additive trolamine again, and uniform mixing liquid is warming up to 75～95 ℃;
2. solvent oil is added in the reactor 2, open and stir, with steam, oil bath or water-bath indirect heating to 20～40 ℃, successively river wax, beeswax, carnauba wax being added in the reactor 2 under constantly stirring then dissolves it fully, additive macromolecule resin (methyl-silicone oil or RHODORSIL EIP emulsion) being added in the reactor 2 under constantly stirring dissolves it fully again, in the adding reactor 2 it is dissolved fully under constantly stirring oleic acid again, temperature remains on 40～60 ℃ during the reinforced stirring and dissolving;
3. the 2. prepared uniform mixing liquid of above-mentioned steps being added above-mentioned steps 1. is equipped with in the reaction ax 1 of obtained uniform mixing liquid, constantly stir and elevate the temperature to 80～90 ℃, with colloidal mill polishing mixed solution 10～20min, add the 5～10min that polishes again after the sanitas (Tegosept M, ethyl p-hydroxybenzoate or Kai Feng-88), add spices again;
4. discharging, standard pack finished product according to the rules.
Embodiment 1
1. 338.64kg distilled water is added in 500 liters of reactors 1, open and stir, with steam indirect heating distilled water to 40 ℃, successively 3.12kgTA-20,1.52kg tween-80,1.52kgTX-10 being added in the reactor 1 under constantly stirring then dissolves it fully, under constantly stirring, in the adding reactor 1 it is dissolved fully the 1.84kg trolamine again, and uniform mixing liquid is warming up to 85 ℃;
2. the 30.84kg200# solvent oil is added in 100 liters of reactors 2, open and stir, with steam indirect heating to 30 ℃, successively 5kg river wax, 2.32kg beeswax, 3.12kg carnauba wax being added in the reactor 2 under constantly stirring then dissolves it fully, the 5kg methyl-silicone oil being added in the reactor 2 under constantly stirring dissolves it fully again, in the adding reactor 2 it is dissolved fully under constantly stirring 5.68kg oleic acid again, temperature remains on 50 ℃ during the reinforced stirring and dissolving;
3. the 2. prepared uniform mixing liquid of above-mentioned steps being added above-mentioned steps 1. is equipped with in the reaction ax 1 of obtained uniform mixing liquid, constantly stir and elevate the temperature to 85 ℃, with colloidal mill polishing mixed solution 15min, add the 5min that polishes again behind the 0.4kg sanitas Tegosept M, add the 1kg lemon flavour again;
4. discharging, standard pack finished product according to the rules.
The composition of the waterless carwash brightening agent that present embodiment is prepared is as shown in table 1:
Table 1.
| Component | Raw material | Manufacturer | Concentration/wt% |
| Glazing is cured | Carnauba wax | The big letter of Beijing member of Imperial Academy Chinese workers company limited | ????0.78 |
| River wax | The Beijing Bee Products Co | ????1.25 | |
| Beeswax | The Beijing Bee Products Co | ????0.58 | |
| Emulsifying agent | ??????TX-10 | Xinghua, sky, Jiangsu worker company limited | ????0.38 |
| Tween-80 | Nanjing prestige and chemical industry company limited | ????0.38 | |
| ??????TA-20 | Henkel KGaA grease chemical article company | ????0.78 | |
| Solvent oil | ?200#(140～200℃) | Qilu Petrochemical | ????7.71 |
| Oleic acid | The Beijing Chemical Plant | ????1.42 | |
| Additive | Trolamine | The big letter of Beijing member of Imperial Academy Chinese workers company limited | ????0.46 |
| Methyl-silicone oil | Henkel KGaA grease chemical article company | ????1.25 | |
| Sanitas | Tegosept M | Source chemical company is thought in the Shanghai Communications University, Xi'an | ????0.10 |
| Spices | Lemon flavour | Beijing beautiful prosperous chemical industry difficult to understand | ????0.25 |
| Distilled water | Self-control | ????84.66 | |
Embodiment 2～10
With preparing the waterless carwash brightening agent with embodiment 1 same method, the composition of the waterless carwash brightening agent that embodiment 2～10 is prepared is as shown in table 2:
Table 2.
| Component | Raw material | Manufacturer | Embodiment 2 (concentration/wt%) | Embodiment 3 (concentration/wt%) | Embodiment 4 (concentration/wt%) | Embodiment 5 (concentration/wt%) | Embodiment 6 (concentration/wt%) | Embodiment 7 (concentration/wt%) | Embodiment 8 (concentration/wt%) | Embodiment 9 (concentration/wt%) | Embodiment 10 (concentration/wt%) | |
| Glazing is cured | Carnauba wax | The big letter of Beijing member of Imperial Academy Chinese workers company limited | ????0.50 | ????1.20 | ????0.33 | ????1.50 | ????0.90 | |||||
| River wax | The Beijing Bee Products Co | ????1.75 | ????2.00 | ????2.22 | ????0.80 | ????3.50 | ????3.50 | ????1.50 | ????3.00 | |||
| Beeswax | The Beijing Bee Products Co | ????1.00 | ????2.00 | ????1.55 | ????1.67 | ????0.30 | ????2.50 | ????0.70 | ????1.00 | |||
| Emulsifying agent | ??????TX-10 | Xinghua, sky, Jiangsu worker company limited | ????0.76 | ????1.00 | ????1.20 | ????0.10 | ????1.20 | ????0.80 | ????0.50 | ????0.90 | ????0.50 | |
| Tween-80 | Nanjing prestige and chemical industry company limited | ????0.50 | ????0.80 | ????0.20 | ????1.50 | |||||||
| Tween-60 | Nanjing prestige and chemical industry company limited | ????0.20 | ????1.00 | |||||||||
| ??????TA-20 | Henkel KGaA grease chemical article company | ????0.88 | ????1.00 | ????1.20 | ????1.50 | ????1.50 | ????0.30 | ????0.50 | ????0.30 | ????1.50 | ||
| Solvent oil | ??200#(140～200℃) | Qilu Petrochemical | ????8.00 | ????10.00 | ????8.50 | ????8.90 | ????4.50 | ????6.00 | ????12.50 | |||
| Kerosene (110～350 ℃) | Qilu Petrochemical | ????5.50 | ????6.50 | |||||||||
| Oleic acid | The Beijing Chemical Plant | ????1.50 | ????0.80 | ????1.00 | ????0.80 | ????2.50 | ????1.20 | ????2.00 | ????0.80 | ????2.50 | ||
| Additive | Trolamine | The big letter of Beijing member of Imperial Academy Chinese workers company limited | ????0.56 | ????1.12 | ????0.80 | ????1.90 | ????0.30 | ????1.50 | ????2.00 | |||
| Macromolecule resin | Methyl-silicone oil | Henkel KGaA grease chemical article company | ????1.50 | ????0.80 | ????0.10 | ????1.00 | ????0.90 | |||||
| RHODORSIL EIP emulsion | NCM | ????4.00 | ????3.00 | ????4.00 | ||||||||
| Sanitas | Tegosept M | Source chemical company is thought in the Shanghai Communications University, Xi'an | ????0.20 | ????0.10 | ????0.10 | ????0.20 | ????0.15 | ????0.20 | ||||
| Ethyl p-hydroxybenzoate | Source chemical company is thought in the Shanghai Communications University, Xi'an | ????0.10 | ||||||||||
| Kai Feng-88 | Source chemical company is thought in the Shanghai Communications University, Xi'an | ????0.10 | ||||||||||
| Spices | Lemon flavour | Beijing beautiful prosperous chemical industry difficult to understand | ????0.10 | ????0.12 | ????0.20 | ????0.30 | ????0.40 | ????0.25 | ????0.40 | |||
| Distilled water | Self-control | ????83.75 | ????81.20 | ????82.89 | ????84.80 | ????74.20 | ????85.50 | ????84.70 | ????89.80 | ????70.00 | ||
Existing waterless carwash brightening agent product keeps at most demixing phenomenon will occurring in 2～3 days, and the waterless carwash brightening agent of the embodiment of the invention 1～10 preparation can keep the stability in 1 year.
Although describe the present invention in conjunction with the preferred embodiments, but the present invention is not limited to the foregoing description and accompanying drawing, should be appreciated that, under the guiding of the present invention's design, those skilled in the art can carry out various modifications and improvement, and claims have been summarized scope of the present invention.
Claims (10)
1. waterless carwash brightening agent, this waterless carwash brightening agent comprises that concentration is the polishing wax of 2～5.5wt%, the emulsifying agent of 1～3.5wt%, the solvent oil of 4.5～12.5wt%, the oleic acid of 0.8～2.5wt%, all the other components are additive and distilled water, described emulsifying agent comprises that concentration is the polyoxyethylene nonylphenol ether of 0.1～1.2wt%, sorbitan monooleate Soxylat A 25-7-80 or the sorbitan monooleate Soxylat A 25-7-60 of 0～2wt%, comprises that also concentration is the TA-20 emulsifying agent of 0.3～1.5wt%.
2. waterless carwash brightening agent according to claim 1 is characterized in that, it is three kinds of any two kinds or they in the beeswax of river wax, 0～2.5wt% of carnauba wax, the 0～3.5wt% of 0～2wt% that described polishing wax adopts concentration.
3. waterless carwash brightening agent according to claim 1 is characterized in that, described solvent oil is the petroleum fractions of boiling range in the kerosene scope.
4. waterless carwash brightening agent according to claim 1 is characterized in that, described additive is that the trolamine of 0～2wt%, the macromolecule resin of 0～4wt% and the sanitas of 0～0.2wt% are formed by concentration mainly.
5. according to claim 1 or 4 described waterless carwash brightening agents, it is characterized in that described macromolecule resin adopts methyl-silicone oil or RHODORSIL EIP emulsion, described sanitas adopts Tegosept M, ethyl p-hydroxybenzoate or Kai Feng-88.
6. according to the described waterless carwash brightening agent of one of claim 1 to 5, it is characterized in that, described waterless carwash brightening agent comprises that concentration is the carnauba wax of 0.5～1.5wt%, the river wax of 1～2wt%, 0.3 the beeswax of～1wt%, 0.2 the polyoxyethylene nonylphenol ether of～0.8wt%, 0.2 the sorbitan monooleate Soxylat A 25-7-80 of～1.5wt% or sorbitan monooleate Soxylat A 25-7-60,0.5 the TA-20 emulsifying agent of～1wt%, the solvent oil of 6～8wt%, the oleic acid of 1～2wt%, 0.25 the trolamine of～1.5wt%, 0.9 the macromolecule resin of～1.5wt%, 0.07～0.15wt% sanitas, all the other components are distilled water.
7. method for preparing the described waterless carwash brightening agent of claim 1, this method may further comprise the steps:
1. distilled water is added in the reactor 1, open to stir, with steam or oil bath indirect heating distilled water to 30～60 ℃, then emulsifying agent is added in the reactor 1 under constantly stirring it is dissolved fully, and uniform mixing liquid is warming up to 75～95 ℃;
2. solvent oil is added in the reactor 2, open and stir, with steam, oil bath or water-bath indirect heating to 20～40 ℃, then polishing wax being added in the reactor 2 under constantly stirring dissolves it fully, in the adding reactor 2 it is dissolved fully under constantly stirring oleic acid again, temperature remains on 40～60 ℃ during the reinforced stirring and dissolving;
3. the 2. prepared uniform mixing liquid of above-mentioned steps being added above-mentioned steps 1. is equipped with in the reaction ax 1 of obtained uniform mixing liquid, constantly stir and make mixeding liquid temperature be increased to 80～90 ℃, with colloidal mill polishing mixed solution 10～20min with steam or oil bath indirect heating;
4. discharging, standard pack finished product according to the rules.
8. the preparation method of waterless carwash brightening agent according to claim 7 is characterized in that, described step dissolves it adding the additive trolamine behind the dissolved emulsifier under constantly stirring in 1. fully.
9. the preparation method of waterless carwash brightening agent according to claim 7 is characterized in that, described step dissolves it adding the additive macromolecule resin behind the dissolving polishing wax under constantly stirring in 2. fully.
10. the preparation method of waterless carwash brightening agent according to claim 7 is characterized in that, described step adds the sanitas 5～10min that polishes again in 3. after colloidal mill polishing mixed solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410033974 CN1245490C (en) | 2004-04-22 | 2004-04-22 | Brightening agent for vehicle without water washing, and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410033974 CN1245490C (en) | 2004-04-22 | 2004-04-22 | Brightening agent for vehicle without water washing, and preparation method |
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| CN1563236A true CN1563236A (en) | 2005-01-12 |
| CN1245490C CN1245490C (en) | 2006-03-15 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 200410033974 Expired - Fee Related CN1245490C (en) | 2004-04-22 | 2004-04-22 | Brightening agent for vehicle without water washing, and preparation method |
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