CN1561827A - Method for producing powder blood fat - Google Patents
Method for producing powder blood fat Download PDFInfo
- Publication number
- CN1561827A CN1561827A CNA2004100311717A CN200410031171A CN1561827A CN 1561827 A CN1561827 A CN 1561827A CN A2004100311717 A CNA2004100311717 A CN A2004100311717A CN 200410031171 A CN200410031171 A CN 200410031171A CN 1561827 A CN1561827 A CN 1561827A
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- Prior art keywords
- blood
- grease
- fat
- hemoglobin
- adds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 210000004369 blood Anatomy 0.000 title claims abstract description 56
- 239000008280 blood Substances 0.000 title claims abstract description 56
- 239000000843 powder Substances 0.000 title claims description 23
- 238000004519 manufacturing process Methods 0.000 title claims description 16
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 12
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 12
- 238000001694 spray drying Methods 0.000 claims abstract description 9
- 239000004519 grease Substances 0.000 claims description 35
- 239000000463 material Substances 0.000 claims description 19
- 102000001554 Hemoglobins Human genes 0.000 claims description 18
- 108010054147 Hemoglobins Proteins 0.000 claims description 18
- 239000003995 emulsifying agent Substances 0.000 claims description 18
- 244000144977 poultry Species 0.000 claims description 15
- 244000144972 livestock Species 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 239000001509 sodium citrate Substances 0.000 claims description 6
- -1 sucrose ester Chemical class 0.000 claims description 6
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims description 6
- 229940038773 trisodium citrate Drugs 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 239000003094 microcapsule Substances 0.000 claims description 5
- 239000003146 anticoagulant agent Substances 0.000 claims description 4
- 229940127219 anticoagulant drug Drugs 0.000 claims description 4
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 3
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- 229920002774 Maltodextrin Polymers 0.000 claims description 3
- 239000005913 Maltodextrin Substances 0.000 claims description 3
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 3
- 241000238370 Sepia Species 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 229930006000 Sucrose Natural products 0.000 claims description 3
- 150000001733 carboxylic acid esters Chemical class 0.000 claims description 3
- 238000004945 emulsification Methods 0.000 claims description 3
- 239000003205 fragrance Substances 0.000 claims description 3
- 229940035034 maltodextrin Drugs 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 239000005720 sucrose Substances 0.000 claims description 3
- 238000010257 thawing Methods 0.000 claims description 2
- 235000018102 proteins Nutrition 0.000 abstract description 10
- 230000001804 emulsifying effect Effects 0.000 abstract description 5
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 abstract description 4
- 235000013619 trace mineral Nutrition 0.000 abstract description 3
- 239000011573 trace mineral Substances 0.000 abstract description 3
- 235000019766 L-Lysine Nutrition 0.000 abstract description 2
- 239000004472 Lysine Substances 0.000 abstract description 2
- 241000272496 Galliformes Species 0.000 abstract 1
- 241001465754 Metazoa Species 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 235000013372 meat Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 235000013305 food Nutrition 0.000 description 4
- 238000009413 insulation Methods 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 239000005996 Blood meal Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 235000013622 meat product Nutrition 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 238000003307 slaughter Methods 0.000 description 2
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 244000208060 Lawsonia inermis Species 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 235000013527 bean curd Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000010836 blood and blood product Substances 0.000 description 1
- 229940125691 blood product Drugs 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 210000003743 erythrocyte Anatomy 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 235000015277 pork Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000013580 sausages Nutrition 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Landscapes
- Fodder In General (AREA)
- Meat, Egg Or Seafood Products (AREA)
Abstract
A powdered blood fat as the additiv of feed is prepared from the blood of domestic animals and fowls, haematoglobin and oil through proportionally mixing, emulsifying for coating oil, and spray drying. It is rich in trace elements, protein and L-lysine.
Description
Technical field
The invention belongs to the manufacturing technology scope of additive.Be particularly related to the production method of making a kind of powder blood fat of food, feed addictive with livestock and poultry blood, hemoglobin and grease.
Background technology
Raising along with living standards of the people, the form of meat products is variation, the informal voucher meat production is on a declining curve, meat product, the chilled meat goods of cutting apart packing become that meat is sold and the principal mode of outlet, certainly will bring raw materials such as the leaf fat that is rich in grease, streaky pork, fat meat, lower abdomen meat more concentrated overstocked like this.Overstocked and higher its economic benefit of raising that solves grease is a difficult problem in current slaughterhouse.Blood is byproduct main in the livestock and poultry slaughtering process, is rich in protein and trace element etc.In recent years, the development of the poultry industry of China is very fast, and the quantity of slaughterhouse and scale, automaticity all have very big development.Remove a part and be made for feed with blood meal, a part is done outside the blood bean curd, and all the other major parts are discharged with the sewage form.Blood is increased to original ten times as directly pouring sewer with the BOD that makes sewage, and solid content is increased to original three times more than.Therefore, expand the livestock and poultry blood Products Development, not only can avoid a large amount of precious resources to run off, alleviate environmental pollution, also can increase economic benefit.In CN 1048487A, mainly be to utilize leftover bits and pieces and blood slag, simply mix behind the dewatered drying, though nutrition balance relatively, grease is not easy and other mixing of materials, and grease directly is exposed in the air, and is putrid and deteriorated easily.In CN 1463632A, utilize blood to make ripe blood meal, and then make capsule 150～350 ℃ of heated-air dryings.The elaioleucite come-up can cause the difficulty that product quality is uneven and increasing is dry in spray-drying.The production technology of reference powder grease of the present invention adopts microcapsules technology, makes the wall material with the protein that is rich in the blood fat is carried out embedding.
Summary of the invention
The purpose of this invention is to provide the production method of making a kind of powder blood fat of food, feed addictive with livestock and poultry blood, hemoglobin and grease, this method is to adopt microcapsules technology, the production technology of reference powder grease, livestock and poultry blood or hemoglobin and grease are passed through emulsifier, the protein that utilizes in the blood to be rich in and the wall material of interpolation use spray drying process to make to the grease embedding again.
The objective of the invention is to realize that by following main technical schemes step is:
1) the bright livestock and poultry whole blood of Shou Jiing adds mass ratio and is 0.2～0.8% trisodium citrate while stirring as anti-coagulants, and wherein trisodium citrate and water are in mass ratio 1: (6～15) ratio, in centrifuge, anticoagulated whole blood is separated then;
2) blood or isolated subnatant hemoglobin by 1: (1～3) volume ratio adds the deionized water broken wall;
3) blood or hemoglobin are mixed at 50～70 ℃ with the grease of thawing, stir and be incubated 5～10 minutes;
4) adding HLB value is 5～10 emulsifying agent emulsification, adds the embedding of wall material simultaneously;
5) carry out homogeneous, pressure is 15～30MPa.Homogeneous can further be pulverized fat globule, and fat is dissolved in protein and the wall material fully;
6) spray-drying: adopting intake air temperature is 160～220 ℃, and the air outlet temperature is 55～85 ℃ the mixed liquor drying made the powder blood fat; Products obtained therefrom is a sepia, and the fragrance of grease is arranged.
Described blood or hemoglobin and grease are in mass ratio (1～6): 1 ratio is mixed.
Described emulsifying agent is the equivalent compound emulsifying agent of glycerin monostearate (monoglyceride), polyoxyethylene sorbitan carboxylic ester (commodity are called Tween-40), sucrose ester and sorbitol ester, and in the mass ratio 1 of compound emulsifying agent and grease: (1～5) ratio adds.
Described wall material also has maltodextrin and starch except hemoglobin, wherein a kind of and the ratio adding of grease by mass ratio 5～20%.
The invention has the beneficial effects as follows the employing microcapsules technology, utilize the protein that is rich in the blood, made a kind of novel additive-powder blood fat as main wall material.It is rich in protein, fat and micro-, is a kind of ultimate food, feed addictive.Product energy height, and can effectively replenish various trace elements and strengthen protein, especially L-lysine.Can replace the partial pigment in the sausage and the interpolation of fat meat, can be used for the feed addictive of livestock and poultry and aquatic products etc., can effectively promote their growth.Reach utilization and the overstocked problem of solution grease, the byproduct that occurs in the comprehensive utilization livestock and poultry slaughtering process to livestock and poultry blood.
Description of drawings
Fig. 1 is the technological process of production figure of powder blood fat.
The specific embodiment
The invention provides the production method of making a kind of powder blood fat of food, feed addictive with livestock and poultry blood, hemoglobin or grease, this method is to adopt microcapsules technology, the production technology of reference powder grease, livestock and poultry blood or hemoglobin and grease are passed through emulsifier, the protein that utilizes in the blood to be rich in and the wall material of interpolation use spray drying process to make to the grease embedding again.
The step of technique scheme is as shown in Figure 1:
(1) the bright livestock and poultry whole blood of Cai Jiing adds mass ratio and is 0.2～0.8% trisodium citrate while stirring as anti-coagulants, and wherein lemon three sour sodium and water are in mass ratio 1: (6～15) ratio, centrifugal then anticoagulated whole blood is separated;
(2) blood or isolated subnatant hemoglobin by 1: (1～3) volume ratio adds the deionized water broken wall;
(3) mass ratio (1～6) of blood or hemoglobin and grease: 1 ratio is mixed at 50～70 ℃, stirs and be incubated 5～10 minutes.
(4) adding HLB value is 5～10 emulsifying agent emulsification, adds the embedding of wall material simultaneously;
(5) carry out homogeneous, pressure is 15～30MPa.Homogeneous can further be pulverized fat globule, and fat is dissolved in protein and the wall material fully;
(6) spray-drying: adopting intake air temperature is 160～220 ℃, and the air outlet temperature is 55～85 ℃ the mixed liquor spray-drying made the powder blood fat; Products obtained therefrom is a sepia, and the fragrance of grease is arranged.
Mentioned emulsifier is the equivalent compound emulsifying agent of glycerin monostearate (monoglyceride), polyoxyethylene sorbitan carboxylic ester (commodity are called Tween-40), sucrose ester and sorbitol ester, and in the mass ratio 1 of compound emulsifying agent and grease: (1～6) ratio adds.
Above-mentioned wall material also adds maltodextrin or starch except hemoglobin, and wherein a kind of and grease are by the ratio adding of mass ratio 5～20%.
For embodiment the present invention is given further more below.
Embodiment 1
Collect healthy pig blood, the trisodium citrate of adding 0.35% is as anti-coagulants.The grease that adds amount of dry matter 25% stirs.Be heated to 60 ℃, add the compound emulsifying agent (the HLB value is 7.5) of oil quantity 2.6%, adding the wall material is 12%, insulation 10min.The spray dryer drying is used in emulsifying under 20Mpa then again, and inlet temperature is 180 ℃, and outlet temperature is 70 ℃, obtains brown whole blood-powder blood fat.
Embodiment 2
Prepare the whole blood-powder blood fat of broken wall with embodiment 1 described method, difference is to add the deionized water broken wall by 1: 1 volume of whole blood, adds the grease of amount of dry matter 15%, stirs.Be heated to 56 ℃, add the compound emulsifying agent (the HLB value is 6.5) of oil quantity 2%, adding the wall material is 9%, insulation 10min.The spray dryer drying is used in emulsifying under 20Mpa then again, and inlet temperature is 200 ℃, and outlet temperature is 60 ℃, obtains brown whole blood-powder blood fat.
Embodiment 3
Collect the anti-freezing pig whole blood of health, separate, take off the hemoglobin of layer, add 15% grease mixing, stir through 10000g centrifugal force.Be heated to 56 ℃, add the emulsifying agent (the HLB value is 9.5) of oil quantity 2%, adding the wall material is 9%, insulation 10min.The spray dryer drying is used in emulsifying under 20Mpa then again, and inlet temperature is 210 ℃, and outlet temperature is 65 ℃, obtains henna hemoglobin-powder blood fat
Embodiment 4
Collect healthy anticoagulated whole blood, separate, take off the red blood cell of layer, add the deionized water broken wall, add the grease of amount of dry matter 25% then, stir by 1: 1 volume through 10000g centrifugal force.Be heated to 70 ℃, add the emulsifying agent (the HLB value is 5) of oil quantity 2%, adding the wall material is 9%, insulation 10min.Dry spray dryer drying is used in emulsifying under 20Mpa then again, and inlet temperature is 210 ℃, and outlet temperature is 70 ℃, obtains the hemoglobin-powder blood fat of red broken wall.
Claims (4)
1. the production method of a powder blood fat, it is characterized in that: this method is to adopt microcapsules technology, the production technology of reference oil powder, livestock and poultry blood or hemoglobin and grease are passed through emulsifier, the protein that utilizes in the blood to be rich in and the wall material of interpolation use spray drying process to make to the grease embedding again;
The steps include:
(1) the bright livestock and poultry whole blood of Shou Jiing adds mass ratio and is 0.2～0.8% trisodium citrate while stirring as anti-coagulants, and wherein trisodium citrate and water are in mass ratio 1: (6～15) ratio, in centrifuge, anticoagulated whole blood is separated then;
(2) blood or isolated subnatant hemoglobin by 1: (1～3) volume ratio adds the deionized water broken wall;
(3) blood or hemoglobin are mixed at 50～70 ℃ with the grease of thawing, stir and be incubated 5～10 minutes;
(4) adding HLB value is 5～10 emulsifying agent emulsification, adds the embedding of wall material simultaneously;
(5) carry out homogeneous, pressure is 15～30MPa.Homogeneous can further be pulverized fat globule, and fat is dissolved in protein and the wall material fully;
(6) spray-drying: adopting intake air temperature is 160～220 ℃, and the air outlet temperature is 55～85 ℃; The mixed liquor drying is made the powder blood fat; Products obtained therefrom is a sepia, and the fragrance of grease is arranged.
2. according to the production method of the described powder blood fat of claim 1, it is characterized in that: described blood or hemoglobin and grease are in mass ratio (1～6): 1 ratio is mixed.
3. according to the production method of the described powder blood fat of claim 1, it is characterized in that: described emulsifying agent is the compound emulsifying agent of glycerin monostearate (monoglyceride), polyoxyethylene sorbitan carboxylic ester (commodity are called Tween-40), sucrose ester and sorbitol ester etc., adds in mass ratio 1～5% ratio with grease.
4. according to the production method of the described powder blood fat of claim 1, it is characterized in that: described wall material also has maltodextrin or starch except hemoglobin, wherein a kind of and grease adds in mass ratio 5～20% ratios.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100311717A CN100496301C (en) | 2004-04-14 | 2004-04-14 | Method for producing powder blood fat |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100311717A CN100496301C (en) | 2004-04-14 | 2004-04-14 | Method for producing powder blood fat |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1561827A true CN1561827A (en) | 2005-01-12 |
| CN100496301C CN100496301C (en) | 2009-06-10 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100311717A Expired - Fee Related CN100496301C (en) | 2004-04-14 | 2004-04-14 | Method for producing powder blood fat |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100496301C (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101124938B (en) * | 2006-08-17 | 2012-07-04 | 上海杰隆生物制品股份有限公司 | Using high-pressure homogenizing technology to process fresh plasma and fresh erythrocyie separated from animal blood |
| CN103734518A (en) * | 2013-12-23 | 2014-04-23 | 安徽农业大学 | Efficiently sheared, homogenized and emulsified oil powder |
| CN105285159A (en) * | 2015-10-20 | 2016-02-03 | 东北农业大学 | Preparation method of high oil containing soybean powdered oil |
| CN106922946A (en) * | 2015-12-31 | 2017-07-07 | 上海杰隆生物制品股份有限公司 | A kind of preparation method for wrapping grease-contained animal blood plasma albumen powder |
| CN108936030A (en) * | 2018-05-21 | 2018-12-07 | 沂南帅克宠物用品有限公司 | A kind of pet nutrition composition reducing pet kenosis peculiar smell containing probiotics |
-
2004
- 2004-04-14 CN CNB2004100311717A patent/CN100496301C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101124938B (en) * | 2006-08-17 | 2012-07-04 | 上海杰隆生物制品股份有限公司 | Using high-pressure homogenizing technology to process fresh plasma and fresh erythrocyie separated from animal blood |
| CN103734518A (en) * | 2013-12-23 | 2014-04-23 | 安徽农业大学 | Efficiently sheared, homogenized and emulsified oil powder |
| CN103734518B (en) * | 2013-12-23 | 2015-07-01 | 安徽农业大学 | Efficiently sheared, homogenized and emulsified oil powder |
| CN105285159A (en) * | 2015-10-20 | 2016-02-03 | 东北农业大学 | Preparation method of high oil containing soybean powdered oil |
| CN106922946A (en) * | 2015-12-31 | 2017-07-07 | 上海杰隆生物制品股份有限公司 | A kind of preparation method for wrapping grease-contained animal blood plasma albumen powder |
| CN108936030A (en) * | 2018-05-21 | 2018-12-07 | 沂南帅克宠物用品有限公司 | A kind of pet nutrition composition reducing pet kenosis peculiar smell containing probiotics |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100496301C (en) | 2009-06-10 |
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