CN1552212A - Oxidative disinfectant bactericide and preparing method thereof - Google Patents
Oxidative disinfectant bactericide and preparing method thereof Download PDFInfo
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- CN1552212A CN1552212A CNA031290329A CN03129032A CN1552212A CN 1552212 A CN1552212 A CN 1552212A CN A031290329 A CNA031290329 A CN A031290329A CN 03129032 A CN03129032 A CN 03129032A CN 1552212 A CN1552212 A CN 1552212A
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- silver
- hydrogen peroxide
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- disinfectant
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Abstract
An oxide-type disinfecting bactericide is prepared from hydrogen peroxide, synergistic, stabilizer, pH regulator and deionized water through preparing Ag component step by step and proportionally mixing with others. Its advantages are broad spectrum, high bactericiding power and long storage time up to 36 months.
Description
One, technical field:
Oxidized form disinfectant of the present invention and preparation method thereof, what relate to is the fine chemical technology field, be particularly related to a kind of chemical constituent of utilizing, composite oxidized form disinfectant and preparation method thereof, be widely used in and kill in the air and bacterium, the virus of body surface, be specially adapted to the disinfection of communicable disease such as respiratory tract.
Two, background technology:
Hydrogen peroxide is as a kind of known sanitizer chemical, and its molecular composition is simple, and catabolite is water and hydrogen, and human body and environment are not produced residual toxicity, belongs to the high-effective disinfecting bactericide.But it has disadvantage is (1) poor stability; (2) sterilizing time is short; (3) sterilization speed is slower; (4) price height; (5) surperficial tension is big, has therefore restricted the application of hydrogen peroxide.
Three, summary of the invention:
The purpose of this invention is to provide a kind of is the disinfectant and preparation method thereof of main component with the hydrogen peroxide, solved disinfectant stability, sterilization speed is faster, stronger, and bacteriocidal concentration reduces, to reduce skin irritatin and the reduction product cost to human body and livestock and poultry.It is characterized in that: its proportioning component of oxidized form disinfectant of the present invention (100 parts) is:
Hydrogen peroxide 5-50%
Synergist 0.5-2.5%
Stabilizing agent 0.2-1.5%
Conditioning agent makes the pH value of disinfectant reach 2-4.5,
Deionized water 86.7%;
Wherein: synergist can be a silver salt, comprises silver sulfate, silver nitrate, and stabilizing agent can be sodium phosphate trimer, and phosphoric acid can be used as conditioning agent; Its preparation method follows these steps to carry out, and (1) prepares the aqueous solution of synergist, obtains the silver components of silver ion; (2) stabilizing agent is added in the above-mentioned silver components that silver ion arranged; (3) mix with aqueous hydrogen peroxide solution; (4) add phosphoric acid and make the acid number conditioning agent and regulate pH value and Jia Shui and supply weight and reach 100%, in above-mentioned preparation method's process, slowly pour in the aqueous hydrogen peroxide solution that contains 5-50% while stirring under the solution normal temperature that obtains; Slowly add while stirring equally at normal temperatures when adding the acid number conditioning agent.
The present invention compared with prior art, the concentration of hydrogen peroxide of the present invention is suitable for the use under the various conditions, proportioning the best of synergist, stabilizing agent and sustained release agent should be that concentration of hydrogen peroxide is high more, the amount of synergist, stabilizing agent and sustained release agent is corresponding wants high.
The oxidized form disinfectant belongs to the compound disinfecting bactericide, with simple hydrogenperoxide steam generator relatively, with the prestige reason oxidized form disinfectant of concentration to Escherichia coli, staphylococcus aureus, hay bacillus, that black mutation gemma is killed ability is obvious, be enhanced about more than once.When organic matter existed, the bactericidal action of oxidized form disinfectant also was better than simple hydrogenperoxide steam generator greatly.Relatively, common hydrogen peroxide is generally about 3 months storage period from stable aspect, needs matching while using, and the storage period of oxidized form disinfectant up to 36 months, the phase was declined greater than 7 years in its end.This disinfectant has clean air, kills in the air and bacterium, the germ of body surface, is specially adapted to the disinfection of communicable disease such as respiratory tract, in the ward and the public place can the person of being implemented in sterilize.Because of it is colourless, tasteless, nontoxic, nonirritant (concentration is below 1%), also can directly be sprayed on oral cavity, nasal cavity, face, mouth mask surface sterilization and carry out the prophylactic disinfection sterilization, can block the propagation of various bacteriums, germ effectively, sterilization and carry out the prophylactic disinfection sterilization, can block the propagation of various bacteriums, germ effectively, cut off source of infection, this disinfectant uses for a long time, and bacterium does not contain and develops immunity to drugs.
The oxidized form disinfectant is a kind of colourless, tasteless, nontoxic transparency liquid, stable storing under the normal temperature, and effective ingredient is annual to be changed less than 2%.And realized the different composite of different disinfectant active matters, and having strengthened the effect of disinfection, social benefit and economic benefit are obvious.
Four, description of drawings:
Fig. 1 is oxidized form disinfectant technological process of production figure;
Five, embodiment:
Below the present invention is further described with producing 100kg oxidized form disinfectant:
Hydrogen peroxide 10%
Silver nitrate 1%
Sodium phosphate trimer 0.3%
Phosphoric acid is as conditioning agent about 2% (regulating pH value reaches in 4.5),
Deionized water 86.7%;
Silver nitrate 1% adds hydrogen peroxide 10%, is prepared into the aqueous solution of synergist, obtains the silver components of silver ion;
Stabilizing agent sodium phosphate trimer 0.3% added in the above-mentioned silver components that silver ion arranged mix, add phosphoric acid 2% in the above-mentioned solution again, make the acid number conditioning agent and regulate pH value and reach in 4.5, in time add deionized water 86.7% water.
In the above-mentioned preparation process, the solution that whenever obtains is all slowly poured at normal temperatures while stirring, is prepared into the oxidized form disinfectant, filling and sealing, test package, warehouse-in.
Claims (2)
1. oxidized form disinfectant of the present invention and preparation method thereof is characterized in that: its proportioning component (by 100 parts):
Hydrogen peroxide 5-50%
Synergist 0.5-2.5%
Stabilizing agent 0.2-1.5%
Conditioning agent makes the pH value of disinfectant reach 2-4.5,
Deionized water 86.7%;
Its preparation method follows these steps to carry out, and (1) prepares the aqueous solution of synergist, obtains the silver components of silver ion; (2) stabilizing agent is added in the above-mentioned silver components that silver ion arranged; (3) mix with aqueous hydrogen peroxide solution; (4) add phosphoric acid and make the acid number conditioning agent and regulate pH value and Jia Shui and supply weight and reach 100%, in above-mentioned preparation method's process, slowly pour in the aqueous hydrogen peroxide solution that contains 5-50% while stirring under the solution normal temperature that obtains; Slowly add while stirring equally at normal temperatures when adding the acid number conditioning agent.
2. require 1 described oxidized form disinfectant and preparation method thereof according to aforesaid right, it is characterized in that: synergist can be a silver salt, comprises silver sulfate, silver nitrate, and stabilizing agent can be sodium phosphate trimer, and phosphoric acid can be used as conditioning agent.
Priority Applications (1)
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CNA031290329A CN1552212A (en) | 2003-06-04 | 2003-06-04 | Oxidative disinfectant bactericide and preparing method thereof |
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CNA031290329A CN1552212A (en) | 2003-06-04 | 2003-06-04 | Oxidative disinfectant bactericide and preparing method thereof |
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CN1552212A true CN1552212A (en) | 2004-12-08 |
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CNA031290329A Pending CN1552212A (en) | 2003-06-04 | 2003-06-04 | Oxidative disinfectant bactericide and preparing method thereof |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101189163B (en) * | 2005-05-19 | 2010-05-19 | 三菱瓦斯化学株式会社 | Aqueous hydrogen peroxide for sterilization |
CN103563983A (en) * | 2012-07-24 | 2014-02-12 | 上海纳米技术及应用国家工程研究中心有限公司 | Nano-silver peroxide composite antibacterial solution and preparation method thereof |
CN106087650A (en) * | 2016-06-16 | 2016-11-09 | 成都市图腾环保科技有限公司 | Hydrogen peroxide goes the application of a good appetite suddenly appearing in a serious disease at synthetic material runway cover harmful substance |
CN109757515A (en) * | 2019-03-18 | 2019-05-17 | 洛阳民康生物工程有限公司 | A kind of colorless and transparent micromicron grade electrolytic silver ion complex antimicrobials and preparation method thereof |
CN110870483A (en) * | 2018-08-30 | 2020-03-10 | 洛阳蓝新生物科技有限公司 | Artemisinin silver ion composite disinfectant |
CN111066813A (en) * | 2019-11-15 | 2020-04-28 | 嘉兴沃特泰科环保科技股份有限公司 | Preparation method and device of oxidation type bactericide |
CN111280189A (en) * | 2020-02-25 | 2020-06-16 | 河南绿澳化工科技有限公司 | Disinfectant for food industry and preparation method thereof |
CN113575610A (en) * | 2021-08-25 | 2021-11-02 | 四川恒通动保生物科技有限公司 | Low-temperature-resistant hydrogen peroxide disinfectant and preparation method thereof |
CN114304144A (en) * | 2021-11-23 | 2022-04-12 | 山东新华莎罗雅生物技术有限公司 | Sporicide capable of killing spores and preparation method thereof |
CN114946880A (en) * | 2022-07-05 | 2022-08-30 | 桂林清研皓隆新材料有限公司 | Silver-loaded titanium dioxide, preparation method and application thereof, and disinfection and odor removal spray containing silver-loaded titanium dioxide |
-
2003
- 2003-06-04 CN CNA031290329A patent/CN1552212A/en active Pending
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101189163B (en) * | 2005-05-19 | 2010-05-19 | 三菱瓦斯化学株式会社 | Aqueous hydrogen peroxide for sterilization |
CN103563983A (en) * | 2012-07-24 | 2014-02-12 | 上海纳米技术及应用国家工程研究中心有限公司 | Nano-silver peroxide composite antibacterial solution and preparation method thereof |
CN103563983B (en) * | 2012-07-24 | 2016-06-15 | 上海纳米技术及应用国家工程研究中心有限公司 | A kind of nano-silver peroxide composite antibacterial solution and its preparation method |
CN106087650A (en) * | 2016-06-16 | 2016-11-09 | 成都市图腾环保科技有限公司 | Hydrogen peroxide goes the application of a good appetite suddenly appearing in a serious disease at synthetic material runway cover harmful substance |
CN110870483A (en) * | 2018-08-30 | 2020-03-10 | 洛阳蓝新生物科技有限公司 | Artemisinin silver ion composite disinfectant |
CN109757515A (en) * | 2019-03-18 | 2019-05-17 | 洛阳民康生物工程有限公司 | A kind of colorless and transparent micromicron grade electrolytic silver ion complex antimicrobials and preparation method thereof |
CN111066813A (en) * | 2019-11-15 | 2020-04-28 | 嘉兴沃特泰科环保科技股份有限公司 | Preparation method and device of oxidation type bactericide |
CN111066813B (en) * | 2019-11-15 | 2021-06-15 | 嘉兴沃特泰科环保科技股份有限公司 | Preparation method and device of oxidation type bactericide |
CN111280189A (en) * | 2020-02-25 | 2020-06-16 | 河南绿澳化工科技有限公司 | Disinfectant for food industry and preparation method thereof |
CN113575610A (en) * | 2021-08-25 | 2021-11-02 | 四川恒通动保生物科技有限公司 | Low-temperature-resistant hydrogen peroxide disinfectant and preparation method thereof |
CN114304144A (en) * | 2021-11-23 | 2022-04-12 | 山东新华莎罗雅生物技术有限公司 | Sporicide capable of killing spores and preparation method thereof |
CN114946880A (en) * | 2022-07-05 | 2022-08-30 | 桂林清研皓隆新材料有限公司 | Silver-loaded titanium dioxide, preparation method and application thereof, and disinfection and odor removal spray containing silver-loaded titanium dioxide |
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