CN1524937A - Maniod eibish oil - Google Patents
Maniod eibish oil Download PDFInfo
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- CN1524937A CN1524937A CNA03105269XA CN03105269A CN1524937A CN 1524937 A CN1524937 A CN 1524937A CN A03105269X A CNA03105269X A CN A03105269XA CN 03105269 A CN03105269 A CN 03105269A CN 1524937 A CN1524937 A CN 1524937A
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- lixiviate
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Abstract
The invention provides a refined functional cooking oil, which contains greatly reduced coloring matter and impurity content, the VE oxidation reaction in the oil is minimized, thus the storage period is extended, the total content of aliphatic acid amounts to over 78%, and the other constituents are, multiple highly active unsaponifiable matter sum 4.88%, VA 0.13mg/100g, lysergol 1.24mg/100g, catechin 4.28mg/100g, beta-sitosterin 5.25mg/100g, natural active VE 1500-2120mg/kg.
Description
Technical field the invention belongs to the food development field, relates to a kind of elaboration edible oil.
The background technology certain herbaceous plants with big flowers relates to the critical positions of occupying the seat of honour in the classical documents of food on China's history.In the Huangdi's Internal Classics before the millennium certain herbaceous plants with big flowers is classified as first of five dishes that people eat, " certain herbaceous plants with big flowers, positive grass are the master of hundred dishes also in " food book on Chinese herbal medicine " record before 400 years." certain herbaceous plants with big flowers in these records, belonging to any plant by modern plants credit class? research, textual criticism pertinent data should be Sunset Abelmoschus Roots, i.e. Malvaceae 0003 Sunset Abelmoschus Root (Manihot (Linn.) Medicus) in Chinese Plants classification and the code.It is main according to being: it is gumbo that the traditional food that the Ministry of Health determines is enumerated the certain herbaceous plants with big flowers dish according to catalogue " Chinese composition table of foods ", gumbo indication plant in a large amount of modern documents is the 0002 coffee ambrette and 0003 Sunset Abelmoschus Root of Malvaceae Abelmoschus in " Chinese Plants classification and code ", " middle national flower warp " proposes the coffee ambrette and " originates in the torrid zone ", and Sunset Abelmoschus Root " originates in China ".Sunset Abelmoschus Root Abelmoschus manihot (L.) Medic. is a Malvaceae annual herb plant.The applicant participates in writing and implement CN1105059A, the CN1051057A document scheme of more than ten years, has narrated the value of Sunset Abelmoschus Root oil, has also run into many problems when stating scheme on the implementation.Yellow hollyhock seed " seed is black, close living pilose antler shape fine hair " is described in " the Chinese agriculture patent " that the Ministry of Agriculture writes.Yellow hollyhock seed fine hair and scurf are black, contain a large amount of colloids, and above-mentioned technical literature does not add processing to this, cause pigment to dissolve in grease, are difficult to remove.Above-mentioned colloid the system oily process in or carbonization or decomposition, in the suspendible grease, the VE in the grease carries out oxidizing reaction to these pigment impurities, reduces its activity.Be far longer than the tooling cost of the present invention if from oil, remove its cost of these impurity, and be difficult to reach removal fully the seed material.In squeezing process, the adjusting of adopting squeezing clamping time, extruding number of times, input speed, spiral is limited in the above-mentioned document, temperature control in preparation process does not limit to material, the drawback of material processing causes and has strengthened the oxidizing reaction of VE in the grease in the manufacture craft in addition.
Above-mentioned document is when utilizing extraction process to produce grease, and the characteristic according to yellow hollyhock seed does not propose the preceding material processing scheme of extraction.The yellow hollyhock seed surface also has the very big gelationus Mierocrystalline cellulose tissue of one deck density except that being covered with the fine hair scurf, when utilizing extraction process to extract grease, these tissues decompose in vat liquor, influence the separation purity of solvent; In that material is carried out fragmentation, in fragmentation, when grease contacted with oxygen from the disruptive cell, above-mentioned impurity resolvent had increased the weight of the VE oxidation in the grease.
Because its foreign matter content height of existence of the problems referred to above, the pigment that dissolves in the oil is difficult to remove, and the color of oil is darker.It is higher that product contains the organic solvent amount, often under critical line up to standard.
Summary of the invention the purpose of this invention is to provide a kind of to take off fine hair, removes the yellow hollyhock seed of scurf and makes raw material, the functional edible oil of the elaboration of preparation.This product has solved the associated problem of mentioning in the background technology.Its product becomes faint yellow or pure look than reducing greatly on the currently available products pigment impurity content by the gloomy yellow that is, and organic solvent content reduces, and the VE oxidizing reaction in the grease drops to Schwellenwert, and the shelf lives of guaranteeing the quality prolongs, and edibleness improves.
The present invention also provides a kind of grease extracting method of general Sunset Abelmoschus Root material simultaneously, this method adopts process order, equipment and the solvent of known oil-producing technique, on processing parameter, limit the temperature of material and vat liquor, limit the time and the mode of squeezing, extruding, lixiviate, reach and produce the greasy purpose of elaboration Sunset Abelmoschus Root.
Embodiment concrete enforcement of the present invention is: the material yellow hollyhock seed of making oil is carried out the lint hair, removes the scurf processing, its method is: adopt earlier the clear general labourer of conventional vibratory screening apparatus and cold air stream to plant and remove seed fine hair, place the cereal processor to grind then or adopt cold air stream to impact or adopt cold water shock to separate and remove seed fine hair and scurf.When adopting the cold water shock cleaning, after cleaning, dewater at once, moisture is remained on below 18%.Sign directly perceived after the qualified cleaning is that seed-coat is smooth, shiny black, and embryo is complete, and it is sound to grab a shake with hand.The system cake hydraulic pressure milling process of the seed employing qualification data of above-mentioned processing or screw extrusion method or extraction make grease.
Qualified point is during with the producing of system blastochyle platen press: material pulverize steam fry, in the system embryo, expressing process, temperature of charge is controlled at below 108 degree, material preheats the time and is controlled in 48 minutes.Pressure process can not settle at one go, by low pressure to the highly compressed time limit more than 1 hour.
Qualified point with the screw extrusion method is: material is directly installed, temperature of charge is controlled at below 130 ℃ in the preparation process, when doing secondary extrusion, for the first time the screw extrusion space is greater than the extruding space of an extrusion process in the common process with processing season, envrionment temperature difference, its sign directly perceived be the biscuit extruded in the form of sheets, it is light brown that color is.The handle biscuit first time carries out the extruding second time at the frontloader of not lowering the temperature when pushing for the second time, extrusion spiral will be with processing envrionment temperature difference in season for the second time, the extruding space is less than for the first time, input speed ratio input speed for the first time is reduced in below 70%, its sign directly perceived is that the cake cypress is coffee color, and cake cypress thickness is below 4 millimeters.
Grasp during with extracting technology following some: adopt the distillation of the previous solvent liquid separating technology that condenses, or adopt the spray membrane process that adopts in the known in recent years Chemical Manufacture, the greasy mixed solution of solvent is separated.Material temperature in fragmentation, lixiviate or extraction is controlled at below 83 ℃, the extraction time of each lixiviate still material was controlled in 8 hours, after each lixiviate still lixiviate, the sepn process of filtering the Oil solvent mixed solution of exporting is controlled in 11 hours the highest being controlled at below 138 ℃ of temperature of lixiviate or extraction liquid when doing lixiviate or extracting and separating grease after the filtration.
The present invention program has solved the problem described in the above-mentioned background, pigment and the colloid of having got rid of seed fine hair, scurf enter grease, improved the quality of product, done food raw material or in medicine, makeup and relevant Chemicals, use as the natural anti-oxidation grease that has no side effect.
The greasy method of Sunset Abelmoschus Root of producing of the present invention is applicable to the Sunset Abelmoschus Root system oil raw material of various materials.
The exceptional function grease that product of the present invention is better than praising highly on the domestic and international market on basal component data and effect.The rare type lipid acid kind of Sunset Abelmoschus Root oil is good, and total content is more than 78%, the unsaponifiables summation 4.88% of multiple high reactivity material, V
A0.13mg/100g, ergosterol 1.24mg/100g, catechin 4.28mg/100g, β-Gu Zaichun 5.25mg/100g, natural radioactivity V
EIt is 11440mg/kg that 1500-2120mg/kg, natural VE detect high-content.Occurred some beyond thought surprising effects in using Sunset Abelmoschus Root oil: the biological center postgraduate Zhang Changqing of the Chinese Academy of Agricultural Sciences uses Sunset Abelmoschus Root oil and supplies with him to suffer from the father of malignant lymphoma edible, his father is after treatment is made a definite diagnosis by Beijing Tumour Hospital, be considered to life and continue two months at most, in illness improvement and the rehabilitation day by day unexpectedly after three months of edible Sunset Abelmoschus Root oil under the desperate state, the no positive body card of check after 2 years; The example that the Parkinsonism that the personage of Beijing professorship of portion uses to be had in the Sunset Abelmoschus Root oil for many years all disappears; Britain Mr. Fred buys 100,000 Sunset Abelmoschus Root oil balls, supplies the people of the trouble climacteric syndrome on ground such as Hong Kong, Singapore to eat, and after the eater took fortnight, symptom was eased or disappears substantially.
Value benefit of the present invention is bright and clear, Xinhua News Agency's telecommunication in March 31 in 1998 claims that " U.S. scientist points out; owing to only contain alpha's vitamin-E in the vitamin E capsule of present most drug company productions, can endanger healthy so take the vitamin-E medicine in a large number.
Research group in this base of a fruit funk of the biochemist of University of California Berkeley headed by gloomy finds, coffee horse vitamin-E in the vitamin-E can be removed the peroxy-nitrate that can cause heart trouble and cancer in the human body, and coffee horse vitamin-E also is the unique vitamin-E kind that can adhere to and remove the dusty gas nitrogen oxide in the laboratory." the maximum enterprise that produces the VE product in the world today is Switzerland Roche Holding Ag, its industry is at 10,000,000,000 dollars, but his contained VE of VE goods be alpha's type, and major part is turned to for animalsly by human in recent years, and price reduces naturally.Contain four types of natural VEs in the product of the present invention, wherein morphine VE content has 50%, and it is self-evident that it is worth benefit.
Embodiment: claim yellow hollyhock seed 2100kg,, grind with rice milling machinery again and remove the seed scurf with tape drum wind apparatus cereal shaker cleaning seed fine hair, must plant skin shiny black, pick up and spread a seed 2000kg that clear and melodious sound is arranged.Get the fragmentation of 1000kg kind, steam stir-fry 13 minutes with 93 ℃ of temperature, system embryo installation pressurization, from 30kg/cm～60kg/cm, progressively pressurization was kept pressure after 1 hour in half an hour, was pressurized to 68kg/cm again, filtered making crude oil, got oily 143kg.Get the direct feed auger system oil of 1000kg seed machine, transfer at 0.5cm in the extruding space, and the material cake that screws out is put into another extruding space 0.3cm screw machine operation immediately.After making the crude oil sedimentation and filtration, get oil product 148kg.
Biscuit behind the above-mentioned system oil when not falling, temperature is ground into the following powder of diameter 0.5cm.Put in the belt stirrer extraction kettle, the control material is cooked vat liquor with 3 times of normal hexanes and was put in the lixiviate still stirring and leaching 1.5 hours at 37 ℃, filters out the oil-containing vat liquor in batches, adds No. 6 stirring solvent lixiviates 40 minutes of 3.8 times of suitable materials again in the lixiviate still.120 ℃ of oil-containing normal hexane vat liquor heating, with vacuum 0.8 MPa, spray film precipitation, operation in 3 hours is finished, and gets oil product 121kg.No. 6 solvent inputs of oil-containing vaporizer distills precipitation under 110 ℃ of temperature, get oil product 63kg.
Claims (3)
1, a kind of edible elaboration vegetables oil is characterized in that utilizing from taking off fine hair, removes in the Sunset Abelmoschus Root seed of scurf squeezing or extraction and makes; The method of preparation adopts process order, equipment and the solvent of known oil-producing technique, on processing parameter, limits the temperature of material and vat liquor, limits the time and the mode of squeezing, extruding, lixiviate, reaches the quality of elaboration oil.
2, a kind of Sunset Abelmoschus Root essential oil preparation method is characterized in that:
When adopting system blastochyle squeezing system oil, material pulverize to steam is fried, in the system embryo, expressing process, temperature of charge is controlled at below 108 degree, material preheats the time and is controlled in 48 minutes, pressure process can not settle at one go, by low pressure to the highly compressed time limit more than 1 hour;
When adopting mechanical screw press to produce, the temperature when material pushes fully is the highest to be controlled at below 130 ℃, when adopting secondary extrusion, pushes the space for the first time and is greater than and pushes the space for the second time;
When adopting extraction or leach extraction method to make, material temperature in broken, lixiviate or extraction is controlled at below 83 ℃, the highest being controlled at below 138 ℃ of temperature of lixiviate or extraction back lixiviate or extraction liquid in separating the grease process;
Make oily key element divided by outer other of last qualification and adopt known technology, known device and medium.
3, claim 1,2 described products and Sunset Abelmoschus Root essential oil preparation method product, its purposes are to cook food or use in medicine, makeup and relevant Chemicals as the natural anti-oxidation grease that has no side effect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB03105269XA CN100497568C (en) | 2003-02-26 | 2003-02-26 | Maniod eibish oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB03105269XA CN100497568C (en) | 2003-02-26 | 2003-02-26 | Maniod eibish oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1524937A true CN1524937A (en) | 2004-09-01 |
| CN100497568C CN100497568C (en) | 2009-06-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB03105269XA Expired - Lifetime CN100497568C (en) | 2003-02-26 | 2003-02-26 | Maniod eibish oil |
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| CN (1) | CN100497568C (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009052681A1 (en) * | 2007-10-22 | 2009-04-30 | Zhiyuan Wang | Abelmoschus manihot (linn.) medius kernel product for natural nutritional edible and pharmaceutical raw material |
| CN103614240A (en) * | 2013-12-09 | 2014-03-05 | 山东金硕生物科技股份有限公司 | Production method of Abelmoschus manihot essential oil |
| CN103952240A (en) * | 2014-05-19 | 2014-07-30 | 安徽科技学院 | Preparation method of abelmoschus manihot essential oil |
| CN104255954A (en) * | 2014-09-02 | 2015-01-07 | 焦作市七月花生物科技有限公司 | Abelmoschus manihot(L.) Medic. compound base seed oil and preparation method and application of abelmoschus manihot(L.) Medic. compound base seed oil |
| CN104342282A (en) * | 2013-07-23 | 2015-02-11 | 台建祥 | Method for preparing functional grease and active protein powder from abelmoschus manilhot |
| WO2016101933A3 (en) * | 2016-01-28 | 2016-11-17 | 王亚伦 | Abelmoschus manihot refined oil |
| CN106962608A (en) * | 2017-03-16 | 2017-07-21 | 济南邦地生物工程有限公司 | A kind of method of gumbo seed processing gumbo oil, mixed feed and mushroom matrix |
-
2003
- 2003-02-26 CN CNB03105269XA patent/CN100497568C/en not_active Expired - Lifetime
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009052681A1 (en) * | 2007-10-22 | 2009-04-30 | Zhiyuan Wang | Abelmoschus manihot (linn.) medius kernel product for natural nutritional edible and pharmaceutical raw material |
| JP2011500065A (en) * | 2007-10-22 | 2011-01-06 | 北京東昇農業技術開発（集団）有限公司 | Natural nutritive foods, troro-aoi seeds (seed) products for pharmaceutical materials |
| CN104342282A (en) * | 2013-07-23 | 2015-02-11 | 台建祥 | Method for preparing functional grease and active protein powder from abelmoschus manilhot |
| CN103614240A (en) * | 2013-12-09 | 2014-03-05 | 山东金硕生物科技股份有限公司 | Production method of Abelmoschus manihot essential oil |
| CN103952240A (en) * | 2014-05-19 | 2014-07-30 | 安徽科技学院 | Preparation method of abelmoschus manihot essential oil |
| CN104255954A (en) * | 2014-09-02 | 2015-01-07 | 焦作市七月花生物科技有限公司 | Abelmoschus manihot(L.) Medic. compound base seed oil and preparation method and application of abelmoschus manihot(L.) Medic. compound base seed oil |
| CN104255954B (en) * | 2014-09-02 | 2016-11-23 | 河南省七月花生物科技有限公司 | A kind of Abelmoschus manihot （L.） Medic compound basic seed oil and its preparation method and application |
| WO2016101933A3 (en) * | 2016-01-28 | 2016-11-17 | 王亚伦 | Abelmoschus manihot refined oil |
| CN106962608A (en) * | 2017-03-16 | 2017-07-21 | 济南邦地生物工程有限公司 | A kind of method of gumbo seed processing gumbo oil, mixed feed and mushroom matrix |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100497568C (en) | 2009-06-10 |
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