CN1498653A - Extract of 'Sheganguo' and its prepn. method - Google Patents
Extract of 'Sheganguo' and its prepn. method Download PDFInfo
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- CN1498653A CN1498653A CNA021501459A CN02150145A CN1498653A CN 1498653 A CN1498653 A CN 1498653A CN A021501459 A CNA021501459 A CN A021501459A CN 02150145 A CN02150145 A CN 02150145A CN 1498653 A CN1498653 A CN 1498653A
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- phyllanthus emblica
- extract
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- hyperglycemia
- diabetes
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- Medicines Containing Plant Substances (AREA)
Abstract
An extract of Fructus phyllanthi in the form of health-care beverage, instant particles, oral liquid, or capsules for preventing and treating hypertension, hyperlipomia, hyperglycemia, thrombus, diabetes and cancer is prepared from Fructus phyllanthi through washing, dripdrying, softening, beating, removing stone, alcoholizing, settling, separation, distilling, concentration, drying and shaping.
Description
The present invention relates to a kind of Phyllanthus emblica L. extract and preparation method thereof, it is characterized in that it is the Phyllanthus emblica L. extract of feedstock production with fresh Phyllanthus emblica L., and be prepared into products such as health beverage, capsule, oral liquid, electuary with it, diseases such as hypertension, hyperlipidemia, hyperglycemia, thrombosis, diabetes, cancer there is drug action.
Known Phyllanthus emblica L. is an euphorbia plant, contain vitamin, aminoacid, polysaccharide and trace element, often the edible fresh Phyllanthus emblica L. truly has certain effectiveness to blood pressure lowering, blood fat reducing, daily diet need reach 250 grams, just have positive effect, particularly diabetes and cancer patient, also need increase daily diet, the big amount and the bitterness of Phyllanthus emblica L. stimulate the burden that produces amount to the patient; Thereby produce anorexia, few food, refusing to eat phenomenon.Fresh Phyllanthus emblica L. juice has corrosion and coloration to metal, influence packing and storage.
The objective of the invention is provides a kind of Phyllanthus emblica L. extract and preparation method thereof in order to solve the defective of above-mentioned existence.
The Phyllanthus emblica L. extract employing that the present invention relates to is prepared as follows method and makes:
1, with fresh Phyllanthus emblica L. washing 5-8 minute, dewatering 15 minutes.
2, softening: under 80 ℃ temperature, heat waterborne was steamed 15 minutes with Phyllanthus emblica L..
3, making beating: pull an oar enucleation with beater when treating that remollescent Phyllanthus emblica L. is cooled to below 40 ℃.
4, alcoholization: the emblic pulp is added cellulase PPM550, and pectase PPM550 stirs, and leaves standstill 60 minutes, adds 95% ethanol, and ratio is 1: 2-3, mixing, left standstill 24 hours, and make its sedimentation.
5, separate: get supernatant liquid filtering and remove slag.
6, distillation: filtrate is imported in the distillator, heated, distill and reclaimed ethanol in 2-2.5 hour, be warming up to again more than 95 and distilled 60 minutes, be cooled to 45-50 ℃ to 58-60.
7, concentrate: get Phyllanthus emblica L. juice input vacuum concentrator, concentrate, when treating that it reaches material-water ratio 30%, be cooled to 37 ℃.
8, drying: will concentrate and carry out drying in lyophilization and spray drying or the electric heating drying baker, moisture is controlled in 3%.
9, pulverize: Phyllanthus emblica L. extract is machined into 200 purpose fine powders with superfine grinding.
10, packing: use plastic film material, vacuum packaging, promptly get Phyllanthus emblica L. extract.
11, irradiation: packaged Phyllanthus emblica L. extract is carried out radiation sterilizing, deposit in the shady and cool exsiccant warehouse;
12, consumption: health beverage 0.3%, electuary are that 1.5 grams add adjuvant 3.5 grams, and oral liquid 1.5 grams add pure water 10-30ml, capsule 500mg/ grain.
The Phyllanthus emblica L. extract that the present invention relates to is characterized by coffee color, and powdery has special micro-fragrance, and water-soluble extractives is no less than 60%, and moisture is less than 3%, and ash is greater than 0.3%.
Pharmacological evaluation shows: health beverage, capsule, oral liquid, the electuary of Phyllanthus emblica L. extract and Phyllanthus emblica L. extract preparation thereof have drug action to hypertension, hyperlipidemia, hyperglycemia, energy blood pressure lowering, blood fat reducing, blood sugar lowering.Take Phyllanthus emblica L. extract 3-4.5 gram every day, divide clothes 2-3 time, obey 1.5 grams at every turn, took 60-90 days, to arteriosclerosis, hypertension, hyperlipidemia, hyperglycemia, thrombosis, diabetes, cancer have obvious control effect.
Acute toxicity test and residual hazard test show: the product of Phyllanthus emblica L. extract and Phyllanthus emblica L. extract preparation thereof, and LD50 is extract 10000mg/kg, the nontoxic level in true border is without any side effects, takes safe and reliable.
Advantage of the present invention is that the fresh Phyllanthus emblica L. of employing is a feedstock production, the health beverage of Phyllanthus emblica L. extract and preparation thereof, capsule, oral liquid, electuary, enlarged the range of application of Phyllanthus emblica L., can make full use of wild and Phyllanthus emblica L. resource artificial growth, its sufficient raw is guaranteed.
Another advantage of the present invention is to utilize fresh Phyllanthus emblica L. to be raw material, has reduced cost of material, preparation extract yield height, and production technology advanced person is fit to modern industrialization production.The most outstanding advantage of the present invention is to provide a kind of new raw material for anti-blood, vascular system disease.
Embodiment:
Get fresh Phyllanthus emblica L. 100kg, clean, dewatering, under 80 ℃ temperature, heat waterborne is steamed and was softened in 15 minutes with Phyllanthus emblica L..Making beating, enucleation, add cellulase 165 grams in the emblic pulp, stir and leave standstill 60 minutes, add 95% ethanol 200kg, mix homogeneously left standstill 24 hours, made its sedimentation, got the supernatant separating and filtering and removed slag.Filtrate is imported in the distillator, heated, distill and reclaimed ethanol in 2.5 hours to 58-60 ℃, be warming up to more than 95 ℃ distillation 60 minutes again, be cooled to 45-50 ℃, Phyllanthus emblica L. juice is imported in the vacuum concentrator concentrated, make the feed liquid ratio reach at 30% o'clock and be cooled to 37 ℃, blowing.Vacuum drying oven is put in the concentrated solution sabot carried out drying, the moisture of control extract is in 3%, dry thing is put into ultrafine crusher make 200 purpose fine powders, Phyllanthus emblica L. extract fine powder yield is 1.533%, actual extract 1533 grams that obtain, pack with plastic film bag, carrying out radiation sterilizing at last is finished product.Get Phyllanthus emblica L. extract 810 grams, being divided in the hard capsule case is the 500mg/ grain, makes 1620 hard capsules, takes for 3 people 60 days, and 3 times for each person every day, the morning, noon and afternoon respectively obey 1 time, each 3.Lab-gown is with each 1 people of 3 philtrum hypertension, hyperlipidemia, hyperglycemic patients, take that its blood pressure, blood fat, blood glucose are obviously controlled after testing after 60 days, reach normal value, explanation is effective to hypertension, hyperlipidemia, hyperglycemia, thrombosis, diabetes, cancer etc., and proof extract can be prepared other products by this consumption also effective.
The above embodiment of the present invention only is for example clearly is described, and be not qualification to embodiment of the present invention, fabricating technology scheme for affiliated field, obviously can make other multi-form variation on the basis of the above description, the product of preparation difformity and pattern need not also can't give all embodiments exhaustive here.And the product of these variations and different types thereof still is among protection scope of the present invention.
Claims (4)
1, a kind of novel substance---Phyllanthus emblica L. extract and preparation method thereof that diseases such as hypertension, hyperlipidemia, hyperglycemia, thrombosis, diabetes, cancer is had drug effect and health-care effect, it is characterized in that with fresh Phyllanthus emblica L. be raw material, technological process by clean, dewatering, softening, making beating, enucleation, alcoholization, sedimentation, separation, distillation, concentrate, drying, pulverizing, packing, irradiation finish.
2, according to the described preparation method of claim 1, softening process is to carry out under 60-80 ℃ of condition, and pure metallization processes Central Plains feed liquid and 95% proportion of ethanol are 1: 2-3; And, add pectin alcohol 550PPM with total liquid measure adding cellulase 550PPM.
3, according to the described preparation method of claim 1, prepared Phyllanthus emblica L. extract, it is characterized in that with fresh Phyllanthus emblica L. be the Phyllanthus emblica L. extract that raw material makes, be coffee-like, powdery has special little fruital flavor, detects water-soluble extractives and is no less than 60%, moisture is less than 3%, and ash is greater than 0.3%.
4,, be prepared into products such as health beverage, capsule, oral liquid, electuary, be used to prevent and treat hypertension, hyperlipidemia, hyperglycemia, thrombosis, diabetes, cancer etc. according to the prepared Phyllanthus emblica L. extract of the described preparation method of claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA021501459A CN1498653A (en) | 2002-11-09 | 2002-11-09 | Extract of 'Sheganguo' and its prepn. method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA021501459A CN1498653A (en) | 2002-11-09 | 2002-11-09 | Extract of 'Sheganguo' and its prepn. method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1498653A true CN1498653A (en) | 2004-05-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA021501459A Pending CN1498653A (en) | 2002-11-09 | 2002-11-09 | Extract of 'Sheganguo' and its prepn. method |
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| CN (1) | CN1498653A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100381434C (en) * | 2005-08-22 | 2008-04-16 | 广西中医学院 | Emblic leafflower fruit extract possessing anticancer, antibiotic actions and its manufacturing method of traditional Chinese medicine formulation |
| CN102475202A (en) * | 2010-11-29 | 2012-05-30 | 王玫 | Fructus phyllanthi pit aided lead elimination health food/drug and method for processing same |
| CN103550333A (en) * | 2013-10-24 | 2014-02-05 | 广西博士海意信息科技有限公司 | Composition for appetizing and reducing blood pressure |
| CN111789256A (en) * | 2020-07-30 | 2020-10-20 | 海南北纬十八度食品加工有限公司 | Pitaya flower polysaccharide composition with insulin balancing effect |
-
2002
- 2002-11-09 CN CNA021501459A patent/CN1498653A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100381434C (en) * | 2005-08-22 | 2008-04-16 | 广西中医学院 | Emblic leafflower fruit extract possessing anticancer, antibiotic actions and its manufacturing method of traditional Chinese medicine formulation |
| CN102475202A (en) * | 2010-11-29 | 2012-05-30 | 王玫 | Fructus phyllanthi pit aided lead elimination health food/drug and method for processing same |
| CN103550333A (en) * | 2013-10-24 | 2014-02-05 | 广西博士海意信息科技有限公司 | Composition for appetizing and reducing blood pressure |
| CN111789256A (en) * | 2020-07-30 | 2020-10-20 | 海南北纬十八度食品加工有限公司 | Pitaya flower polysaccharide composition with insulin balancing effect |
| CN111789256B (en) * | 2020-07-30 | 2022-12-30 | 海南北纬十八度食品加工有限公司 | Pitaya flower polysaccharide composition with insulin balancing effect |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |